CA2783604C - Process for epoxidation start-up - Google Patents
Process for epoxidation start-up Download PDFInfo
- Publication number
- CA2783604C CA2783604C CA2783604A CA2783604A CA2783604C CA 2783604 C CA2783604 C CA 2783604C CA 2783604 A CA2783604 A CA 2783604A CA 2783604 A CA2783604 A CA 2783604A CA 2783604 C CA2783604 C CA 2783604C
- Authority
- CA
- Canada
- Prior art keywords
- ethylene
- temperature
- catalyst
- moderator
- epoxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C11/00—Aliphatic unsaturated hydrocarbons
- C07C11/02—Alkenes
- C07C11/04—Ethene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
- C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US28739309P | 2009-12-17 | 2009-12-17 | |
| US61/287,393 | 2009-12-17 | ||
| PCT/US2010/060769 WO2011084600A2 (en) | 2009-12-17 | 2010-12-16 | Process for epoxidation start-up |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2783604A1 CA2783604A1 (en) | 2011-07-14 |
| CA2783604C true CA2783604C (en) | 2018-05-01 |
Family
ID=44152004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2783604A Expired - Fee Related CA2783604C (en) | 2009-12-17 | 2010-12-16 | Process for epoxidation start-up |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US8530682B2 (2) |
| EP (2) | EP2778157A1 (2) |
| JP (1) | JP5946772B2 (2) |
| KR (1) | KR101790254B1 (2) |
| CN (1) | CN102666514B (2) |
| BR (1) | BR112012014695A2 (2) |
| CA (1) | CA2783604C (2) |
| IN (1) | IN2012DN05178A (2) |
| MX (1) | MX2012007043A (2) |
| MY (1) | MY157612A (2) |
| RU (1) | RU2542978C2 (2) |
| TW (1) | TWI485141B (2) |
| WO (1) | WO2011084600A2 (2) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101678332A (zh) | 2007-05-09 | 2010-03-24 | 国际壳牌研究有限公司 | 环氧化催化剂及其制备方法和生产环氧烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或烷醇胺的方法 |
| IN2012DN05178A (2) * | 2009-12-17 | 2015-10-23 | Scient Design Co | |
| US20110152073A1 (en) | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
| SG193989A1 (en) | 2011-04-11 | 2013-11-29 | Dow Technology Investments Llc | Process for conditioning a high efficiency ethylene oxide catalyst |
| WO2013102177A1 (en) | 2011-12-30 | 2013-07-04 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particle and method of forming same |
| CA2987793C (en) | 2012-01-10 | 2019-11-05 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive particles having complex shapes and methods of forming same |
| WO2013177446A1 (en) | 2012-05-23 | 2013-11-28 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particles and methods of forming same |
| KR101736085B1 (ko) | 2012-10-15 | 2017-05-16 | 생-고뱅 어브레이시브즈, 인코포레이티드 | 특정한 형태들을 가진 연마 입자들 및 이러한 입자들을 형성하는 방법들 |
| CN104884443B (zh) * | 2012-12-31 | 2017-07-04 | 科学设计公司 | 用于环氧乙烷催化剂的启动方法 |
| CN105008339B (zh) * | 2013-01-11 | 2017-09-12 | 科学设计公司 | 具有后调节步骤的环氧化工艺 |
| BR112015024901B1 (pt) | 2013-03-29 | 2022-01-18 | Saint-Gobain Abrasifs | Partículas abrasivas tendo formas particulares e métodos para formar essas partículas |
| RU2643004C2 (ru) | 2013-09-30 | 2018-01-29 | Сен-Гобен Серэмикс Энд Пластикс, Инк. | Формованные абразивные частицы и способы их получения |
| CN105980368B (zh) * | 2013-12-23 | 2019-02-19 | 科学设计有限公司 | 环氧化方法 |
| CA2934938C (en) | 2013-12-31 | 2019-04-30 | Saint-Gobain Abrasives, Inc. | Abrasive article including shaped abrasive particles |
| US9771507B2 (en) | 2014-01-31 | 2017-09-26 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particle including dopant material and method of forming same |
| CN111331524B (zh) | 2014-04-14 | 2022-04-29 | 圣戈本陶瓷及塑料股份有限公司 | 包括成形磨粒的研磨制品 |
| US9914864B2 (en) | 2014-12-23 | 2018-03-13 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particles and method of forming same |
| CN107636109A (zh) | 2015-03-31 | 2018-01-26 | 圣戈班磨料磨具有限公司 | 固定磨料制品和其形成方法 |
| TWI634200B (zh) | 2015-03-31 | 2018-09-01 | 聖高拜磨料有限公司 | 固定磨料物品及其形成方法 |
| RU2017144427A (ru) * | 2015-06-02 | 2019-07-09 | Сайентифик Дизайн Компани, Инк. | Пористые тела с улучшенной архитектурой пор |
| CA3118262C (en) | 2015-06-11 | 2023-09-19 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| WO2017197002A1 (en) | 2016-05-10 | 2017-11-16 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive particles and methods of forming same |
| EP4071224A3 (en) | 2016-05-10 | 2023-01-04 | Saint-Gobain Ceramics and Plastics, Inc. | Methods of forming abrasive articles |
| WO2018064642A1 (en) | 2016-09-29 | 2018-04-05 | Saint-Gobain Abrasives, Inc. | Fixed abrasive articles and methods of forming same |
| WO2018102377A1 (en) | 2016-12-02 | 2018-06-07 | Shell Oil Company | Methods for conditioning an ethylene epoxidation catalyst and associated methods for the production of ethylene oxide |
| US10563105B2 (en) | 2017-01-31 | 2020-02-18 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| US10865148B2 (en) | 2017-06-21 | 2020-12-15 | Saint-Gobain Ceramics & Plastics, Inc. | Particulate materials and methods of forming same |
| US11059017B2 (en) | 2017-09-15 | 2021-07-13 | MultiPhase Solutions, Inc. | Halogen selective detection gas chromatography for the on-line analysis and control of selective oxidation chemical production processes |
| DK3749449T3 (da) * | 2018-02-07 | 2022-04-19 | Basf Se | Fremgangsmåde til fremstilling af en sølvimprægnerings-opløsning |
| EP4081609A4 (en) | 2019-12-27 | 2024-06-05 | Saint-Gobain Ceramics & Plastics Inc. | Abrasive articles and methods of forming same |
| EP4081370A4 (en) | 2019-12-27 | 2024-04-24 | Saint-Gobain Ceramics & Plastics Inc. | ABRASIVE ARTICLES AND THEIR FORMATION PROCESSES |
| WO2021133901A1 (en) | 2019-12-27 | 2021-07-01 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive articles and methods of forming same |
| CN113121474A (zh) * | 2019-12-30 | 2021-07-16 | 中国石油化工股份有限公司 | 乙烯环氧化银催化剂的开车方法 |
| CN114057669B (zh) * | 2020-07-29 | 2023-12-08 | 中国石油化工股份有限公司 | 一种乙烯环氧化恒温开车方法 |
| CN114436998A (zh) * | 2020-11-05 | 2022-05-06 | 中国石油化工股份有限公司 | 一种乙烯环氧化开车方法 |
| EP4457054A4 (en) | 2021-12-30 | 2026-01-14 | Saint Gobain Abrasives Inc | ABRASIVE ARTICLES AND THEIR FORMATION PROCESSES |
| WO2023130053A1 (en) | 2021-12-30 | 2023-07-06 | Saint-Gobain Abrasives, Inc. | Abrasive articles and methods of forming same |
| CN118591436A (zh) | 2021-12-30 | 2024-09-03 | 圣戈班磨料磨具有限公司 | 磨料制品及其形成方法 |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1170663A (en) | 1967-03-22 | 1969-11-12 | Shell Int Research | Process for preparing Silver Catalysts |
| US3702259A (en) | 1970-12-02 | 1972-11-07 | Shell Oil Co | Chemical production of metallic silver deposits |
| US4766105A (en) | 1986-10-31 | 1988-08-23 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4761394A (en) | 1986-10-31 | 1988-08-02 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4908343A (en) | 1987-02-20 | 1990-03-13 | Union Carbide Chemicals And Plastics Company Inc. | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5057481A (en) | 1987-02-20 | 1991-10-15 | Union Carbide Chemicals And Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US4874879A (en) * | 1988-07-25 | 1989-10-17 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
| EP0357293B1 (en) | 1988-08-30 | 1996-02-28 | Union Carbide Corporation | Catalysts for the production of ethylene oxide and their preparation processes |
| US5187140A (en) | 1989-10-18 | 1993-02-16 | Union Carbide Chemicals & Plastics Technology Corporation | Alkylene oxide catalysts containing high silver content |
| US5102848A (en) | 1990-09-28 | 1992-04-07 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5155242A (en) * | 1991-12-05 | 1992-10-13 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
| US5407888A (en) | 1992-05-12 | 1995-04-18 | Basf Aktiengesellschaft | Silver catalyst |
| US5856534A (en) | 1997-12-18 | 1999-01-05 | Arco Chemical Technology, L.P. | Epoxidation process using supported silver catalysts treated with carbon dioxide |
| JP4042332B2 (ja) * | 2001-02-27 | 2008-02-06 | 三菱化学株式会社 | レニウム含有触媒を用いるオレフィンオキシドの製造方法 |
| MX257124B (es) * | 2002-06-28 | 2008-05-14 | Shell Int Research | Metodo para iniciar un proceso de epoxidacion, catalizador y proceso de epoxidacion de una olefina. |
| CN100512966C (zh) | 2002-06-28 | 2009-07-15 | 国际壳牌研究有限公司 | 提高催化剂选择性的方法和烯烃环氧化方法 |
| DE60333292D1 (de) * | 2002-06-28 | 2010-08-19 | Shell Int Research | Verfahren für den start eines epoxierungsprozesses und epoxidierungsverfahren für olefine |
| BRPI0414766A (pt) * | 2003-09-29 | 2006-11-28 | Union Carbide Chem Plastic | processo para manufaturar óxido de etileno através da epoxidação de etileno |
| US8791280B2 (en) | 2005-08-10 | 2014-07-29 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for preparation of catalyst carrier and its use in catalyst preparation |
| US7696368B2 (en) * | 2007-05-11 | 2010-04-13 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Start-up of high selectivity catalysts in olefin oxide plants |
| US7553980B2 (en) * | 2007-09-26 | 2009-06-30 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for initiating a highly selective ethylene oxide catalyst |
| CA2723517C (en) * | 2008-05-07 | 2017-03-07 | Shell Internationale Research Maatschappij B.V. | A process for the start-up of an epoxidation process, a process for the production of ethylene oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine |
| IN2012DN05178A (2) * | 2009-12-17 | 2015-10-23 | Scient Design Co | |
| US20110152073A1 (en) | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
-
2010
- 2010-12-16 IN IN5178DEN2012 patent/IN2012DN05178A/en unknown
- 2010-12-16 WO PCT/US2010/060769 patent/WO2011084600A2/en not_active Ceased
- 2010-12-16 TW TW099144226A patent/TWI485141B/zh not_active IP Right Cessation
- 2010-12-16 KR KR1020127018627A patent/KR101790254B1/ko not_active Expired - Fee Related
- 2010-12-16 MX MX2012007043A patent/MX2012007043A/es active IP Right Grant
- 2010-12-16 EP EP20140171850 patent/EP2778157A1/en not_active Withdrawn
- 2010-12-16 US US12/970,392 patent/US8530682B2/en not_active Expired - Fee Related
- 2010-12-16 MY MYPI2012002389A patent/MY157612A/en unknown
- 2010-12-16 RU RU2012130065/04A patent/RU2542978C2/ru not_active IP Right Cessation
- 2010-12-16 JP JP2012544826A patent/JP5946772B2/ja not_active Expired - Fee Related
- 2010-12-16 EP EP10842602.4A patent/EP2513077B1/en not_active Revoked
- 2010-12-16 BR BR112012014695A patent/BR112012014695A2/pt not_active IP Right Cessation
- 2010-12-16 CN CN201080057763.XA patent/CN102666514B/zh not_active Expired - Fee Related
- 2010-12-16 CA CA2783604A patent/CA2783604C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CA2783604A1 (en) | 2011-07-14 |
| TW201136906A (en) | 2011-11-01 |
| EP2513077A4 (en) | 2013-05-22 |
| EP2778157A1 (en) | 2014-09-17 |
| KR20120106809A (ko) | 2012-09-26 |
| JP2013514387A (ja) | 2013-04-25 |
| JP5946772B2 (ja) | 2016-07-06 |
| CN102666514B (zh) | 2015-11-25 |
| KR101790254B1 (ko) | 2017-10-26 |
| MY157612A (en) | 2016-06-30 |
| BR112012014695A2 (pt) | 2015-09-15 |
| MX2012007043A (es) | 2012-07-20 |
| WO2011084600A3 (en) | 2011-11-17 |
| US20110152548A1 (en) | 2011-06-23 |
| RU2542978C2 (ru) | 2015-02-27 |
| TWI485141B (zh) | 2015-05-21 |
| IN2012DN05178A (2) | 2015-10-23 |
| US8530682B2 (en) | 2013-09-10 |
| RU2012130065A (ru) | 2014-01-27 |
| WO2011084600A2 (en) | 2011-07-14 |
| CN102666514A (zh) | 2012-09-12 |
| EP2513077B1 (en) | 2014-06-11 |
| EP2513077A2 (en) | 2012-10-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20151113 |
|
| MKLA | Lapsed |
Effective date: 20191216 |