CA2113799A1 - Thin film depolymerization to dimeric cyclic esters - Google Patents

Thin film depolymerization to dimeric cyclic esters

Info

Publication number
CA2113799A1
CA2113799A1 CA 2113799 CA2113799A CA2113799A1 CA 2113799 A1 CA2113799 A1 CA 2113799A1 CA 2113799 CA2113799 CA 2113799 CA 2113799 A CA2113799 A CA 2113799A CA 2113799 A1 CA2113799 A1 CA 2113799A1
Authority
CA
Canada
Prior art keywords
oligomer
cyclic ester
evaporator
film
lactic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA 2113799
Other languages
English (en)
French (fr)
Inventor
Kamlesh Kumar Bhatia
Kang Lin
Robert Stephen Nash
Thomas Walter Stambaugh
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2113799A1 publication Critical patent/CA2113799A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D319/00Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D319/101,4-Dioxanes; Hydrogenated 1,4-dioxanes
    • C07D319/121,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/22Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • B01D1/222In rotating vessels; vessels with movable parts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1887Stationary reactors having moving elements inside forming a thin film
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J6/00Heat treatments such as Calcining; Fusing ; Pyrolysis

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
CA 2113799 1991-07-24 1992-07-23 Thin film depolymerization to dimeric cyclic esters Abandoned CA2113799A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US73497791A 1991-07-24 1991-07-24
US07/734,977 1991-07-24

Publications (1)

Publication Number Publication Date
CA2113799A1 true CA2113799A1 (en) 1993-02-04

Family

ID=24953831

Family Applications (1)

Application Number Title Priority Date Filing Date
CA 2113799 Abandoned CA2113799A1 (en) 1991-07-24 1992-07-23 Thin film depolymerization to dimeric cyclic esters

Country Status (6)

Country Link
EP (1) EP0641336A1 (ja)
JP (1) JP3255413B2 (ja)
AU (1) AU2374092A (ja)
CA (1) CA2113799A1 (ja)
TW (1) TW211577B (ja)
WO (1) WO1993002075A1 (ja)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6326458B1 (en) * 1992-01-24 2001-12-04 Cargill, Inc. Continuous process for the manufacture of lactide and lactide polymers
US6005067A (en) 1992-01-24 1999-12-21 Cargill Incorporated Continuous process for manufacture of lactide polymers with controlled optical purity
US5686630A (en) * 1993-09-29 1997-11-11 Chronopol, Inc. Purifying cyclic esters by aqueous solvent extraction
US5338822A (en) * 1992-10-02 1994-08-16 Cargill, Incorporated Melt-stable lactide polymer composition and process for manufacture thereof
AU5296393A (en) * 1992-10-02 1994-04-26 Cargill Incorporated Paper having a melt-stable lactide polymer coating and process for manufacture thereof
US6005068A (en) 1992-10-02 1999-12-21 Cargill Incorporated Melt-stable amorphous lactide polymer film and process for manufacture thereof
US5359026A (en) * 1993-07-30 1994-10-25 Cargill, Incorporated Poly(lactide) copolymer and process for manufacture thereof
BE1008099A3 (fr) * 1994-03-04 1996-01-16 Brussels Biotech Sa Production semi-continue de polylactides par ouverture de cycle lactides obtenus a partir de derives d'acide lactique.
US5830991A (en) * 1996-02-09 1998-11-03 Kureha Kagaku Kagyo Kk Preparation process and purification process of dimeric cyclic ester of hydroxycarboxylic acid
US6313319B1 (en) 1998-09-25 2001-11-06 Shimadzu Corporation Method for purifying lactide and lactide for food additives
US7005496B2 (en) * 2003-07-24 2006-02-28 Shell Oil Company Production of trimethylene carbonate from poly (trimethylene carbonate) by wiped film reactive evaporation
AT412951B (de) * 2003-10-02 2005-09-26 Vtu Engineering Planungs Und B Dünnschichtverdampfer
JP4696824B2 (ja) * 2005-10-07 2011-06-08 株式会社日立プラントテクノロジー ポリエステルの製造方法及びポリエステルの製造装置
JP5098233B2 (ja) * 2006-06-30 2012-12-12 株式会社日立プラントテクノロジー ポリヒドロキシカルボン酸合成方法及び装置
JP5489720B2 (ja) * 2006-11-28 2014-05-14 ピュラック バイオケム ビー. ブイ. 安定なラクチド粒子
JP4650427B2 (ja) * 2007-01-04 2011-03-16 株式会社日立プラントテクノロジー 遠心薄膜蒸発装置及びその運転方法
JP5229268B2 (ja) * 2010-05-10 2013-07-03 株式会社日立プラントテクノロジー ポリ乳酸の合成装置及び方法
EP2559725B1 (de) * 2011-08-19 2024-05-08 Uhde Inventa-Fischer GmbH Verfahren und Vorrichtung zur Rückgewinnung von Lactid aus Polylactid bzw. Glycolid aus Polyglycolid
CN105536653A (zh) * 2015-12-22 2016-05-04 江苏瑞安特重型机械有限公司 一种处理高粘物料的熔融混合器
CN111013520B (zh) * 2019-12-23 2022-04-05 重庆市天友乳业股份有限公司 一种固体乳酸的制备工艺

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5023349A (en) * 1990-05-08 1991-06-11 E. I. Du Pont De Nemours And Company Continuous process for rapid conversion of oligomers to cyclic esters

Also Published As

Publication number Publication date
JP3255413B2 (ja) 2002-02-12
AU2374092A (en) 1993-02-23
WO1993002075A1 (en) 1993-02-04
EP0641336A1 (en) 1995-03-08
JPH07500091A (ja) 1995-01-05
TW211577B (ja) 1993-08-21

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Legal Events

Date Code Title Description
FZDE Dead