BRPI0610906A2 - processo para preparar misturas, e, mistura de poliisocianato - Google Patents
processo para preparar misturas, e, mistura de poliisocianatoInfo
- Publication number
- BRPI0610906A2 BRPI0610906A2 BRPI0610906-3A BRPI0610906A BRPI0610906A2 BR PI0610906 A2 BRPI0610906 A2 BR PI0610906A2 BR PI0610906 A BRPI0610906 A BR PI0610906A BR PI0610906 A2 BRPI0610906 A2 BR PI0610906A2
- Authority
- BR
- Brazil
- Prior art keywords
- chlorides
- polyisocyanates
- amine
- mixtures
- polyphenyl polymethylene
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title abstract 6
- 229920001228 polyisocyanate Polymers 0.000 title abstract 5
- 239000005056 polyisocyanate Substances 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- -1 polymethylene Polymers 0.000 abstract 5
- CKDWPUIZGOQOOM-UHFFFAOYSA-N Carbamyl chloride Chemical class NC(Cl)=O CKDWPUIZGOQOOM-UHFFFAOYSA-N 0.000 abstract 2
- 229920006389 polyphenyl polymer Polymers 0.000 abstract 2
- KLPSGEJVKSFEHK-UHFFFAOYSA-N C(=O)(Cl)Cl.NC(C1=CC=CC=C1)(C1=CC=CC=C1)N Chemical class C(=O)(Cl)Cl.NC(C1=CC=CC=C1)(C1=CC=CC=C1)N KLPSGEJVKSFEHK-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 1
- HIFVAOIJYDXIJG-UHFFFAOYSA-N benzylbenzene;isocyanic acid Chemical class N=C=O.N=C=O.C=1C=CC=CC=1CC1=CC=CC=C1 HIFVAOIJYDXIJG-UHFFFAOYSA-N 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 229920000768 polyamine Polymers 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
- C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/82—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCESSO PARA PREPARAR MISTURAS, E, MISTURA DE POLIISOCIANATO. Processo para preparar misturas compreendendo diisocianatosde difenilmetano e poliisocianatos de polifenilpolimetileno tendo um número de cor HunterLab superior (L) por reação estagiada das misturas correspondentes de difenilmetanodiaminas e polifenilpolimetilenopoliaminas com fosgénio, na presença de pelo menos um solvente, por meio do que em um primeiro estágio os correspondentes cloretos de carbamoila e cloridretos de amina são formados e, por meio do que, em um estágio subseqúente os cloretos de carbamoila residuais são dissociados nos correspondentes poliisocianatos e cloreto de hidrogênio, e os cloridretos de amina são fosgenados para formar finalmente os poliisocianatos correspondentes, em que alguns cloridretos de amina permanecem não reagidos ao ponto em que o excesso residual de fosgênio é removido da mistura de reação.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP05104608 | 2005-05-30 | ||
PCT/US2006/020065 WO2006130405A2 (en) | 2005-05-30 | 2006-05-23 | Process for the preparation of polyisocyanates of the diphenylmethane series |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI0610906A2 true BRPI0610906A2 (pt) | 2008-12-02 |
BRPI0610906B1 BRPI0610906B1 (pt) | 2016-03-29 |
Family
ID=34981325
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0610906A BRPI0610906B1 (pt) | 2005-05-30 | 2006-05-23 | processo para preparar misturas compreendendo diisocianatos de difenilmetano e poliisocianatos de polifenilpolimetileno |
Country Status (12)
Country | Link |
---|---|
EP (1) | EP1890998B1 (pt) |
JP (1) | JP4938007B2 (pt) |
KR (1) | KR101232431B1 (pt) |
CN (1) | CN101184727B (pt) |
AU (1) | AU2006252770B2 (pt) |
BR (1) | BRPI0610906B1 (pt) |
CA (1) | CA2606107C (pt) |
ES (1) | ES2453145T3 (pt) |
MX (1) | MX2007014890A (pt) |
PT (1) | PT1890998E (pt) |
RU (1) | RU2415129C2 (pt) |
WO (1) | WO2006130405A2 (pt) |
Families Citing this family (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2042485A1 (en) * | 2007-09-28 | 2009-04-01 | Huntsman International Llc | Process for fractionating a mixture of polyisocyanates |
EP2060560B1 (en) * | 2007-11-14 | 2016-04-13 | Covestro Deutschland AG | Preparation of light-colored isocyanates |
JP5380931B2 (ja) * | 2008-07-14 | 2014-01-08 | 日本ポリウレタン工業株式会社 | メチレン架橋ポリフェニルポリイソシアネートの製造方法 |
EP2370400B2 (en) | 2008-11-26 | 2019-10-16 | Huntsman International LLC | Process for manufacturing isocyanates |
EP2373616B1 (de) * | 2008-12-03 | 2014-10-22 | Basf Se | Verfahren zur herstellung von isocyanaten |
FR2940283B1 (fr) * | 2008-12-18 | 2011-03-11 | Perstorp Tolonates France | Utilisation d'un reacteur de type piston pour la mise en oeuvre d'un procede de phosgenation. |
PT2507206E (pt) | 2009-12-04 | 2014-12-26 | Basf Se | Método para a produção de isocianatos |
