CA2723471A1 - A method for production of inorganic nanofibres through electrostatic spinning - Google Patents
A method for production of inorganic nanofibres through electrostatic spinning Download PDFInfo
- Publication number
- CA2723471A1 CA2723471A1 CA2723471A CA2723471A CA2723471A1 CA 2723471 A1 CA2723471 A1 CA 2723471A1 CA 2723471 A CA2723471 A CA 2723471A CA 2723471 A CA2723471 A CA 2723471A CA 2723471 A1 CA2723471 A1 CA 2723471A1
- Authority
- CA
- Canada
- Prior art keywords
- solution
- spinning
- alkoxide
- nanofibres
- vinylpyrrolidone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 47
- 238000010041 electrostatic spinning Methods 0.000 title claims abstract description 35
- 238000009987 spinning Methods 0.000 claims abstract description 64
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 61
- -1 poly(vinylpyrrolidone) Polymers 0.000 claims abstract description 52
- 150000004703 alkoxides Chemical class 0.000 claims abstract description 38
- 238000000265 homogenisation Methods 0.000 claims abstract description 16
- 229910052751 metal Inorganic materials 0.000 claims abstract description 16
- 239000002184 metal Substances 0.000 claims abstract description 16
- 230000005686 electrostatic field Effects 0.000 claims abstract description 11
- 239000002738 chelating agent Substances 0.000 claims abstract description 10
- 230000007062 hydrolysis Effects 0.000 claims abstract description 7
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 7
- 239000012298 atmosphere Substances 0.000 claims abstract description 6
- 229910052755 nonmetal Inorganic materials 0.000 claims abstract description 6
- 239000002904 solvent Substances 0.000 claims abstract description 5
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical group CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 claims description 31
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 22
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 19
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 15
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 8
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 claims description 8
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 claims description 6
- WOZZOSDBXABUFO-UHFFFAOYSA-N tri(butan-2-yloxy)alumane Chemical compound [Al+3].CCC(C)[O-].CCC(C)[O-].CCC(C)[O-] WOZZOSDBXABUFO-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- SMZOGRDCAXLAAR-UHFFFAOYSA-N aluminium isopropoxide Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(C)[O-] SMZOGRDCAXLAAR-UHFFFAOYSA-N 0.000 claims description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- ZGSOBQAJAUGRBK-UHFFFAOYSA-N propan-2-olate;zirconium(4+) Chemical compound [Zr+4].CC(C)[O-].CC(C)[O-].CC(C)[O-].CC(C)[O-] ZGSOBQAJAUGRBK-UHFFFAOYSA-N 0.000 claims description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 26
- 238000001228 spectrum Methods 0.000 description 8
- 239000002105 nanoparticle Substances 0.000 description 6
- 229920000642 polymer Polymers 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 229910010272 inorganic material Inorganic materials 0.000 description 3
- 239000011147 inorganic material Substances 0.000 description 3
- 230000007774 longterm Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000006641 stabilisation Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229910002986 Li4Ti5O12 Inorganic materials 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 241001082241 Lythrum hyssopifolia Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 1
- 150000004683 dihydrates Chemical class 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001523 electrospinning Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/0007—Electro-spinning
- D01D5/0015—Electro-spinning characterised by the initial state of the material
- D01D5/003—Electro-spinning characterised by the initial state of the material the material being a polymer solution or dispersion
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/02—Heat treatment
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Inorganic Fibers (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Nonwoven Fabrics (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CZPV2008-277 | 2008-05-06 | ||
| CZ20080277A CZ2008277A3 (cs) | 2008-05-06 | 2008-05-06 | Zpusob výroby anorganických nanovláken elektrostatickým zvláknováním |
| PCT/CZ2009/000065 WO2009135448A2 (en) | 2008-05-06 | 2009-05-05 | A method for production of inorganic nanofibres through electrostatic spinning |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2723471A1 true CA2723471A1 (en) | 2009-11-12 |
Family
ID=41258174
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2723471A Abandoned CA2723471A1 (en) | 2008-05-06 | 2009-05-05 | A method for production of inorganic nanofibres through electrostatic spinning |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US20110049769A1 (cs) |
| EP (1) | EP2276880A2 (cs) |
| JP (1) | JP2011520045A (cs) |
| KR (1) | KR20100135975A (cs) |
| CN (1) | CN102084044A (cs) |
| AU (1) | AU2009243816A1 (cs) |
| BR (1) | BRPI0912221A2 (cs) |
| CA (1) | CA2723471A1 (cs) |
| CZ (1) | CZ2008277A3 (cs) |
| IL (1) | IL209135A0 (cs) |
| RU (1) | RU2010147892A (cs) |
| WO (1) | WO2009135448A2 (cs) |
Families Citing this family (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8513147B2 (en) * | 2003-06-19 | 2013-08-20 | Eastman Chemical Company | Nonwovens produced from multicomponent fibers |
| US20040260034A1 (en) | 2003-06-19 | 2004-12-23 | Haile William Alston | Water-dispersible fibers and fibrous articles |
| US7892993B2 (en) | 2003-06-19 | 2011-02-22 | Eastman Chemical Company | Water-dispersible and multicomponent fibers from sulfopolyesters |
| EP2204480B1 (en) * | 2008-12-25 | 2013-03-20 | Shinshu University | Process of manufacturing inorganic nanofibers |
| CZ2009152A3 (cs) | 2009-03-10 | 2010-11-10 | Elmarco S.R.O. | Vrstvený filtracní materiál a zarízení pro cištení plynného média |
| US8512519B2 (en) * | 2009-04-24 | 2013-08-20 | Eastman Chemical Company | Sulfopolyesters for paper strength and process |
| AT509504A1 (de) * | 2010-02-19 | 2011-09-15 | Rubacek Lukas | Verfahren zum herstellen von lithiumtitanat |
| KR101113311B1 (ko) * | 2010-03-31 | 2012-03-13 | 광주과학기술원 | 금속 산화물 나노선을 함유하는 혼합 촉매 제조방법, 이에 의해 제조된 혼합 촉매를 포함하는 전극 및 연료전지 |
| WO2013103332A2 (en) * | 2011-10-03 | 2013-07-11 | Ndsu Research Foundation | Liquid silane-based compositions and methods of fabrication |
| CN101922060B (zh) * | 2010-09-01 | 2012-07-04 | 青岛大学 | 一种稀土荧光微纳米纤维的制备方法 |
| US9273417B2 (en) | 2010-10-21 | 2016-03-01 | Eastman Chemical Company | Wet-Laid process to produce a bound nonwoven article |
| CZ2011540A3 (cs) | 2011-08-30 | 2012-10-31 | Vysoká Škola Bánská -Technická Univerzita Ostrava | Zpusob prípravy vláknitých a lamelárních mikrostruktur a nanostruktur rízeným vakuovým vymrazováním kapalinové disperze nanocástic |
| US8906200B2 (en) | 2012-01-31 | 2014-12-09 | Eastman Chemical Company | Processes to produce short cut microfibers |
| EP2850230A4 (en) * | 2012-05-16 | 2016-01-13 | Univ North Carolina State | APPARATUS AND METHOD FOR PRODUCING NANO FIBERS FROM DISPLACED SOLUTIONS UNDER CONTINUOUS RIVER |
| US9617685B2 (en) | 2013-04-19 | 2017-04-11 | Eastman Chemical Company | Process for making paper and nonwoven articles comprising synthetic microfiber binders |
| US9605126B2 (en) | 2013-12-17 | 2017-03-28 | Eastman Chemical Company | Ultrafiltration process for the recovery of concentrated sulfopolyester dispersion |
| US9598802B2 (en) | 2013-12-17 | 2017-03-21 | Eastman Chemical Company | Ultrafiltration process for producing a sulfopolyester concentrate |
| CN103752848B (zh) * | 2014-02-10 | 2016-02-03 | 南昌欧菲光科技有限公司 | 一种纳米银线的制备方法 |
| CZ308566B6 (cs) * | 2014-06-27 | 2020-12-09 | Ústav fyzikální chemie J. Heyrovského AV ČR, v. v. i. | Způsob přípravy anorganických nanovláken, zejména pro použití jako heterogenní katalyzátory, a anorganická nanovlákna |
| CN106207149A (zh) * | 2015-04-30 | 2016-12-07 | 中国电力科学研究院 | 一种制备亚微米级钛酸锂材料的方法 |
| CZ306773B6 (cs) * | 2016-04-26 | 2017-06-28 | Pardam, S.R.O. | Prekurzorové vlákno určené pro přípravu křemíkových vláken, způsob jeho výroby, způsob jeho modifikace a jeho použití |
| WO2017186201A1 (en) | 2016-04-26 | 2017-11-02 | Pardam, S.R.O. | Precursor fibers intended for preparation of silica fibers, method of manufacture thereof, method of modification thereof, use of silica fibers |
| JP6864263B2 (ja) * | 2017-03-30 | 2021-04-28 | Jnc株式会社 | チタン酸金属塩繊維の製造方法 |
| KR102248182B1 (ko) * | 2018-01-26 | 2021-05-04 | (주)엘지하우시스 | 창호용 미세먼지 필터 및 이의 제조방법 |
| CN108498868B (zh) * | 2018-04-03 | 2020-09-15 | 北京大学口腔医学院 | 具有细胞外基质电学拓扑特征的带电复合膜及其制备方法 |
| CN109082769A (zh) * | 2018-06-22 | 2018-12-25 | 西安工程大学 | 一种柔性氧化钛纳米纤维磷酸化肽富集材料的制备方法 |
| CN109095894A (zh) * | 2018-06-22 | 2018-12-28 | 西安工程大学 | 柔性金属氧化物纳米纤维磷酸化肽富集材料的制备方法 |
| CN110004519A (zh) * | 2019-04-16 | 2019-07-12 | 天津工业大学 | 一种可生产"毛毛虫"状多尺度氧化铝纤维的静电纺丝液 |
| CN111187424A (zh) * | 2020-02-14 | 2020-05-22 | 山东大学 | 镧系稀土-有机聚合物前驱体、镧系稀土氧化物纤维及制备方法与应用 |
| CN111995393B (zh) * | 2020-09-10 | 2022-04-29 | 山东大学 | 一种钛-铝聚合物前驱体制备钛酸铝陶瓷纤维的方法 |
| CN112899889B (zh) * | 2021-01-22 | 2022-06-21 | 清华大学深圳国际研究生院 | 钛酸盐纤维膜的制备方法 |
| CN113151933A (zh) * | 2021-05-21 | 2021-07-23 | 北京邮电大学 | 一种利用静电纺丝制备氧化铝纳米纤维的方法 |
