CA1081881A - Process and device for the preparation of polymer dispersions having a low monomer content - Google Patents

Process and device for the preparation of polymer dispersions having a low monomer content

Info

Publication number
CA1081881A
CA1081881A CA257,161A CA257161A CA1081881A CA 1081881 A CA1081881 A CA 1081881A CA 257161 A CA257161 A CA 257161A CA 1081881 A CA1081881 A CA 1081881A
Authority
CA
Canada
Prior art keywords
vessel
dispersion
sprayed
gas
vessels
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA257,161A
Other languages
English (en)
French (fr)
Inventor
Franz Botsch
Christoph Heinze
Horst Wolff
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Application granted granted Critical
Publication of CA1081881A publication Critical patent/CA1081881A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/14Treatment of polymer emulsions
    • C08F6/16Purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/16Evaporating by spraying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06Flash distillation
    • B01D3/065Multiple-effect flash distillation (more than two traps)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/08Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38Steam distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/02Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1862Stationary reactors having moving elements inside placed in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1868Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Polymerisation Methods In General (AREA)
CA257,161A 1975-07-18 1976-07-16 Process and device for the preparation of polymer dispersions having a low monomer content Expired CA1081881A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DEP2532173.7 1975-07-18
DE19752532173 DE2532173C2 (de) 1975-07-18 1975-07-18 Verfahren und Vorrichtung zur kontinuierlichen Entfernung von Restgehalten an Monomeren aus wäßrigen Dispersionen von Polymerisaten des Vinylchlorids

Publications (1)

Publication Number Publication Date
CA1081881A true CA1081881A (en) 1980-07-15

Family

ID=5951848

Family Applications (1)

Application Number Title Priority Date Filing Date
CA257,161A Expired CA1081881A (en) 1975-07-18 1976-07-16 Process and device for the preparation of polymer dispersions having a low monomer content

Country Status (13)

Country Link
JP (1) JPS5213588A (de)
AR (1) AR207421A1 (de)
AT (1) AT347125B (de)
BE (1) BE844288R (de)
BR (1) BR7604673A (de)
CA (1) CA1081881A (de)
CH (1) CH629508A5 (de)
DD (1) DD125909A5 (de)
DE (1) DE2532173C2 (de)
ES (1) ES449785A2 (de)
GB (1) GB1509127A (de)
IT (1) IT1064769B (de)
SE (1) SE418296B (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2166446B (en) * 1984-11-02 1989-07-05 Malaysia The Board Of The Rubb Method and apparatus for the coagulation of natural rubber latex
CN113209654B (zh) * 2021-04-22 2022-02-11 燕山大学 无填料无孔板喷雾精馏床
CN115445548A (zh) * 2022-08-25 2022-12-09 浙江亿普新材料科技有限公司 外循环法生产碳酸亚乙烯酯的设备及方法

Also Published As

Publication number Publication date
GB1509127A (en) 1978-04-26
DE2532173A1 (de) 1977-01-27
CH629508A5 (en) 1982-04-30
SE7608156L (sv) 1977-01-19
SE418296B (sv) 1981-05-18
DE2532173C2 (de) 1981-10-01
ATA525876A (de) 1978-04-15
IT1064769B (it) 1985-02-25
JPS5213588A (en) 1977-02-01
BE844288R (fr) 1977-01-19
AT347125B (de) 1978-12-11
ES449785A2 (es) 1978-07-16
DD125909A5 (de) 1977-06-01
BR7604673A (pt) 1977-08-02
AR207421A1 (es) 1976-09-30

Similar Documents

Publication Publication Date Title
US4158092A (en) Process for the manufacture of vinyl chloride polymer dispersions with a low monomer content
CA1094748A (en) Process and apparatus for the continuous production of vinyl chloride polymers in aqueous emulsion
CA1081880A (en) Process and device for the manufacture of polymer dispersions with low monomer content
US4301275A (en) Process and device for continuously treating with gases aqueous dispersions of polyvinyl chloride
KR100359391B1 (ko) 잔류단량체의제거방법및제거용탑
CA1089146A (en) Monomer removal from the slurry of vinyl chloride resin with steam by using improved plate tower
US3930931A (en) Apparatus and method for stripping styrene from an aqueous dispersion of styrene-butadiene polymer latex
US4077135A (en) Apparatus for the manufacture of vinyl chloride polymers
US3189080A (en) Circulating solids dispersed in a liquid
CA1081881A (en) Process and device for the preparation of polymer dispersions having a low monomer content
US4032497A (en) Method and apparatus for removal of unreacted monomer from synthesized high polymer latex
US4732784A (en) Process for treating a polymerization reactor
JPH10182728A (ja) 残留モノマー除去方法および装置
CA1152689A (en) Process for removing monomer from vinyl chloride resin slurry by steam treatment and apparatus employed therefor
US4056667A (en) Process permitting a polymerization batch to be additionally cooled
US2389958A (en) Recovery of polymeric materials
DE2141770A1 (de) Verfahren und vorrichtung zur herstellung von polymerisaten oder copolymerisaten von vinylchlorid durch kontinuierliche polymerisation in masse
US7153929B2 (en) Copolymers, devoid of rubber, with low residual monomer content and a method and device for producing the same
US4184924A (en) Apparatus for steam stripping polyvinyl chloride resins
CA1211891A (en) Process for the separation treatment of polymer from polymer solution
US3980628A (en) Large capacity external cooled vinyl halide polymerization reactor
US4283526A (en) Method of treating polymerlatices
US4128516A (en) Process for the gentle degasification of coagulation-sensitive PVC latices
US4315843A (en) Thin film monomer removal from polyvinyl chloride latexes
US3464967A (en) Circulating solids dispersed in a liquid

Legal Events

Date Code Title Description
MKEX Expiry