BRPI0508304A - processo para o processamento do ácido beta-sulfatoetilsulfonilanilina-2-sulfÈnico partindo de uma solução em ácido sulfúrico aquoso - Google Patents
processo para o processamento do ácido beta-sulfatoetilsulfonilanilina-2-sulfÈnico partindo de uma solução em ácido sulfúrico aquosoInfo
- Publication number
- BRPI0508304A BRPI0508304A BRPI0508304-4A BRPI0508304A BRPI0508304A BR PI0508304 A BRPI0508304 A BR PI0508304A BR PI0508304 A BRPI0508304 A BR PI0508304A BR PI0508304 A BRPI0508304 A BR PI0508304A
- Authority
- BR
- Brazil
- Prior art keywords
- solution
- sulfatoethylsulfonylaniline
- sulfuric acid
- sulfonic acid
- aqueous sulfuric
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
- C07C315/06—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C317/00—Sulfones; Sulfoxides
- C07C317/26—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
- C07C317/32—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton with sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
- C07C317/34—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton with sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having sulfone or sulfoxide groups and amino groups bound to carbon atoms of six-membered aromatic rings being part of the same non-condensed ring or of a condensed ring system containing that ring
- C07C317/36—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton with sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having sulfone or sulfoxide groups and amino groups bound to carbon atoms of six-membered aromatic rings being part of the same non-condensed ring or of a condensed ring system containing that ring with the nitrogen atoms of the amino groups bound to hydrogen atoms or to carbon atoms
Abstract
PROCESSO PARA O PROCESSAMENTO DO áCIDO BETASULFATOETILSULFONILANILINA-2-SULFÈNICO PARTINDO DE UMA SOLUçãO EM áCIDO SULFúRICO AQUOSO. Método para o processamento do ácido <225>-sulfatoetilsulfonilanilina-2-sulfónico partindo de uma solução em ácido sulfúrico aquoso, que compreende uma primeira etapa do ácido <225>-sulfatoetilsulfonilanilina-2-sulfónico sendo precipitado através da adição de sais de metais alcalinos ou alcalinos terrosos e/ou de amónio, separado e dissolvido ou o ácido sulfúrico sendo precipitado através da adição de sais de cálcio e o sulfato de cálcio resultante sendo separado, se apropriado e uma segunda etapa da solução resultante sendo ajustada em um pH entre 1 e 5 através da adição de hidróxido, carbonato, bicarbonato e/ou acetato de metais alcalinos ou alcalinos terrosos ou de armónio, qualquer sulfato de cálcio ainda presente sendo separado e o ácido <225>-sulfatoetilsulfonilanilina-2-sulfónico sendo isolado da solução.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102004010950A DE102004010950A1 (de) | 2004-03-03 | 2004-03-03 | Verfahren zur Aufarbeitung von ß-Sulfatoethylsulfonylanilin-2-sulfonsäure |
DE102004010950.8 | 2004-03-03 | ||
PCT/EP2005/002054 WO2005085190A1 (de) | 2004-03-03 | 2005-02-26 | VERFAHREN ZUR AUFARBEITUNG VON ß-SULFATOETHYLSULFONYLANILIN-2-SULFONSÄURE |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI0508304A true BRPI0508304A (pt) | 2007-07-17 |
BRPI0508304B1 BRPI0508304B1 (pt) | 2014-12-09 |
Family
ID=34877463
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0508304-4A BRPI0508304B1 (pt) | 2004-03-03 | 2005-02-26 | “processo para o processamento do ácido 4- betasulfatoetilsulfonilanilina-2-sulfônico partindo de uma solução em ácido sulfúrico aquoso” |
Country Status (10)
Country | Link |
---|---|
US (1) | US7371892B2 (pt) |
EP (1) | EP1723103B1 (pt) |
KR (1) | KR101161458B1 (pt) |
CN (1) | CN100484917C (pt) |
AR (1) | AR047824A1 (pt) |
BR (1) | BRPI0508304B1 (pt) |
DE (1) | DE102004010950A1 (pt) |
ES (1) | ES2534751T3 (pt) |
TW (1) | TWI325418B (pt) |
WO (1) | WO2005085190A1 (pt) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101633631B (zh) * | 2009-08-17 | 2012-10-03 | 浙江劲光化工有限公司 | 一种磺化对位酯的合成方法 |
CN102311372A (zh) * | 2011-07-04 | 2012-01-11 | 天津德凯化工股份有限公司 | 一种4-β-乙基砜基硫酸酯苯胺-2-磺酸的制备方法 |
CN102391163A (zh) * | 2011-07-04 | 2012-03-28 | 天津德凯化工股份有限公司 | 一种染料中间体磺化对位酯的制备方法 |
DE102011112716A1 (de) | 2011-09-07 | 2013-03-07 | Audi Ag | Verfahren zum Betreiben eines Scheinwerfers eines Kraftfahrzeugs |
CN105130858B (zh) * | 2015-08-25 | 2018-07-06 | 江苏远征化工有限公司 | 一种染料中间体磺化对位酯的清洁生产工艺 |
CN110066230A (zh) * | 2018-08-30 | 2019-07-30 | 内蒙古利元科技有限公司 | 一种新型磺化对位酯生产系统和工艺 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2154943C2 (de) * | 1971-11-05 | 1983-12-08 | Hoechst Ag, 6230 Frankfurt | 1-Aminobenzol-4-(β-sulfatoxyäthylsulfon)-2-sulfonsäure, die entsprechende 4-Vinylsulfon-Verbindung, Verfahren zur Herstellung dieser Verbindungen und ihre Verwendung als Diazokomponente |
DE2538722C2 (de) * | 1975-08-30 | 1984-10-11 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Herstellung von 1-Aminobenzol-5-β-sulfatoäthylsulfon-2-sulfonsäure und 1-Aminobenzol-5-vinylsulfon-2-sulfonsäure und deren Alkali- und Erdalkalisalzen |
DE2538723C2 (de) * | 1975-08-30 | 1982-12-23 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von 1-Aminobenzol-4- und -5-β-sulfatoäthylsulfon-2-sulfonsäure und der entsprechenden Hydroxyäthylsulfon-und Vinylsulfonverbindungen |
CN1090655C (zh) * | 1994-07-16 | 2002-09-11 | 克莱里安特财务(Bvi)有限公司 | 染料 |
DE19521620A1 (de) * | 1995-06-14 | 1996-12-19 | Bayer Ag | Aufarbeitungsverfahren für ß-Sulfatoethyl-anilin-sulfonsäuren |
-
2004
- 2004-03-03 DE DE102004010950A patent/DE102004010950A1/de not_active Withdrawn
-
2005
- 2005-02-26 WO PCT/EP2005/002054 patent/WO2005085190A1/de active Application Filing
- 2005-02-26 ES ES05733648.9T patent/ES2534751T3/es active Active
- 2005-02-26 BR BRPI0508304-4A patent/BRPI0508304B1/pt active IP Right Grant
- 2005-02-26 US US10/589,972 patent/US7371892B2/en active Active
- 2005-02-26 KR KR1020067020722A patent/KR101161458B1/ko not_active IP Right Cessation
- 2005-02-26 CN CNB2005800066582A patent/CN100484917C/zh active Active
- 2005-02-26 EP EP05733648.9A patent/EP1723103B1/de active Active
- 2005-03-01 AR ARP050100761A patent/AR047824A1/es active IP Right Grant
- 2005-03-03 TW TW094106378A patent/TWI325418B/zh active
Also Published As
Publication number | Publication date |
---|---|
KR101161458B1 (ko) | 2012-07-02 |
KR20060129524A (ko) | 2006-12-15 |
ES2534751T3 (es) | 2015-04-27 |
WO2005085190A1 (de) | 2005-09-15 |
US7371892B2 (en) | 2008-05-13 |
CN1926100A (zh) | 2007-03-07 |
TWI325418B (en) | 2010-06-01 |
EP1723103B1 (de) | 2015-01-14 |
EP1723103A1 (de) | 2006-11-22 |
CN100484917C (zh) | 2009-05-06 |
DE102004010950A1 (de) | 2005-09-22 |
US20070173661A1 (en) | 2007-07-26 |
TW200533639A (en) | 2005-10-16 |
AR047824A1 (es) | 2006-02-22 |
BRPI0508304B1 (pt) | 2014-12-09 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 26/02/2005, OBSERVADAS AS CONDICOES LEGAIS. |
|
B25D | Requested change of name of applicant approved | ||
B25A | Requested transfer of rights approved |