CA1103650A - Treatment of silica - Google Patents
Treatment of silicaInfo
- Publication number
- CA1103650A CA1103650A CA289,418A CA289418A CA1103650A CA 1103650 A CA1103650 A CA 1103650A CA 289418 A CA289418 A CA 289418A CA 1103650 A CA1103650 A CA 1103650A
- Authority
- CA
- Canada
- Prior art keywords
- silica
- compounds
- process according
- treatment
- hydrothermal treatment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 138
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 69
- 238000011282 treatment Methods 0.000 title claims description 24
- 238000010335 hydrothermal treatment Methods 0.000 claims abstract description 29
- 150000001875 compounds Chemical class 0.000 claims abstract description 28
- 239000011148 porous material Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 239000007788 liquid Substances 0.000 claims description 13
- 239000003054 catalyst Substances 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 7
- 238000001354 calcination Methods 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 5
- 239000004215 Carbon black (E152) Substances 0.000 claims description 4
- 229910052791 calcium Inorganic materials 0.000 claims description 4
- 229930195733 hydrocarbon Natural products 0.000 claims description 4
- 150000002430 hydrocarbons Chemical class 0.000 claims description 4
- 229910052700 potassium Inorganic materials 0.000 claims description 4
- 230000008929 regeneration Effects 0.000 claims description 4
- 238000011069 regeneration method Methods 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 229910052792 caesium Inorganic materials 0.000 claims description 2
- 229910052744 lithium Inorganic materials 0.000 claims description 2
- 229910052701 rubidium Inorganic materials 0.000 claims description 2
- 229910052712 strontium Inorganic materials 0.000 claims description 2
- 229910052788 barium Inorganic materials 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 230000001172 regenerating effect Effects 0.000 claims 1
- 238000002474 experimental method Methods 0.000 description 10
- 230000000694 effects Effects 0.000 description 7
- 239000000243 solution Substances 0.000 description 5
- 238000005470 impregnation Methods 0.000 description 4
- 238000011835 investigation Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 2
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Inorganic materials [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 101100536354 Drosophila melanogaster tant gene Proteins 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000013375 chromatographic separation Methods 0.000 description 1
- VCJMYUPGQJHHFU-UHFFFAOYSA-N iron(III) nitrate Inorganic materials [Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VCJMYUPGQJHHFU-UHFFFAOYSA-N 0.000 description 1
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Inorganic materials [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 238000002336 sorption--desorption measurement Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
- B01J21/08—Silica
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/12—Silica and alumina
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/14—Silica and magnesia
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/745—Iron
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/10—Feedstock materials
- C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Catalysts (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Silicon Compounds (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7613414A NL7613414A (nl) | 1976-12-02 | 1976-12-02 | Behandeling van silica. |
| NL7613414 | 1976-12-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1103650A true CA1103650A (en) | 1981-06-23 |
Family
ID=19827322
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA289,418A Expired CA1103650A (en) | 1976-12-02 | 1977-10-25 | Treatment of silica |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4166047A (enExample) |
| JP (1) | JPS5370099A (enExample) |
| BE (1) | BE861036A (enExample) |
| CA (1) | CA1103650A (enExample) |
| DE (1) | DE2753392A1 (enExample) |
| FR (1) | FR2372770A1 (enExample) |
| GB (1) | GB1590024A (enExample) |
| IT (1) | IT1089337B (enExample) |
| NL (1) | NL7613414A (enExample) |
| SE (2) | SE428466B (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1177811A (en) * | 1981-04-13 | 1984-11-13 | Theo G. Spek | Process for the preparation of silica particles; silica particles with a narrow pore diameter distribution, catalysts made therefrom and use of these catalysts |
