CA2203352C - Methode et appareil pour purifier une substance - Google Patents
Methode et appareil pour purifier une substance Download PDFInfo
- Publication number
- CA2203352C CA2203352C CA002203352A CA2203352A CA2203352C CA 2203352 C CA2203352 C CA 2203352C CA 002203352 A CA002203352 A CA 002203352A CA 2203352 A CA2203352 A CA 2203352A CA 2203352 C CA2203352 C CA 2203352C
- Authority
- CA
- Canada
- Prior art keywords
- column
- distillation column
- heat exchange
- distillation
- bottoms
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000126 substance Substances 0.000 title claims abstract description 43
- 238000000034 method Methods 0.000 title claims abstract description 26
- 238000004821 distillation Methods 0.000 claims abstract description 110
- 239000012535 impurity Substances 0.000 claims abstract description 47
- 239000012530 fluid Substances 0.000 claims abstract description 32
- 230000001174 ascending effect Effects 0.000 claims abstract description 16
- 239000012808 vapor phase Substances 0.000 claims abstract description 16
- 238000009833 condensation Methods 0.000 claims abstract description 13
- 230000005494 condensation Effects 0.000 claims abstract description 13
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 8
- 238000009835 boiling Methods 0.000 claims abstract 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical group O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 17
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 15
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
- 239000001569 carbon dioxide Substances 0.000 claims description 11
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 11
- CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 claims description 10
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 claims description 10
- 229910000077 silane Inorganic materials 0.000 claims description 9
- 230000008016 vaporization Effects 0.000 claims description 9
- 239000002826 coolant Substances 0.000 claims description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 239000001257 hydrogen Substances 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 6
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 229910000042 hydrogen bromide Inorganic materials 0.000 claims description 5
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 4
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 3
- MROCJMGDEKINLD-UHFFFAOYSA-N dichlorosilane Chemical compound Cl[SiH2]Cl MROCJMGDEKINLD-UHFFFAOYSA-N 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 3
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 3
- 238000009834 vaporization Methods 0.000 claims description 3
- 239000001294 propane Substances 0.000 claims description 2
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 claims description 2
- 239000005052 trichlorosilane Substances 0.000 claims description 2
- 238000005485 electric heating Methods 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 238000012856 packing Methods 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000010992 reflux Methods 0.000 description 4
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- -1 siloxanes Chemical class 0.000 description 3
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000013529 heat transfer fluid Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 239000010937 tungsten Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 239000005046 Chlorosilane Substances 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 150000001649 bromium compounds Chemical class 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000009972 noncorrosive effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000012264 purified product Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/04—Hydrides of silicon
- C01B33/046—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Silicon Compounds (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US66014796A | 1996-06-07 | 1996-06-07 | |
| US08/660,147 | 1996-06-07 | ||
| US08/781,463 US5735141A (en) | 1996-06-07 | 1997-01-10 | Method and apparatus for purifying a substance |
| US08/781,463 | 1997-01-10 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2203352A1 CA2203352A1 (fr) | 1997-12-07 |
| CA2203352C true CA2203352C (fr) | 2000-08-01 |
Family
ID=27097989
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002203352A Expired - Fee Related CA2203352C (fr) | 1996-06-07 | 1997-04-22 | Methode et appareil pour purifier une substance |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP0811815B1 (fr) |
| JP (1) | JP4050805B2 (fr) |
| CN (1) | CN1172685A (fr) |
| CA (1) | CA2203352C (fr) |
| DE (1) | DE69714912T2 (fr) |
| ID (1) | ID17773A (fr) |
| SG (1) | SG50828A1 (fr) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5066309B2 (ja) | 1999-04-05 | 2012-11-07 | 株式会社日本触媒 | 易重合性物質含有物の精製方法 |
| JP2001081050A (ja) * | 1999-09-10 | 2001-03-27 | Nippon Shokubai Co Ltd | 易重合性化合物の取り扱い装置および取り扱い方法 |
| WO2005094986A1 (fr) | 2004-03-30 | 2005-10-13 | Taiyo Nippon Sanso Corporation | Purificateur de pre-traitement d'appareil de separation a liquefaction d'air et, pour y etre utilise, adsorbant d'hydrocarbures et procede de pre-traitement d'air brut |
| KR101159674B1 (ko) * | 2009-11-16 | 2012-06-25 | 주식회사 케이씨씨 | 모노실란의 정제방법 |
| JP5767243B2 (ja) * | 2009-12-17 | 2015-08-19 | ダウ グローバル テクノロジーズ エルエルシー | 塩素ガス製造 |
| US8524048B2 (en) | 2010-10-05 | 2013-09-03 | Memc Electronic Materials, Inc. | Processes for recovering silane from heavy-ends separation operations |
| US8524045B2 (en) | 2010-10-05 | 2013-09-03 | Memc Electronic Materials, Inc. | Systems for purifying silane |
| CN103153420B (zh) * | 2010-10-05 | 2015-06-17 | Memc电子材料有限公司 | 纯化硅烷的方法和系统 |
| US8524044B2 (en) | 2010-10-05 | 2013-09-03 | Memc Electronic Materials, Inc. | Systems for recovering silane from heavy-ends separation operations |
| KR101309030B1 (ko) * | 2011-06-16 | 2013-09-17 | 코아텍주식회사 | 고순도 염화수소 제조방법 및 장치 |
| WO2013101431A1 (fr) | 2011-12-30 | 2013-07-04 | Memc Electronic Materials, Inc. | Procédés et systèmes pour l'épuration de silane |
| CN103242126A (zh) * | 2012-02-03 | 2013-08-14 | 青岛伊科思技术工程有限公司 | 一种高纯度1,2-丁二烯的生产方法 |
| CN103922414B (zh) * | 2014-04-30 | 2016-04-13 | 邯郸净化设备研究所 | 一种连续精馏纯化六氟化钨的方法及装置 |
| CN110963494B (zh) * | 2019-12-13 | 2023-04-07 | 内蒙古兴洋科技股份有限公司 | 一种制备硅烷的系统和方法 |
| CN115321486B (zh) * | 2022-07-23 | 2023-11-17 | 四川红华实业有限公司 | 电子级别三氟化氯纯化方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2901406A (en) * | 1955-02-18 | 1959-08-25 | Exxon Research Engineering Co | Separation of liquids by altering their relative volatilities |
| FR1441627A (fr) * | 1965-04-26 | 1966-06-10 | Rhone Poulenc Sa | Procédé d'isolement de produits à point de fusion élevé |
| US4284423A (en) * | 1978-02-15 | 1981-08-18 | Exxon Research & Engineering Co. | Separation of carbon dioxide and other acid gas components from hydrocarbon feeds containing admixtures of methane and hydrogen |
-
1997
- 1997-04-22 CA CA002203352A patent/CA2203352C/fr not_active Expired - Fee Related
- 1997-05-06 ID IDP971510A patent/ID17773A/id unknown
- 1997-05-09 SG SG1997001432A patent/SG50828A1/en unknown
- 1997-06-04 JP JP14636197A patent/JP4050805B2/ja not_active Expired - Fee Related
- 1997-06-05 EP EP97303871A patent/EP0811815B1/fr not_active Expired - Lifetime
- 1997-06-05 DE DE69714912T patent/DE69714912T2/de not_active Expired - Lifetime
- 1997-06-06 CN CN97105531A patent/CN1172685A/zh active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| SG50828A1 (en) | 1998-07-20 |
| JPH1066801A (ja) | 1998-03-10 |
| JP4050805B2 (ja) | 2008-02-20 |
| EP0811815B1 (fr) | 2002-08-28 |
| EP0811815A2 (fr) | 1997-12-10 |
| CA2203352A1 (fr) | 1997-12-07 |
| DE69714912D1 (de) | 2002-10-02 |
| CN1172685A (zh) | 1998-02-11 |
| EP0811815A3 (fr) | 1998-03-25 |
| DE69714912T2 (de) | 2003-03-20 |
| ID17773A (id) | 1998-01-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |