CA2347697A1 - Procede et dispositif permettant d'explorer des bibliotheques de catalyseurs - Google Patents
Procede et dispositif permettant d'explorer des bibliotheques de catalyseurs Download PDFInfo
- Publication number
- CA2347697A1 CA2347697A1 CA002347697A CA2347697A CA2347697A1 CA 2347697 A1 CA2347697 A1 CA 2347697A1 CA 002347697 A CA002347697 A CA 002347697A CA 2347697 A CA2347697 A CA 2347697A CA 2347697 A1 CA2347697 A1 CA 2347697A1
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- CA
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- Prior art keywords
- catalyst
- orifice
- product
- sampling
- library
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
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Classifications
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- G01N31/10—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
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- H01J49/161—Ion sources; Ion guns using surface ionisation, e.g. field-, thermionic- or photo-emission using photoionisation, e.g. by laser
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- B01J2219/00653—Making arrays on substantially continuous surfaces the compounds being bound to electrodes embedded in or on the solid supports
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/0068—Means for controlling the apparatus of the process
- B01J2219/00702—Processes involving means for analysing and characterising the products
- B01J2219/00704—Processes involving means for analysing and characterising the products integrated with the reactor apparatus
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
- B01J2219/00747—Catalysts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
- B01J2219/0075—Metal based compounds
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- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B30/00—Methods of screening libraries
- C40B30/08—Methods of screening libraries by measuring catalytic activity
-
- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B40/00—Libraries per se, e.g. arrays, mixtures
- C40B40/18—Libraries containing only inorganic compounds or inorganic materials
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- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Plasma & Fusion (AREA)
- Engineering & Computer Science (AREA)
- Optics & Photonics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Sampling And Sample Adjustment (AREA)
- Catalysts (AREA)
Abstract
L'invention concerne un procédé permettant d'explorer rapidement les activités et les sélectivités de bibliothèques de catalyseurs ayant des sites adressables par mise en contact de catalyseurs potentiels, aux sites d'essai, avec des flux réactifs formant des plumes de produits au niveau de ces sites. On analyse les plumes de produits en transférant une sonde échantillon et/ou la bibliothèque à une position telle qu'un site adressable soit proche de l'orifice d'échantillonnage de la sonde échantillon, puis en faisant passer une partie des produits de réaction par cet orifice, de manière à former un volume étendu de jet libre dans au moins une zone de vide et à faire passer ensuite une partie du jet sous pression refroidi et réduit par l'orifice d'admission d'un spectromètre de masse aux fins d'analyse. Il est possible de combiner cette analyse avec tel ou tel procédé de détection en ionisation multiphotonique améliorée par résonance pour assurer une évaluation très rapide des bibliothèques. L'invention concerne également des réacteurs, des microréacteurs et des microsondes échantillons de transfert de produit que l'on peut utiliser de manière appropriée pour le transfert de produits vers un spectromètre de masse.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US19184998A | 1998-11-12 | 1998-11-12 | |
| US09/191,849 | 1998-11-12 | ||
| PCT/GB1999/003767 WO2000029844A1 (fr) | 1998-11-12 | 1999-11-11 | Procede et dispositif permettant d'explorer des bibliotheques de catalyseurs |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2347697A1 true CA2347697A1 (fr) | 2000-05-25 |
Family
ID=22707151
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002347697A Abandoned CA2347697A1 (fr) | 1998-11-12 | 1999-11-11 | Procede et dispositif permettant d'explorer des bibliotheques de catalyseurs |
Country Status (13)
| Country | Link |
|---|---|
| EP (1) | EP1129348A1 (fr) |
| JP (1) | JP2002530647A (fr) |
| KR (1) | KR20010092734A (fr) |
| CN (1) | CN1333871A (fr) |
| AU (1) | AU1064200A (fr) |
| BR (1) | BR9915268A (fr) |
| CA (1) | CA2347697A1 (fr) |
| ID (1) | ID29172A (fr) |
| MX (1) | MXPA01004785A (fr) |
| NO (1) | NO20012341D0 (fr) |
| NZ (1) | NZ511228A (fr) |
| PL (1) | PL348157A1 (fr) |
