CA2424754C - Process for the preparation of bicyclic diketone salts - Google Patents

Process for the preparation of bicyclic diketone salts Download PDF

Info

Publication number
CA2424754C
CA2424754C CA2424754A CA2424754A CA2424754C CA 2424754 C CA2424754 C CA 2424754C CA 2424754 A CA2424754 A CA 2424754A CA 2424754 A CA2424754 A CA 2424754A CA 2424754 C CA2424754 C CA 2424754C
Authority
CA
Canada
Prior art keywords
formula
ch2ch2
compound
preparation
sodium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA2424754A
Other languages
English (en)
French (fr)
Other versions
CA2424754A1 (en
Inventor
Hermann Schneider
Christoph Luethy
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Syngenta Participations AG
Original Assignee
Syngenta Participations AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Syngenta Participations AG filed Critical Syngenta Participations AG
Publication of CA2424754A1 publication Critical patent/CA2424754A1/en
Application granted granted Critical
Publication of CA2424754C publication Critical patent/CA2424754C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/87—Preparation of ketenes or dimeric ketenes
    • C07C45/88—Preparation of ketenes or dimeric ketenes from ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/511—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C07C45/60—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom in six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C07C49/417—Saturated compounds containing a keto group being part of a ring polycyclic
    • C07C49/423—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system
    • C07C49/427—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system having two rings
    • C07C49/443—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system having two rings the condensed ring system containing eight or nine carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/703—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups
    • C07C49/723—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups polycyclic
    • C07C49/727—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups polycyclic a keto group being part of a condensed ring system
    • C07C49/733—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups polycyclic a keto group being part of a condensed ring system having two rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D313/00—Heterocyclic compounds containing rings of more than six members having one oxygen atom as the only ring hetero atom
    • C07D313/02—Seven-membered rings
    • C07D313/06—Seven-membered rings condensed with carbocyclic rings or ring systems
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Pyrane Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA2424754A 2002-04-09 2003-04-07 Process for the preparation of bicyclic diketone salts Expired - Fee Related CA2424754C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH597/02 2002-04-09
CH5972002 2002-04-09

Publications (2)

Publication Number Publication Date
CA2424754A1 CA2424754A1 (en) 2003-10-09
CA2424754C true CA2424754C (en) 2011-01-04

Family

ID=28048299

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2424754A Expired - Fee Related CA2424754C (en) 2002-04-09 2003-04-07 Process for the preparation of bicyclic diketone salts

Country Status (16)

Country Link
US (1) US6911547B1 (enExample)
EP (1) EP1352890A1 (enExample)
JP (1) JP4294997B2 (enExample)
KR (1) KR100929789B1 (enExample)
CN (1) CN1235855C (enExample)
AR (1) AR039384A1 (enExample)
AU (1) AU2003203479B2 (enExample)
BR (1) BR0300880A (enExample)
CA (1) CA2424754C (enExample)
IL (1) IL155233A (enExample)
MX (1) MXPA03003062A (enExample)
PL (1) PL209717B1 (enExample)
RU (1) RU2315743C2 (enExample)
TW (1) TWI309642B (enExample)
UA (1) UA77947C2 (enExample)
ZA (1) ZA200302613B (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0710223D0 (en) 2007-05-29 2007-07-11 Syngenta Ltd Novel Herbicides
GB0901835D0 (en) 2009-02-04 2009-03-11 Syngenta Ltd Novel herbicides
CN103086852B (zh) * 2013-02-21 2015-10-21 南京林业大学 一种制备2,3-蒎二酮的新方法
DE102017116990B4 (de) 2017-07-27 2019-08-22 Gebr. Schmidt Fabrik für Feinmechanik GmbH & Co. KG Trennende Schutzeinrichtung
CN116041167B (zh) * 2023-01-28 2023-07-07 山东潍坊润丰化工股份有限公司 双环酮类化合物及其制备方法、双环[3.2.1]-3-辛烷-2,4-二酮的制备方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2261751C3 (de) * 1972-12-16 1981-12-24 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung von Cyclohexandionen-(1,3)
DE3314816A1 (de) * 1983-04-23 1984-10-25 Basf Ag Verfahren zur herstellung von cyclohexandionderivaten
CH680044A5 (en) * 1990-01-29 1992-06-15 Firmenich & Cie Di:methyl-oxa-bi:cyclo-octanone derivs. - useful as perfume components, with herbaceous, spicy notes for cosmetics, shampoo, etc.
JP3929545B2 (ja) 1997-03-25 2007-06-13 株式会社エス・ディー・エス バイオテック ３−アセチル−シクロペンタンカルボン酸エステルの製造方法
PT1114030E (pt) 1998-09-15 2005-09-30 Syngenta Participations Ag Piridina cetonas uteis como herbicidas
WO2000037437A1 (en) 1998-12-21 2000-06-29 Syngenta Participations Ag Novel herbicides
WO2001066522A1 (en) 2000-03-09 2001-09-13 Syngenta Participations Ag Acylated phenyl or pyridine herbicides
GT200100103A (es) 2000-06-09 2002-02-21 Nuevos herbicidas

