GB1509127A - Process and device for the preparation of polymer dispersions having a low monomer content - Google Patents

Process and device for the preparation of polymer dispersions having a low monomer content

Info

Publication number
GB1509127A
GB1509127A GB2974276A GB2974276A GB1509127A GB 1509127 A GB1509127 A GB 1509127A GB 2974276 A GB2974276 A GB 2974276A GB 2974276 A GB2974276 A GB 2974276A GB 1509127 A GB1509127 A GB 1509127A
Authority
GB
United Kingdom
Prior art keywords
container
dispersion
polymer dispersions
substances
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2974276A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of GB1509127A publication Critical patent/GB1509127A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/14—Treatment of polymer emulsions
    • C08F6/16—Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06—Flash distillation
    • B01D3/065—Multiple-effect flash distillation (more than two traps)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/08—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/02—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Polymerisation Methods In General (AREA)

Abstract

Polymer dispersions are prepared by emulsion or suspension polymerisation with opening of C-C double bonds of at least one monomer in aqueous liquor, decompression of the polymer batch and discharge and condensation of the gaseous products. In at least two vertical, rotationally symmetrical containers connected in series, the dispersion is sprayed radially, in the form of a hollow cone or disc, against the container wall; the droplets have a maximum diameter of 6 mm. They are deposited on the container wall and collected in the lower part of the container. The gaseous substances are drawn out of the spray device above the dispersion exit. The gaseous substances are passed from container to container in only one direction and the dispersion in the opposite direction. This process allows physiologically unacceptable substances to be removed directly after the polymerisation, using comparatively low apparatus volumes. <IMAGE>
GB2974276A 1975-07-18 1976-07-16 Process and device for the preparation of polymer dispersions having a low monomer content Expired GB1509127A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19752532173 DE2532173C2 (en) 1975-07-18 1975-07-18 Process and device for the continuous removal of residual amounts of monomers from aqueous dispersions of polymers of vinyl chloride

Publications (1)

Publication Number Publication Date
GB1509127A true GB1509127A (en) 1978-04-26

Family

ID=5951848

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2974276A Expired GB1509127A (en) 1975-07-18 1976-07-16 Process and device for the preparation of polymer dispersions having a low monomer content

Country Status (13)

Country Link
JP (1) JPS5213588A (en)
AR (1) AR207421A1 (en)
AT (1) AT347125B (en)
BE (1) BE844288R (en)
BR (1) BR7604673A (en)
CA (1) CA1081881A (en)
CH (1) CH629508A5 (en)
DD (1) DD125909A5 (en)
DE (1) DE2532173C2 (en)
ES (1) ES449785A2 (en)
GB (1) GB1509127A (en)
IT (1) IT1064769B (en)
SE (1) SE418296B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2166446B (en) * 1984-11-02 1989-07-05 Malaysia The Board Of The Rubb Method and apparatus for the coagulation of natural rubber latex
CN113209654A (en) * 2021-04-22 2021-08-06 燕山大学 Packless pore-plate-free spray rectification bed

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115445548A (en) * 2022-08-25 2022-12-09 浙江亿普新材料科技有限公司 Equipment and method for producing vinylene carbonate by external circulation method

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2166446B (en) * 1984-11-02 1989-07-05 Malaysia The Board Of The Rubb Method and apparatus for the coagulation of natural rubber latex
CN113209654A (en) * 2021-04-22 2021-08-06 燕山大学 Packless pore-plate-free spray rectification bed
CN113209654B (en) * 2021-04-22 2022-02-11 燕山大学 Packless pore-plate-free spray rectification bed

Also Published As

Publication number Publication date
DE2532173A1 (en) 1977-01-27
CH629508A5 (en) 1982-04-30
SE7608156L (en) 1977-01-19
SE418296B (en) 1981-05-18
DE2532173C2 (en) 1981-10-01
ATA525876A (en) 1978-04-15
IT1064769B (en) 1985-02-25
JPS5213588A (en) 1977-02-01
BE844288R (en) 1977-01-19
AT347125B (en) 1978-12-11
CA1081881A (en) 1980-07-15
ES449785A2 (en) 1978-07-16
DD125909A5 (en) 1977-06-01
BR7604673A (en) 1977-08-02
AR207421A1 (en) 1976-09-30

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Legal Events

Date Code Title Description
PS Patent sealed