| CN113307632B (zh) * | 2021-05-26 | 2022-04-12 | 山东大学 | 一种氧化物高熵陶瓷纤维的制备方法 |
| CN114560709B (zh) * | 2021-11-19 | 2023-05-02 | 东华大学 | 一种具有铰接结构的陶瓷纳米纤维气凝胶及其制备方法 |
| CN114149024B (zh) * | 2021-11-30 | 2023-07-28 | 陕西科技大学 | 一种硼掺杂多孔二氧化钛/碳纤维负极材料及制备方法 |
| CN116924798A (zh) * | 2022-04-02 | 2023-10-24 | 厦门稀土材料研究所 | 一种铬酸稀土基高熵陶瓷导电纳米纤维及其制备方法和应用 |
| CN114920552B (zh) * | 2022-05-20 | 2023-08-01 | 湘潭大学 | 一种二维纳米片的制备工艺 |
| WO2024070017A1 (ja) * | 2022-09-27 | 2024-04-04 | Jnc株式会社 | シリカ繊維製造用紡糸溶液 |
| WO2024070018A1 (ja) * | 2022-09-27 | 2024-04-04 | Jnc株式会社 | シリカ繊維およびその製造方法 |
| JP2024051672A (ja) * | 2022-09-30 | 2024-04-11 | Jnc株式会社 | 金属酸化物多孔質繊維 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4584365A (en) * | 1985-02-15 | 1986-04-22 | Manville Sales Corporation | Production of polymer from metal alkoxide and reaction mixture of carboxylic acid and hydroxy compound |
| KR910000294B1 (ko) * | 1988-07-20 | 1991-01-24 | 한국과학기술원 | 비수용액에서 중합알루미나졸의 합성방법 및 그를 이용한 알루미나 다결정질 무기섬유 제조방법 |
| JPH04263615A (ja) * | 1991-02-18 | 1992-09-18 | Colloid Res:Kk | アルミノシリケート系粘性ゾルの製造方法 |
| JP3963439B2 (ja) * | 2001-06-08 | 2007-08-22 | 日本バイリーン株式会社 | 無機系構造体の製造方法、及び無機系構造体 |
| US7575707B2 (en) * | 2005-03-29 | 2009-08-18 | University Of Washington | Electrospinning of fine hollow fibers |
| WO2006129844A1 (ja) * | 2005-05-31 | 2006-12-07 | Teijin Limited | セラミック繊維及びその製造方法 |
| CN101189283B (zh) * | 2005-05-31 | 2011-10-26 | 日东纺绩株式会社 | 由有机基硅烷化合物和硼化合物制备的聚合物 |
| US9267220B2 (en) * | 2006-03-31 | 2016-02-23 | Cornell University | Nanofibers, nanotubes and nanofiber mats comprising crystaline metal oxides and methods of making the same |
-
2008
- 2008-05-06 CZ CZ20080277A patent/CZ2008277A3/cs unknown
-
2009
- 2009-05-05 KR KR1020107027149A patent/KR20100135975A/ko not_active Withdrawn
- 2009-05-05 WO PCT/CZ2009/000065 patent/WO2009135448A2/en not_active Ceased
- 2009-05-05 AU AU2009243816A patent/AU2009243816A1/en not_active Abandoned
- 2009-05-05 EP EP09741722A patent/EP2276880A2/en not_active Withdrawn
- 2009-05-05 US US12/991,000 patent/US20110049769A1/en not_active Abandoned
- 2009-05-05 JP JP2011507784A patent/JP2011520045A/ja active Pending
- 2009-05-05 RU RU2010147892/05A patent/RU2010147892A/ru not_active Application Discontinuation
- 2009-05-05 CN CN2009801262333A patent/CN102084044A/zh active Pending
- 2009-05-05 BR BRPI0912221A patent/BRPI0912221A2/pt not_active IP Right Cessation
- 2009-05-05 CA CA2723471A patent/CA2723471A1/en not_active Abandoned
-
2010
- 2010-11-04 IL IL209135A patent/IL209135A0/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN102084044A (zh) | 2011-06-01 |
| JP2011520045A (ja) | 2011-07-14 |
| AU2009243816A1 (en) | 2009-11-12 |
| BRPI0912221A2 (pt) | 2015-10-06 |
| EP2276880A2 (en) | 2011-01-26 |
| WO2009135448A3 (en) | 2010-01-21 |
| RU2010147892A (ru) | 2012-06-20 |
| CZ2008277A3 (cs) | 2009-11-18 |
| WO2009135448A2 (en) | 2009-11-12 |
| KR20100135975A (ko) | 2010-12-27 |
| US20110049769A1 (en) | 2011-03-03 |
| IL209135A0 (en) | 2011-01-31 |
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