| WO (1) | WO2000029844A1 (fr) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19642261A1 (de) * | 1996-10-11 | 1998-04-16 | Hoechst Ag | Verfahren und Vorrichtung zum Erkennen der katalytischen Aktivität von Feststoffen |
| US7491677B2 (en) | 1999-01-15 | 2009-02-17 | Basf Catalysts Llc | Combinatorial synthesis |
| DE19959973A1 (de) * | 1999-12-13 | 2001-06-21 | Basf Ag | Verfahren zur kombinatorischen Herstellung und Testung von Heterogenkatalysatoren |
| WO2002014854A1 (fr) * | 2000-08-14 | 2002-02-21 | Chevron U.S.A. Inc. | Utilisation de reacteurs a microcanaux en chimie combinatoire |
| US6864091B1 (en) | 2000-08-31 | 2005-03-08 | Symyx Technologies, Inc. | Sampling probe |
| US6692708B2 (en) | 2001-04-05 | 2004-02-17 | Symyx Technologies, Inc. | Parallel reactor for sampling and conducting in situ flow-through reactions and a method of using same |
| DE10117274B4 (de) * | 2001-04-06 | 2005-03-03 | Hte Ag The High Throughput Experimentation Company | Verfahren zur Analyse und Archivierung von wenigstens einer Materialbibliothek |
| DE10117275B4 (de) * | 2001-04-06 | 2005-02-24 | Hte Ag The High Throughput Experimentation Company | Vorrichtung zur Archivierung und Analyse von Materialien |
| WO2002094431A2 (fr) * | 2001-05-23 | 2002-11-28 | Nanoscape Ag | Laboratoire de chimie miniature integre |
| US6838052B2 (en) | 2001-06-29 | 2005-01-04 | Symyx Technologies, Inc. | In-situ injection and materials screening device |
| US6923939B1 (en) | 2001-07-05 | 2005-08-02 | Uop Llc | Heat activated membrane introduction apparatus and method for screening materials |
| US6949267B2 (en) | 2002-04-08 | 2005-09-27 | Engelhard Corporation | Combinatorial synthesis |
| WO2005033712A1 (fr) * | 2002-10-29 | 2005-04-14 | E. I. Du Pont De Nemours And Company | Procede et appareil pour mettre en oeuvre des reactions chimiques dans une pluralite d'echantillons |
| CN1695061A (zh) | 2002-10-29 | 2005-11-09 | 纳幕尔杜邦公司 | 对多个试样进行化学反应的方法和装置 |
| US7390664B2 (en) | 2002-12-20 | 2008-06-24 | Exxonmobil Research And Engineering Company | Method and apparatus for high throughput catalysts screening and optimization |
| CN105784917B (zh) * | 2014-12-26 | 2018-06-29 | 中国科学院大连化学物理研究所 | 质谱仪在检测催化反应离子化中间体过程中的应用 |
| CN105823820B (zh) * | 2015-11-13 | 2019-02-15 | 亚申科技研发中心（上海）有限公司 | 催化剂评价装置 |
| CN110100162B (zh) * | 2016-12-22 | 2022-08-30 | 文塔纳医疗系统公司 | 用于样本处理的系统和方法 |
| CN107024560B (zh) * | 2017-02-24 | 2023-11-21 | 金华职业技术学院 | 一种用于气体与反应面多相催化的测试装置 |
| GB2566326A (en) * | 2017-09-11 | 2019-03-13 | Owlstone Inc | Ion mobility filter |
| CN109884168B (zh) * | 2017-12-06 | 2021-11-05 | 中国科学院大连化学物理研究所 | 一种用于催化反应过程实时在线分析的装置及方法 |
| CN113295763B (zh) * | 2021-06-03 | 2023-07-25 | 浙江师范大学 | 一种可消除反应物背景信号干扰的交叉分子束探测装置 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR900005250B1 (ko) * | 1986-10-28 | 1990-07-21 | 몬산토 캄파니 | 촉매화 화학반응을 수행하고, 촉매작용을 연구하기 위한 방법과 장치 |
| US6063633A (en) * | 1996-02-28 | 2000-05-16 | The University Of Houston | Catalyst testing process and apparatus |
| EP0934515B1 (fr) * | 1996-10-09 | 2006-03-08 | Symyx Technologies, Inc. | Spectroscopie a infrarouge et imagerie des bibliotheques |
| JP2001520380A (ja) * | 1997-10-10 | 2001-10-30 | ビーピー ケミカルズ リミテッド | 触媒評価のための触媒ライブラリの照射活性化およびスクリーニング並びにそのための反応器 |
-
1999
- 1999-11-11 MX MXPA01004785A patent/MXPA01004785A/es unknown
- 1999-11-11 NZ NZ511228A patent/NZ511228A/xx unknown
- 1999-11-11 KR KR1020017005945A patent/KR20010092734A/ko not_active Application Discontinuation
- 1999-11-11 PL PL99348157A patent/PL348157A1/xx unknown
- 1999-11-11 EP EP99954228A patent/EP1129348A1/fr not_active Withdrawn
- 1999-11-11 AU AU10642/00A patent/AU1064200A/en not_active Abandoned
- 1999-11-11 JP JP2000582796A patent/JP2002530647A/ja active Pending
- 1999-11-11 CA CA002347697A patent/CA2347697A1/fr not_active Abandoned
- 1999-11-11 CN CN99815596A patent/CN1333871A/zh active Pending
- 1999-11-11 BR BR9915268-1A patent/BR9915268A/pt not_active Application Discontinuation
- 1999-11-11 WO PCT/GB1999/003767 patent/WO2000029844A1/fr not_active Application Discontinuation
- 1999-11-11 ID IDW00200101044A patent/ID29172A/id unknown
-
2001
- 2001-05-11 NO NO20012341A patent/NO20012341D0/no not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| WO2000029844A1 (fr) | 2000-05-25 |
| KR20010092734A (ko) | 2001-10-26 |
| NZ511228A (en) | 2003-01-31 |
| ID29172A (id) | 2001-08-09 |
| PL348157A1 (en) | 2002-05-06 |
| NO20012341L (no) | 2001-05-11 |
| NO20012341D0 (no) | 2001-05-11 |
| MXPA01004785A (es) | 2002-05-06 |
| BR9915268A (pt) | 2001-08-07 |
| AU1064200A (en) | 2000-06-05 |
| JP2002530647A (ja) | 2002-09-17 |
| CN1333871A (zh) | 2002-01-30 |
| EP1129348A1 (fr) | 2001-09-05 |
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