EP2640694B1 (de) | 2010-11-17 | 2019-01-09 | Basf Se | Verfahren zur herstellung von methylendiphenyldiisocyanat |
US8907124B2 (en) | 2010-11-17 | 2014-12-09 | Basf Se | Process for preparing methylenedi(phenyl isocyanate) |
US8933262B2 (en) | 2011-05-24 | 2015-01-13 | Basf Se | Process for preparing polyisocyanates from biomass |
EP2714650A1 (de) | 2011-05-24 | 2014-04-09 | Basf Se | Verfahren zur herstellung von polyisocyanaten aus biomasse |
EP2907562A1 (en) * | 2014-02-12 | 2015-08-19 | Huntsman International LLC | A process for extracting phosgene |
KR101854429B1 (ko) * | 2016-12-29 | 2018-05-03 | 한화케미칼 주식회사 | 지방족 이소시아네이트의 제조 방법 |
JP6940694B2 (ja) * | 2017-09-11 | 2021-09-29 | ハンワ ソリューションズ コーポレイションHanwha Solutions Corporation | 脂肪族イソシアネートの製造方法 |
CN113831262B (zh) * | 2020-06-24 | 2023-01-17 | 万华化学集团股份有限公司 | 一种连续光气化法制备异氰酸酯的方法 |
CN111961185B (zh) * | 2020-08-27 | 2022-07-12 | 万华化学集团股份有限公司 | 一种多亚甲基多苯基多异氰酸酯组合物及其制备方法 |
PT4208441T (pt) * | 2020-09-01 | 2024-07-29 | Basf Se | Processo para produção de isocianatos |
WO2022047681A1 (zh) * | 2020-09-03 | 2022-03-10 | 万华化学集团股份有限公司 | 制备mdi的方法和光气制备方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4465639A (en) * | 1983-01-26 | 1984-08-14 | The Upjohn Company | Process for polyisocyanates |
DE4232769A1 (de) * | 1992-09-30 | 1994-03-31 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmethandiisocyanaten und Polyphenyl-polymethylen-polyisocyanaten mit einer verminderten Iodfarbzahl |
DE19523851A1 (de) * | 1995-06-30 | 1997-01-02 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmethan-diisocyanaten und Polyphenyl-polymethylen-polyisocyanaten mit einer verminderten Iodfarbzahl und einem reduzierten Chlorgehalt |
DE19804915A1 (de) * | 1998-02-07 | 1999-08-12 | Basf Ag | Verfahren zur Herstellung von Methylendi(phenylamin) und Methylendi(phenylisocyanat) |
DE19817691A1 (de) * | 1998-04-21 | 1999-10-28 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl |
DE19928741A1 (de) * | 1999-06-23 | 2000-12-28 | Basf Ag | Helle Isocyanate, Verfahren zu deren Herstellung und deren Verwendung |
JP4110377B2 (ja) * | 2002-07-16 | 2008-07-02 | 日本ポリウレタン工業株式会社 | ポリメチレンポリフェニルポリイソシアネートの製造方法 |
DE10245584A1 (de) * | 2002-09-27 | 2004-04-08 | Basf Ag | Aufarbeitung von Reaktionsausträgen aus Phosgenierreaktoren |
DE10260082A1 (de) * | 2002-12-19 | 2004-07-01 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von Isocyanaten |
-
2006
- 2006-05-23 EP EP06771056.6A patent/EP1890998B1/en active Active
- 2006-05-23 KR KR1020077027796A patent/KR101232431B1/ko active IP Right Grant
- 2006-05-23 RU RU2007144511/04A patent/RU2415129C2/ru active
- 2006-05-23 BR BRPI0610906A patent/BRPI0610906B1/pt not_active IP Right Cessation
- 2006-05-23 WO PCT/US2006/020065 patent/WO2006130405A2/en active Application Filing
- 2006-05-23 ES ES06771056.6T patent/ES2453145T3/es active Active
- 2006-05-23 PT PT67710566T patent/PT1890998E/pt unknown
- 2006-05-23 CN CN2006800189252A patent/CN101184727B/zh active Active
- 2006-05-23 JP JP2008514695A patent/JP4938007B2/ja active Active
- 2006-05-23 MX MX2007014890A patent/MX2007014890A/es active IP Right Grant
- 2006-05-23 AU AU2006252770A patent/AU2006252770B2/en active Active
- 2006-05-23 CA CA2606107A patent/CA2606107C/en active Active
Also Published As
Publication number | Publication date |
---|---|
EP1890998A4 (en) | 2011-09-07 |
JP4938007B2 (ja) | 2012-05-23 |
BRPI0610906B1 (pt) | 2016-03-29 |
WO2006130405A2 (en) | 2006-12-07 |
EP1890998B1 (en) | 2014-02-26 |
PT1890998E (pt) | 2014-03-06 |
CA2606107A1 (en) | 2006-12-07 |
CN101184727A (zh) | 2008-05-21 |
RU2007144511A (ru) | 2009-06-10 |
ES2453145T3 (es) | 2014-04-04 |
AU2006252770A1 (en) | 2006-12-07 |
JP2008545745A (ja) | 2008-12-18 |
RU2415129C2 (ru) | 2011-03-27 |
AU2006252770B2 (en) | 2011-02-03 |
MX2007014890A (es) | 2008-01-28 |
KR20080021621A (ko) | 2008-03-07 |
WO2006130405A3 (en) | 2007-02-15 |
EP1890998A2 (en) | 2008-02-27 |
KR101232431B1 (ko) | 2013-02-12 |
CN101184727B (zh) | 2012-01-11 |
CA2606107C (en) | 2013-12-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 23/05/2006, OBSERVADAS AS CONDICOES LEGAIS. |
|
B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 18A ANUIDADE. |
|
B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2776 DE 19-03-2024 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |