CA2782908C - Appareil et procede pour lyophilisation continue - Google Patents

Appareil et procede pour lyophilisation continue Download PDF

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Publication number
CA2782908C
CA2782908C CA2782908A CA2782908A CA2782908C CA 2782908 C CA2782908 C CA 2782908C CA 2782908 A CA2782908 A CA 2782908A CA 2782908 A CA2782908 A CA 2782908A CA 2782908 C CA2782908 C CA 2782908C
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CA
Canada
Prior art keywords
substance
environment
desiccant
processing chamber
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2782908A
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English (en)
Other versions
CA2782908A1 (fr
Inventor
Edward Weisselberg
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Komline Sanderson Corp
Original Assignee
Wyssmont Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wyssmont Co Inc filed Critical Wyssmont Co Inc
Priority to CA2911341A priority Critical patent/CA2911341C/fr
Publication of CA2782908A1 publication Critical patent/CA2782908A1/fr
Application granted granted Critical
Publication of CA2782908C publication Critical patent/CA2782908C/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/14—Drying solid materials or objects by processes not involving the application of heat by applying pressure, e.g. wringing; by brushing; by wiping
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/40—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by drying or kilning; Subsequent reconstitution
    • A23L3/44—Freeze-drying
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/001—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement the material moving down superimposed floors
    • F26B17/003—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement the material moving down superimposed floors with fixed floors provided with scrapers
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/001—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement the material moving down superimposed floors
    • F26B17/005—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement the material moving down superimposed floors with rotating floors, e.g. around a vertical axis, which may have scrapers
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/001—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement the material moving down superimposed floors
    • F26B17/006—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement the material moving down superimposed floors the movement being imparted by oscillation or vibration
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/02—Circulating air or gases in closed cycles, e.g. wholly within the drying enclosure
    • F26B21/022—Circulating air or gases in closed cycles, e.g. wholly within the drying enclosure with provisions for changing the drying gas flow pattern, e.g. by reversing gas flow, by moving the materials or objects through subsequent compartments, at least two of which have a different direction of gas flow
    • F26B21/024—Circulating air or gases in closed cycles, e.g. wholly within the drying enclosure with provisions for changing the drying gas flow pattern, e.g. by reversing gas flow, by moving the materials or objects through subsequent compartments, at least two of which have a different direction of gas flow by using movable fan units
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/02—Circulating air or gases in closed cycles, e.g. wholly within the drying enclosure
    • F26B21/04—Circulating air or gases in closed cycles, e.g. wholly within the drying enclosure partly outside the drying enclosure
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/06—Controlling, e.g. regulating, parameters of gas supply
    • F26B21/08—Humidity
    • F26B21/083—Humidity by using sorbent or hygroscopic materials, e.g. chemical substances, molecular sieves
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

La présente invention a trait à un procédé et à un appareil pour la sublimation continue d'une substance incluant l'étape consistant à faire tomber en cascade une matière contenant une substance capable de sublimation, telle que l'eau, entre une pluralité de plateaux (130) verticalement superposés à l'intérieur d'une zone de traitement prévue à l'intérieur d'une chambre de traitement (120). Un environnement sensiblement atmosphérique est maintenu à l'intérieur de la zone de traitement à une température permettant à la substance de sublimer ce qui permet de former un sublimé à l'intérieur de l'environnement. L'environnement contenant le sublimé est mis en contact avec un siccatif tel qu'un déshydratant pour maintenir l'environnement, ce qui permet à la substance de sublimer à une pression sensiblement atmosphérique et à la température contrôlée.
CA2782908A 2009-12-11 2010-11-19 Appareil et procede pour lyophilisation continue Active CA2782908C (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CA2911341A CA2911341C (fr) 2009-12-11 2010-11-19 Appareil et procede pour lyophilisation continue

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US28406809P 2009-12-11 2009-12-11
US61/284,068 2009-12-11
US35528210P 2010-06-16 2010-06-16
US61/355,282 2010-06-16
PCT/US2010/057404 WO2011071676A1 (fr) 2009-12-11 2010-11-19 Appareil et procédé pour lyophilisation continue

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CA2911341A Division CA2911341C (fr) 2009-12-11 2010-11-19 Appareil et procede pour lyophilisation continue

Publications (2)

Publication Number Publication Date
CA2782908A1 CA2782908A1 (fr) 2011-06-16
CA2782908C true CA2782908C (fr) 2016-02-09

Family

ID=44141317

Family Applications (2)

Application Number Title Priority Date Filing Date
CA2782908A Active CA2782908C (fr) 2009-12-11 2010-11-19 Appareil et procede pour lyophilisation continue
CA2911341A Active CA2911341C (fr) 2009-12-11 2010-11-19 Appareil et procede pour lyophilisation continue

Family Applications After (1)

Application Number Title Priority Date Filing Date
CA2911341A Active CA2911341C (fr) 2009-12-11 2010-11-19 Appareil et procede pour lyophilisation continue

Country Status (4)

Country Link
US (4) US8528225B2 (fr)
EP (1) EP2509873B1 (fr)
CA (2) CA2782908C (fr)
WO (1) WO2011071676A1 (fr)

Families Citing this family (28)

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CA2782908C (fr) * 2009-12-11 2016-02-09 Edward Weisselberg Appareil et procede pour lyophilisation continue
IT1397930B1 (it) * 2009-12-23 2013-02-04 Telstar Technologies S L Metodo per monitorare l'essiccamento primario di un processo di liofilizzazione.
US20130017039A1 (en) * 2011-07-15 2013-01-17 Wyssmont Company Inc. Multi stream material processing apparatus
EP2578976A1 (fr) * 2011-10-06 2013-04-10 Sanofi Pasteur Sa Tambour rotatif à utiliser dans un lyophilisateur sous vide
US8464437B1 (en) 2012-05-25 2013-06-18 Wyssmont Company Inc. Apparatus and method for the treatment of biosolids
CN103726389B (zh) * 2013-11-26 2015-10-07 吴园园 一种浸渍干燥箱
US11781811B2 (en) 2015-08-03 2023-10-10 Gen-Probe Incorporated Apparatus for maintaining a controlled environment
KR102296720B1 (ko) 2015-08-03 2021-09-02 젠-프로브 인코포레이티드 제어된 환경을 유지하는 장치
BR112019003013A2 (pt) 2016-08-16 2019-05-14 Genzyme Corporation métodos de processamento de um fluido incluindo uma proteína terapêutica recombinante e uso do mesmo
WO2018033468A1 (fr) * 2016-08-16 2018-02-22 Universiteit Gent Procédé, appareil et récipient pour lyophilisation
US10113797B2 (en) 2016-09-09 2018-10-30 Sp Industries, Inc. Energy recovery in a freeze-drying system
CN106889058B (zh) * 2017-02-20 2019-07-19 徐小杨 一种细胞冻干系统和方法
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US20190041131A1 (en) * 2017-08-04 2019-02-07 Taylor Fresh Foods, Inc. Produce dryer distribution system
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EP3502649B1 (fr) * 2017-12-22 2021-01-27 safematic GmbH Procédé de déshydratation et de séchage de point critique
CN109289218B (zh) * 2018-09-29 2024-02-09 平顶山金晶生物科技股份有限公司 一种多糖溶液加工用干燥装置
JP7232097B2 (ja) * 2019-03-26 2023-03-02 株式会社アルバック 凍結乾燥方法及び凍結乾燥装置
CN110523096B (zh) * 2019-07-24 2022-03-04 天津科技大学 可缩短益生菌料液冷冻干燥时间的规模化干燥装置与方法
RU2729309C1 (ru) * 2019-08-07 2020-08-05 федеральное государственное бюджетное образовательное учреждение высшего образования "Национальный исследовательский университет "МЭИ" (ФГБОУ ВО "НИУ "МЭИ") Устройство для сушки
CN111397330A (zh) * 2020-03-25 2020-07-10 深圳市群卜鸿科技有限公司 一种高效且节能的封闭式回转滚筒干燥系统
CO2020004451A1 (es) 2020-04-14 2020-05-15 Biotecnologia Y Bioingenieria Core S A Reactor vertical continuo multifásico para la producción limpia de hidrocarburos y energía y proceso termoquímico realizado
US11732964B2 (en) * 2020-04-15 2023-08-22 Navinta Iii Inc Lyophilization promoting element
CN111623596A (zh) * 2020-06-23 2020-09-04 南京浩睿达环保科技有限公司 一种用于餐厨垃圾的烘干设备
CN112629170A (zh) * 2020-12-21 2021-04-09 上海大晶实业发展有限公司 一种大型冷冻式干燥机
WO2022175999A1 (fr) * 2021-02-16 2022-08-25 株式会社アルバック Appareil et procédé de lyophilisation
CN113758161B (zh) * 2021-09-02 2022-12-23 天津市康瑞药业有限公司 一种生物医药药渣脱水装置
CN114001524B (zh) * 2021-10-20 2023-02-07 江西华明纳米碳酸钙有限公司 一种新型纳米碳酸钙干燥设备

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Also Published As

Publication number Publication date
US20110138646A1 (en) 2011-06-16
US8528225B2 (en) 2013-09-10
US10551122B2 (en) 2020-02-04
US20200149816A1 (en) 2020-05-14
CA2782908A1 (fr) 2011-06-16
EP2509873A1 (fr) 2012-10-17
WO2011071676A1 (fr) 2011-06-16
US11137207B2 (en) 2021-10-05
US20180106538A1 (en) 2018-04-19
CA2911341C (fr) 2018-06-26
EP2509873A4 (fr) 2014-07-23
US9879910B2 (en) 2018-01-30
CA2911341A1 (fr) 2011-06-16
US20140007454A1 (en) 2014-01-09
EP2509873B1 (fr) 2019-03-20

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