CA2483191A1 - Extraction process for separation of lipophilic compounds from urea-containing solutions - Google Patents

Extraction process for separation of lipophilic compounds from urea-containing solutions Download PDF

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Publication number
CA2483191A1
CA2483191A1 CA002483191A CA2483191A CA2483191A1 CA 2483191 A1 CA2483191 A1 CA 2483191A1 CA 002483191 A CA002483191 A CA 002483191A CA 2483191 A CA2483191 A CA 2483191A CA 2483191 A1 CA2483191 A1 CA 2483191A1
Authority
CA
Canada
Prior art keywords
process according
solution
urea
critical fluid
lipophilic compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002483191A
Other languages
English (en)
French (fr)
Inventor
Owen John Catchpole
Andrew Douglas Mackenzie
John Bertram Grey
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Callaghan Innovation Research Ltd
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2483191A1 publication Critical patent/CA2483191A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C11B7/005—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents used at superatmospheric pressures
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • C11C1/025—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by saponification and release of fatty acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Analytical Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
CA002483191A 2002-04-22 2003-04-11 Extraction process for separation of lipophilic compounds from urea-containing solutions Abandoned CA2483191A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
NZ518504 2002-04-22
NZ518504A NZ518504A (en) 2002-04-22 2002-04-22 Use of near-critical fluids in the separation of saturated and mono-unsaturated fatty acids from urea-containing solutions
PCT/NZ2003/000062 WO2003089399A1 (en) 2002-04-22 2003-04-11 Improvements in or relating to separation technology

Publications (1)

Publication Number Publication Date
CA2483191A1 true CA2483191A1 (en) 2003-10-30

Family

ID=29245084

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002483191A Abandoned CA2483191A1 (en) 2002-04-22 2003-04-11 Extraction process for separation of lipophilic compounds from urea-containing solutions

Country Status (8)

Country Link
US (1) US7709668B2 (enExample)
EP (1) EP1501782A4 (enExample)
JP (1) JP2005523323A (enExample)
KR (1) KR100972703B1 (enExample)
AU (1) AU2003222522B8 (enExample)
CA (1) CA2483191A1 (enExample)
NZ (1) NZ518504A (enExample)
WO (1) WO2003089399A1 (enExample)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100603974B1 (ko) * 2003-12-05 2006-07-25 김갑식 고체상 지질을 용매로 이용한 나노수준의 또는 비결정질입자의 제조 방법
NZ545146A (en) * 2006-02-07 2009-03-31 Ind Res Ltd Near-critical fluid fractionation process for extracting plant or animal material
ES2294956B1 (es) * 2006-09-29 2009-04-01 Universidad Autonoma De Madrid Alcoxigliceroles modificados.
WO2008153426A1 (en) * 2007-06-15 2008-12-18 Sealord Group Limited Anti-inflammatory composition and use thereof
NZ556769A (en) * 2007-07-27 2010-01-29 Ind Res Ltd Use of ionic liquids for extraction or fractionation of lipids
US10376550B2 (en) * 2007-12-12 2019-08-13 Dacy Tech Pty Ltd. Nutraceutical composition and methods of use
US8308954B2 (en) 2008-09-25 2012-11-13 Battelle Energy Alliance, Llc Methods for recovering a polar solvent from a fluid stream contaminated with at least one polar impurity
US8747673B2 (en) 2008-09-25 2014-06-10 Battelle Energy Alliance, Llc Methods for recovering a solvent from a fluid volume and methods of removing at least one compound from a nonpolar solvent
US8071656B2 (en) * 2009-03-03 2011-12-06 Dynasep Llc Nylon extraction from commingled materials
ITMI20102297A1 (it) 2010-12-15 2012-06-16 Prime Europ Therapeuticals Procedimento per stabilizzare acidi grassi poliinsaturi per mezzo di idruri metallici
CN102321005A (zh) * 2011-09-22 2012-01-18 中国海洋大学 一种亚临界流体萃取虾青素的方法
LT2800563T (lt) 2012-01-06 2018-10-25 Omthera Pharmaceuticals Inc. Laisvos rūgšties formos omega-3 polinesočiųjų riebalų rūgščių dpa praturtintos kompozicijos
JP6173437B2 (ja) 2012-05-07 2017-08-02 オムセラ・ファーマシューティカルズ・インコーポレイテッド スタチン及びω−３脂肪酸の組成物
WO2014081881A2 (en) * 2012-11-20 2014-05-30 Andrew Paul Joseph Fluid-based extractor
KR102265636B1 (ko) 2013-03-13 2021-06-16 디에스엠 뉴트리셔널 프라덕츠 아게 우레아/오일 복합체로부터 우레아 및 오일의 회수
US9163198B2 (en) 2014-01-17 2015-10-20 Orochem Technologies, Inc. Process for purification of EPA (eicosapentanoic acid) ethyl ester from fish oil
US9546125B2 (en) 2015-02-11 2017-01-17 Orochem Technologies, Inc. Continuous process for extraction of unsaturated triglycerides from fish oil
US20180187121A1 (en) * 2015-06-15 2018-07-05 White Dog Labs, Inc. Method for producing one or more oil-soluble bioproducts
CN109481333A (zh) * 2018-12-13 2019-03-19 昆明白鸥微藻技术有限公司 一种虾青素egf原液及其制备方法
CN110668945B (zh) * 2019-09-29 2022-02-15 青岛利和生物科技有限公司 一种结合超临界流体提取鱼油中dha和epa的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60214757A (ja) 1984-04-07 1985-10-28 Jgc Corp 高度不飽和脂肪酸又はそのエステルの濃縮分離方法
JPS6272793A (ja) * 1985-09-26 1987-04-03 バブコツク日立株式会社 魚油からのエイコサペンタエン酸の濃縮分離法
JPH0225447A (ja) 1988-07-13 1990-01-26 Nippon Oil & Fats Co Ltd 高度不飽和脂肪酸類の製造方法
GB8819110D0 (en) * 1988-08-11 1988-09-14 Norsk Hydro As Antihypertensive drug & method for production
SE9303446D0 (sv) 1993-10-20 1993-10-20 Trikonex Ab A novel urea fractionation process
JPH1095744A (ja) * 1996-09-20 1998-04-14 Nof Corp 高度不飽和脂肪酸又はそのアルキルエステルの製造方法
NO310113B1 (no) * 1999-08-11 2001-05-21 Norsk Hydro As Fremgangsmåte for utvinning av flerumettede fettsyrer fra ureakomplekser
ES2159257B1 (es) 1999-11-19 2002-04-16 Kd Iqa S L Nuevo procedimiento de preparacion del ester etilico del acido eicosa pentaenoico.

Also Published As

Publication number Publication date
AU2003222522A1 (en) 2003-11-03
KR100972703B1 (ko) 2010-07-27
EP1501782A1 (en) 2005-02-02
US7709668B2 (en) 2010-05-04
WO2003089399A1 (en) 2003-10-30
AU2003222522B8 (en) 2009-01-08
US20060035350A1 (en) 2006-02-16
AU2003222522B2 (en) 2008-11-27
KR20040111542A (ko) 2004-12-31
JP2005523323A (ja) 2005-08-04
NZ518504A (en) 2005-05-27
EP1501782A4 (en) 2006-11-08

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Legal Events

Date Code Title Description
EEER Examination request
FZDE Discontinued

Effective date: 20140411