CA2511478A1 - Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa) - Google Patents

Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa) Download PDF

Info

Publication number
CA2511478A1
CA2511478A1 CA002511478A CA2511478A CA2511478A1 CA 2511478 A1 CA2511478 A1 CA 2511478A1 CA 002511478 A CA002511478 A CA 002511478A CA 2511478 A CA2511478 A CA 2511478A CA 2511478 A1 CA2511478 A1 CA 2511478A1
Authority
CA
Canada
Prior art keywords
catalyst
hydrogenation
psig
dimethylaminopropylamine
hydroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002511478A
Other languages
English (en)
French (fr)
Inventor
Gregory J. Ward
Bryan C. Blanchard
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solutia Inc
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US10/327,765 external-priority patent/US6660887B1/en
Application filed by Individual filed Critical Individual
Publication of CA2511478A1 publication Critical patent/CA2511478A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/755—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J25/00—Catalysts of the Raney type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J25/00—Catalysts of the Raney type
    • B01J25/02—Raney nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J25/00—Catalysts of the Raney type
    • B01J25/04—Regeneration or reactivation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA002511478A 2002-12-23 2003-12-12 Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa) Abandoned CA2511478A1 (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US10/327,765 US6660887B1 (en) 2002-12-23 2002-12-23 Low pressure process for manufacture of 3-dimethylaminopropylamine (DMAPA)
US10/327,765 2002-12-23
US10/731,733 US6951959B2 (en) 2002-12-23 2003-12-09 Low pressure process for manufacture of 3-dimethylaminopropylamine (DMAPA)
US10/731,733 2003-12-09
PCT/US2003/039447 WO2004060853A1 (en) 2002-12-23 2003-12-12 Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa)

Publications (1)

Publication Number Publication Date
CA2511478A1 true CA2511478A1 (en) 2004-07-22

Family

ID=32716859

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002511478A Abandoned CA2511478A1 (en) 2002-12-23 2003-12-12 Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa)

Country Status (10)

Country Link
EP (1) EP1575897A4 (de)
JP (1) JP2006512415A (de)
KR (1) KR20050095831A (de)
AU (1) AU2003299603A1 (de)
BR (1) BR0317706A (de)
CA (1) CA2511478A1 (de)
MX (1) MXPA05006883A (de)
PL (1) PL377466A1 (de)
RU (1) RU2326108C2 (de)
WO (1) WO2004060853A1 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7196223B2 (en) * 2005-05-03 2007-03-27 Solutia, Inc. Higher alcohols for solvents in amine production
DE102005052457A1 (de) * 2005-11-03 2007-05-10 Basf Ag Verfahren zur Synthese von DMAPA
US7939027B2 (en) 2005-11-03 2011-05-10 Basf Se Process for the synthesis of DMAPA
ATE551318T1 (de) 2008-05-13 2012-04-15 Basf Se Verfahren zur herstellung von n,n-substituierten- 1,3-propandiaminen
BR112013002105B1 (pt) * 2010-07-29 2019-04-30 Basf Se Processo para preparar um composto, mistura de dmapn e dgn, e, uso de uma mistura
JP6276048B2 (ja) * 2014-01-31 2018-02-07 広栄化学工業株式会社 アミン化合物の製造方法
CN106795095B (zh) * 2014-08-28 2020-06-26 巴斯夫欧洲公司 使用钴基全接触催化剂生产伯胺的方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2722784B3 (fr) * 1994-07-21 1996-09-06 Rhone Poulenc Chimie Procede d'hydrogenation catalytique de nitriles en amines en presence d'un catalyseur de type nickel de raney dope
US5869653A (en) * 1997-10-30 1999-02-09 Air Products And Chemicals, Inc. Hydrogenation of nitriles to produce amines
WO2000037424A1 (en) * 1998-12-22 2000-06-29 Solutia Inc Low pressure amine reactor
US6660887B1 (en) * 2002-12-23 2003-12-09 Solutia Inc. Low pressure process for manufacture of 3-dimethylaminopropylamine (DMAPA)

Also Published As

Publication number Publication date
WO2004060853A1 (en) 2004-07-22
BR0317706A (pt) 2005-11-22
KR20050095831A (ko) 2005-10-04
RU2326108C2 (ru) 2008-06-10
JP2006512415A (ja) 2006-04-13
EP1575897A1 (de) 2005-09-21
AU2003299603A1 (en) 2004-07-29
EP1575897A4 (de) 2007-03-14
RU2005123396A (ru) 2006-01-20
PL377466A1 (pl) 2006-02-06
MXPA05006883A (es) 2005-10-18

Similar Documents

Publication Publication Date Title
IL169278A (en) Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa)
JP5409393B2 (ja) エチレンアミンの製造方法
EP0913388B1 (de) Hydrierung von Nitrilen zur Herstellung von Aminen
US6087296A (en) Raney iron catalyst and a process for hydrogenating organic compounds using said catalyst
US7915454B2 (en) Method for producing ethylenediamine
US20100099872A1 (en) Production method for ethyleneamine mixtures
KR20090122437A (ko) 비처리된 ａａｎ으로부터의 에틸렌아민의 제조 방법
EP0971876B1 (de) Ein verfahren zur kontinuierlichen herstellung von adiponitril
WO1998043940A9 (en) A process for continuous hydrogenation of adiponitrile
CA2511478A1 (en) Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa)
CA2477085C (en) Method for the production of primary amines by hydrogenating nitriles
JP5565799B2 (ja) 超臨界二酸化炭素中における有機ニトリル化合物の水素化物の製造方法
KR101129878B1 (ko) 디니트릴 수소화 방법에서의 개질제의 사용
KR20010005715A (ko) 아디포니트릴의 연속 수소화 방법

Legal Events

Date Code Title Description
EEER Examination request
FZDE Discontinued
FZDE Discontinued

Effective date: 20111212