CA2383728A1 - Composition adhesive a temperature d'activation basse dotee d'une resistance elevee au pelage et d'une rupture de cohesion - Google Patents
Composition adhesive a temperature d'activation basse dotee d'une resistance elevee au pelage et d'une rupture de cohesion Download PDFInfo
- Publication number
- CA2383728A1 CA2383728A1 CA002383728A CA2383728A CA2383728A1 CA 2383728 A1 CA2383728 A1 CA 2383728A1 CA 002383728 A CA002383728 A CA 002383728A CA 2383728 A CA2383728 A CA 2383728A CA 2383728 A1 CA2383728 A1 CA 2383728A1
- Authority
- CA
- Canada
- Prior art keywords
- weight
- parts
- resin composition
- resin
- polyethylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
- B32B7/04—Interconnection of layers
- B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B15/00—Layered products comprising a layer of metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B15/00—Layered products comprising a layer of metal
- B32B15/04—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B15/08—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L25/00—Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
- C08L25/02—Homopolymers or copolymers of hydrocarbons
- C08L25/04—Homopolymers or copolymers of styrene
- C08L25/06—Polystyrene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J123/00—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers
- C09J123/02—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
- C09J123/04—Homopolymers or copolymers of ethene
- C09J123/06—Polyethene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J123/00—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers
- C09J123/02—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
- C09J123/04—Homopolymers or copolymers of ethene
- C09J123/08—Copolymers of ethene
- C09J123/0807—Copolymers of ethene with unsaturated hydrocarbons only containing more than three carbon atoms
- C09J123/0815—Copolymers of ethene with aliphatic 1-olefins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J123/00—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers
- C09J123/02—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
- C09J123/04—Homopolymers or copolymers of ethene
- C09J123/08—Copolymers of ethene
- C09J123/0846—Copolymers of ethene with unsaturated hydrocarbons containing other atoms than carbon or hydrogen atoms
- C09J123/0853—Vinylacetate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/08—Copolymers of ethene
- C08L23/0807—Copolymers of ethene with unsaturated hydrocarbons only containing more than three carbon atoms
- C08L23/0815—Copolymers of ethene with aliphatic 1-olefins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/08—Copolymers of ethene
- C08L23/0846—Copolymers of ethene with unsaturated hydrocarbons containing other atoms than carbon or hydrogen atoms
- C08L23/0853—Vinylacetate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/16—Elastomeric ethene-propene or ethene-propene-diene copolymers, e.g. EPR and EPDM rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
- C08L23/20—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
- C08L23/22—Copolymers of isobutene; Butyl rubber ; Homo- or copolymers of other iso-olefins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2314/00—Polymer mixtures characterised by way of preparation
- C08L2314/06—Metallocene or single site catalysts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L25/00—Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
- C08L25/02—Homopolymers or copolymers of hydrocarbons
- C08L25/04—Homopolymers or copolymers of styrene
- C08L25/08—Copolymers of styrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L25/00—Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
- C08L25/02—Homopolymers or copolymers of hydrocarbons
- C08L25/04—Homopolymers or copolymers of styrene
- C08L25/08—Copolymers of styrene
- C08L25/10—Copolymers of styrene with conjugated dienes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2666/00—Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
- C08L2666/02—Organic macromolecular compounds, natural resins, waxes or and bituminous materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L51/00—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C08L51/06—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers grafted on to homopolymers or copolymers of aliphatic hydrocarbons containing only one carbon-to-carbon double bond
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2400/00—Presence of inorganic and organic materials
- C09J2400/10—Presence of inorganic materials
- C09J2400/16—Metal
- C09J2400/163—Metal in the substrate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Laminated Bodies (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
La présente invention concerne une composition de résine élaborée par adjonction de matières premières comprenant: (a) 0 à 90 parties en poids d'une polyoléfine, (b) 5 à 95 parties en poids d'une polyoléfine fonctionnelle, (c) 5 à 40 parties en poids d'un polystyrolène, et (d) 0 à 30 parties en poids d'un élastomère, la quantité totale des composés de (a), (b), (c) et (d) de la composition de résine étant 100 parties en poids. Dans un autre mode de réalisation, le composé (a) n'est pas un copolymère exempt d'oléfine et le composé (c) est un polystyrène à impact élevé. Les compositions de résine sont utilisées comme des adhésifs pour des substrats de polyoléfine et de métal.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US15253999P | 1999-09-03 | 1999-09-03 | |
US60/152,539 | 1999-09-03 | ||
PCT/CA2000/001017 WO2001018141A1 (fr) | 1999-09-03 | 2000-09-01 | Composition adhesive a temperature d'activation basse dotee d'une resistance elevee au pelage et d'une rupture de cohesion |
Publications (1)
Publication Number | Publication Date |
---|---|
CA2383728A1 true CA2383728A1 (fr) | 2001-03-15 |
Family
ID=22543357
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002383728A Abandoned CA2383728A1 (fr) | 1999-09-03 | 2000-09-01 | Composition adhesive a temperature d'activation basse dotee d'une resistance elevee au pelage et d'une rupture de cohesion |
Country Status (5)
Country | Link |
---|---|
KR (1) | KR100743355B1 (fr) |
CN (1) | CN100354385C (fr) |
CA (1) | CA2383728A1 (fr) |
HK (1) | HK1050911A1 (fr) |
WO (1) | WO2001018141A1 (fr) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6875813B2 (en) | 1999-05-19 | 2005-04-05 | Exxonmobil Chemical Patents Inc. | Isobutylene-based elastomer blends |
BR0110707A (pt) * | 2000-05-11 | 2003-01-28 | Exxonmobil Chem Patents Inc | Misturas de elastÈmero à base de isobutileno |
US7879949B2 (en) | 2004-10-06 | 2011-02-01 | E.I. Du Pont De Nemours And Company | Blends of ethylene copolymers with high-frequency weldability |
US20060148988A1 (en) | 2004-10-06 | 2006-07-06 | Chou Richard T | Miscible blends of ethylene copolymers with improved temperature resistance |
BRPI0506475A (pt) * | 2004-01-09 | 2007-02-06 | Du Pont | composição polimérica, pelìcula de embalagem e método de preparação de uma composição polimérica metalizável |
US7767311B2 (en) | 2004-07-29 | 2010-08-03 | E.I. Du Pont De Nemours And Company | Adhesive compositions derived from highly functionalized ethylene copolymers |
FR2896249A1 (fr) * | 2006-01-16 | 2007-07-20 | Arkema Sa | Liant a base de polyethylene greffe et de polystyrene choc ou cristal a rupture cohesive |
CN101896567B (zh) * | 2008-02-05 | 2014-04-30 | 三井-杜邦聚合化学株式会社 | 粘合性树脂组合物及粘合膜或片材 |
US9000091B2 (en) | 2009-01-08 | 2015-04-07 | Equistar Chemicals, Lp | Preparation of polyolefin-based adhesives |
US8378025B2 (en) * | 2010-03-12 | 2013-02-19 | Equistar Chemicals, Lp | Adhesive composition |
US20120196138A1 (en) * | 2011-01-27 | 2012-08-02 | Equistar Chemicals, Lp | Process for forming multilayer structures containing a metal layer |
CN102128317A (zh) * | 2011-03-15 | 2011-07-20 | 广东联塑科技实业有限公司 | 一种pe-rt钢丝网骨架复合管及其制备方法和应用 |
EP2692780B1 (fr) * | 2011-03-30 | 2016-11-16 | Kuraray Co., Ltd. | Procédé de production d'une résine à base d'un copolymère d'éthylène/alcool vinylique, résine à base d'un copolymère d'éthylène/alcool vinylique, et structure multicouche |
CN102585729A (zh) * | 2011-12-15 | 2012-07-18 | 广州市合诚化学有限公司 | 一种低熔点粘接树脂及其制备方法与应用 |
JP6229208B2 (ja) * | 2013-11-05 | 2017-11-15 | 三菱ケミカル株式会社 | 粘着剤組成物 |
KR101540740B1 (ko) * | 2013-11-22 | 2015-07-30 | 롯데케미칼 주식회사 | 접착성 수지 조성물 및 알루미늄 복합 판넬 |
DE102014218260A1 (de) | 2014-09-11 | 2016-03-17 | Albis Plastic Gmbh | Haftungsmodifizierte olefinische thermoplastische Elastomere, insbesondere TPE-V, TPE-O |
CN106905892B (zh) * | 2016-09-23 | 2021-05-28 | 厦门内加湖新材料科技有限公司 | 一种基于非极性聚烯烃树脂的粘合剂 |
DE102016124555A1 (de) * | 2016-12-15 | 2018-06-21 | Nora Systems Gmbh | Bodenbelag und Verfahren zu dessen Herstellung |
CN109321172A (zh) * | 2018-10-17 | 2019-02-12 | 河源市普立隆新材料科技有限公司 | 铝塑板用粘接树脂、其制备方法及铝塑板 |
CN111154427B (zh) * | 2019-12-30 | 2022-06-21 | 河源市普立隆新材料科技有限公司 | 一种铝天花板胶膜结构及其铝天花板结构 |
CN114854332A (zh) * | 2021-02-04 | 2022-08-05 | 厦门内加湖新材料科技有限公司 | 粘合剂组合物、锂电池包材以及锂电池 |
KR102650069B1 (ko) * | 2021-10-12 | 2024-03-21 | 주식회사 알앤에프케미칼 | 고내열성 마스킹 필름 |
CN114231211A (zh) * | 2021-12-30 | 2022-03-25 | 上海邦中高分子材料股份有限公司 | 一种以药液浸泡为钢管前处理方式的衬塑复合管专用粘接树脂及其制备方法 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA1206312A (fr) * | 1981-10-08 | 1986-06-24 | Seymour Schmukler | Structures composites, et leur fabrication |
JPS5983651A (ja) * | 1982-11-06 | 1984-05-15 | 住友ベークライト株式会社 | 包装体 |
JPS6114272A (ja) * | 1984-06-29 | 1986-01-22 | Ube Ind Ltd | 接着性ポリエチレン組成物及びその金属積層体 |
EP0188901B1 (fr) * | 1984-12-20 | 1991-06-12 | Mitsui Petrochemical Industries, Ltd. | Composition adhésive de matière synthétique |
JPH0641544B2 (ja) * | 1985-06-26 | 1994-06-01 | 三井石油化学工業株式会社 | 熱可塑性樹脂組成物 |
KR930011760B1 (ko) * | 1989-08-07 | 1993-12-20 | 미쓰이 세끼유 가가꾸 고오교오 가부시끼가이샤 | 접착제 수지조성물, 이 조성물을 접착층으로 하는 적층체 및 그의 제조방법 |
US5597865A (en) * | 1994-11-21 | 1997-01-28 | Quantum Chemical Corporation | Adhesive blends for polystyrene |
CA2237917A1 (fr) * | 1997-05-20 | 1998-11-20 | Mitsui Chemicals, Incorporated | Composition de resine adhesive |
-
2000
- 2000-09-01 CA CA002383728A patent/CA2383728A1/fr not_active Abandoned
- 2000-09-01 CN CNB008141495A patent/CN100354385C/zh not_active Expired - Lifetime
- 2000-09-01 KR KR1020027002888A patent/KR100743355B1/ko active IP Right Grant
- 2000-09-01 WO PCT/CA2000/001017 patent/WO2001018141A1/fr active Application Filing
-
2003
- 2003-05-05 HK HK03103185A patent/HK1050911A1/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
HK1050911A1 (en) | 2003-07-11 |
KR20020034183A (ko) | 2002-05-08 |
KR100743355B1 (ko) | 2007-07-26 |
CN100354385C (zh) | 2007-12-12 |
CN1378579A (zh) | 2002-11-06 |
WO2001018141A1 (fr) | 2001-03-15 |
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Legal Events
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EEER | Examination request | ||
FZDE | Dead |