Also Published As

Publication number Publication date
AU2003203479B2 (en) 2005-10-06
IL155233A (en) 2010-11-30
ZA200302613B (en) 2003-10-09
AR039384A1 (es) 2005-02-16
CA2424754A1 (en) 2003-10-09
JP4294997B2 (ja) 2009-07-15
BR0300880A (pt) 2004-06-22
UA77947C2 (en) 2007-02-15
RU2315743C2 (ru) 2008-01-27
TW200306304A (en) 2003-11-16
MXPA03003062A (es) 2003-10-14
PL359519A1 (en) 2003-10-20
AU2003203479A1 (en) 2003-10-23
TWI309642B (en) 2009-05-11
IL155233A0 (en) 2003-11-23
PL209717B1 (pl) 2011-10-31
JP2004002372A (ja) 2004-01-08
KR100929789B1 (ko) 2009-12-07
CN1450044A (zh) 2003-10-22
EP1352890A1 (en) 2003-10-15
CN1235855C (zh) 2006-01-11
KR20030081079A (ko) 2003-10-17
US6911547B1 (en) 2005-06-28

Similar Documents

Publication Publication Date Title
KR920000907B1 (ko) 아실화 디케톤 화합물의 제조방법
JP2012528104A (ja) 中間体としてのスピロエポキシド
CA2424754C (en) Process for the preparation of bicyclic diketone salts
Srinivas et al. Stereoselective total synthesis of (+)-varitriol
JP3929545B2 (ja) ３−アセチル−シクロペンタンカルボン酸エステルの製造方法
GB2059955A (en) Process for preparing methylvanillyl ketone
EP0127920B1 (en) A process for preparing an alkylene compound starting from a fluorocyclopropane compound
HU209916B (en) Process for preparation of 2-aryl-5-/trifluoro-methyl/-pyrrole derivatives having insecticidal, acaricidal, nematocidal activity
US5917067A (en) Process for producing an omega-functionalized aliphatic carboxylic acid and intermediate products of said process, including 2-oxepanone-7-substituted products
US4266067A (en) Process for preparing thiophene derivatives
Chou et al. Cage compounds. Part 1. Base-promoted reaction of 5, 6, 7, 8-tetrachloro-5, 8-dimethoxymethano-4a, 5, 8, 8a-tetrahydro-1, 4-naphthoquinone epoxide
EP0053950A1 (fr) Nouveau procédé de préparation de dérivés de la tétrahydro-5,6,7,7a-4H-thiéno(3,2-c)pyridinone-2
JP2011084499A (ja) ラクトン化合物の製造方法
WO2005061479A1 (ja) テトラヒドロピラン−４−オン及びピラン−４−オンの製法
Jackson et al. A photochemical route to dibenzonaphthyrones
JP2615780B2 (ja) ２−シクロペンテノン誘導体の製造法
RU2331627C2 (ru) Способ получения 7,7-диметоксибицикло[2.2.1]-гептадиена-2,5
Dong et al. Formation of β-Lactones by [2+ 2] Cycloaddition of Dichloroketene with Unreactive Carbonyl Compounds
WO2016141563A1 (zh) 脂环式环氧化合物及其制造方法、以及2-羟基-4-氧杂-5-硫杂三环[4.2.1.03，7]壬烷衍生物的制造方法
JPH0669984B2 (ja) シクロペンテノン誘導体の製造法
EP0194840A2 (en) Process for producing an aldehydelactone
Kashima et al. Synthesis of 1, 2‐benzoquinones by the oxidation of 1, 4‐benzodioxins by peroxide derivatives
SU624575A3 (ru) Способ получени производных пиридо (2,3- )пиримидина
Fu et al. Synthesis of 4-hydroxybenzo [a] pyrene
Klaus et al. Mechanistic studies in the attempted synthesis of 5, 5-dimethyl-2-isopropylidene-1, 3-cyclohexanedione

Legal Events

Date Code Title Description
EEER Examination request
MKLA Lapsed

Effective date: 20150407