| GB2100710B (en) * | 1981-06-19 | 1985-01-03 | Coal Ind | Amorphous silica-based catalyst and process for its production |
| FR2553430B1 (fr) * | 1983-10-14 | 1986-02-21 | Shell Int Research | Procede pour l'hydro-isomerisation de cires de petrole |
| DE3479429D1 (en) * | 1983-10-14 | 1989-09-21 | Shell Int Research | Hydrocarbon conversion processes and modified refractory oxides which can be used in such processes |
| FR2553302B1 (fr) * | 1983-10-14 | 1986-04-18 | Shell Int Research | Procede pour la preparation d'oxydes refractaires modifies et leur utilisation dans des procedes d'hydroconversion |
| DE4020406A1 (de) * | 1990-06-27 | 1992-01-02 | Kali Chemie Ag | Anorganischer traeger auf basis von siliciumdioxid und traegergebundene enzyme |
| US6180559B1 (en) | 1999-03-02 | 2001-01-30 | Eastman Chemical Company | Supported catalysts and catalyst support materials and process for the manufacture of 1,2-epoxybutane |
| RU2152903C1 (ru) * | 1999-09-17 | 2000-07-20 | Исангулов Кашфиль Исмагилович | Способ получения модифицированного дисперсного кремнезема |
| CN103906708B (zh) | 2011-10-28 | 2015-09-23 | 旭硝子硅素技术株式会社 | 二氧化硅球状体及亲和载体 |
| US9222230B2 (en) * | 2012-09-14 | 2015-12-29 | Potters Industries, Llc | Porous silicon oxide drying agents for waterborne latex paint compositions |
| WO2014061723A1 (ja) * | 2012-10-17 | 2014-04-24 | 株式会社島津製作所 | 分離媒体、その分離媒体を用いたカラム、そのカラムを備えた液体クロマトグラフ、及びその分離媒体の製造方法 |
| CN109833857B (zh) * | 2017-11-28 | 2022-01-04 | 中国石油天然气股份有限公司 | 一种烯烃催化用载体硅胶的制备方法 |
| CN109833861B (zh) * | 2017-11-28 | 2022-01-04 | 中国石油天然气股份有限公司 | 硅胶载体的改性制备方法 |
| CN109833860B (zh) * | 2017-11-28 | 2022-01-04 | 中国石油天然气股份有限公司 | 一种硅胶载体的制备方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB745890A (en) | 1951-10-09 | 1956-03-07 | Columbia Southern Chem Corp | Improvements in or relating to a method and process for preparing and treating finely divided pigmentary silica |
| DE1150955B (de) | 1961-04-20 | 1963-07-04 | Degussa | Verfahren und Vorrichtung zum Reinigen von hochdispersen Oxyden |
| US3404097A (en) * | 1965-08-16 | 1968-10-01 | Grace W R & Co | Method for preparing silica-magnesiafluoride catalyst |
| FR1573174A (enExample) * | 1968-04-10 | 1969-07-04 | ||
| DE1940412A1 (de) * | 1969-08-08 | 1971-04-29 | Degussa | Verfahren zur Herstellung feinteiliger,durch Metalloxid modifizierter Kieselsaeuren |
| US3996162A (en) * | 1970-02-27 | 1976-12-07 | Nuclear Medical Laboratories, Inc. | Analytical sorbent and method of use |
| FR2093176A5 (enExample) * | 1970-06-04 | 1972-01-28 | Pechiney Saint Gobain | |
| FR2125748A5 (enExample) * | 1971-02-19 | 1972-09-29 | Pechiney Saint Gobain | |
| US3843341A (en) * | 1972-03-02 | 1974-10-22 | Ppg Industries Inc | Method of making thermally stable and crush resistant microporous glass catalyst supports |
| GB1415668A (en) * | 1972-04-24 | 1975-11-26 | Ici Ltd | Catalyst treatment |
| US3892580A (en) | 1973-03-26 | 1975-07-01 | Corning Glass Works | Method of making porous inorganic bodies |
| US3969274A (en) * | 1974-03-14 | 1976-07-13 | National Distillers And Chemical Corporation | Fixed bed catalyst |
| GB1509003A (en) * | 1974-11-25 | 1978-04-26 | British Petroleum Co | Desulphurisation catalysts |
-
1976
- 1976-12-02 NL NL7613414A patent/NL7613414A/xx not_active Application Discontinuation
-
1977
- 1977-10-25 CA CA289,418A patent/CA1103650A/en not_active Expired
- 1977-11-14 US US05/850,984 patent/US4166047A/en not_active Expired - Lifetime
- 1977-11-22 BE BE1008531A patent/BE861036A/xx not_active IP Right Cessation
- 1977-11-29 IT IT30204/77A patent/IT1089337B/it active
- 1977-11-30 GB GB49872/77A patent/GB1590024A/en not_active Expired
- 1977-11-30 FR FR7736108A patent/FR2372770A1/fr active Granted
- 1977-11-30 SE SE7713591A patent/SE428466B/sv not_active IP Right Cessation
- 1977-11-30 JP JP14287177A patent/JPS5370099A/ja active Granted
- 1977-11-30 DE DE19772753392 patent/DE2753392A1/de active Granted
- 1977-11-30 SE SE7713591D patent/SE7713591L/xx not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| SE7713591L (sv) | 1978-06-03 |
| DE2753392C2 (enExample) | 1989-03-30 |
| FR2372770B1 (enExample) | 1980-01-18 |
| BE861036A (nl) | 1978-05-22 |
| NL7613414A (nl) | 1978-06-06 |
| IT1089337B (it) | 1985-06-18 |
| US4166047A (en) | 1979-08-28 |
| JPS6120487B2 (enExample) | 1986-05-22 |
| GB1590024A (en) | 1981-05-28 |
| SE428466B (sv) | 1983-07-04 |
| FR2372770A1 (fr) | 1978-06-30 |
| DE2753392A1 (de) | 1978-06-08 |
| JPS5370099A (en) | 1978-06-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |