BR9900414A - Processo para tratamento de acetonitrila bruta contendo acrilonitrila como uma impureza e processo para a fabricação de acetonitrila grau hplc. - Google Patents

Processo para tratamento de acetonitrila bruta contendo acrilonitrila como uma impureza e processo para a fabricação de acetonitrila grau hplc.

Info

Publication number
BR9900414A
BR9900414A BR9900414-3A BR9900414A BR9900414A BR 9900414 A BR9900414 A BR 9900414A BR 9900414 A BR9900414 A BR 9900414A BR 9900414 A BR9900414 A BR 9900414A
Authority
BR
Brazil
Prior art keywords
impurity
acetonitrile
acrylonitrile
manufacture
hplc grade
Prior art date
Application number
BR9900414-3A
Other languages
English (en)
Other versions
BRPI9900414B1 (pt
Inventor
Sanjay Purushottam Godbole
Paul Alan Jacobson
Richard Lee Wappelhorst
Original Assignee
Standar Oil Company
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Standar Oil Company filed Critical Standar Oil Company
Publication of BR9900414A publication Critical patent/BR9900414A/pt
Publication of BRPI9900414B1 publication Critical patent/BRPI9900414B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/02—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms of an acyclic and saturated carbon skeleton
    • C07C255/03—Mononitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

"PROCESSO PARA TRATAMENTO DE ACETONITRILA BRUTA CONTENDO ACRILONITRILA COMO UMA IMPUREZA E PROCESSO PARA A FABRICAçãO DE ACETONITRILA GRAU HPLC". O método da presente invenção compreende alimentar acetonitrila bruta contendo acrilonitrila como uma impureza e água para dentro da porção superior de uma coluna de destilação, destilar a acetonitrila bruta na presença da água por um tempo suficiente para permitir substancialmente toda a impureza de acrilonitrila ser vaporizada na presença da água, remover substancialmente toda a acrilonitrila em uma corrente superior saindo da coluna de destilação e recuperar a acetonitrila bruta substancialmente livre de impureza de acrilonitrila da porção inferior da coluna de destilação. Em particular, o método pode ser utilizado para produzir acetonitrila grau HPLC (supressão de UV < 190).
BRPI9900414-3A 1998-02-23 1999-02-12 Processo para a fabricação de acetonitrila grau hplc. BRPI9900414B1 (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US2786498A 1998-02-23 1998-02-23

Publications (2)

Publication Number Publication Date
BR9900414A true BR9900414A (pt) 2000-05-02
BRPI9900414B1 BRPI9900414B1 (pt) 2015-03-31

Family

ID=21840206

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI9900414-3A BRPI9900414B1 (pt) 1998-02-23 1999-02-12 Processo para a fabricação de acetonitrila grau hplc.

Country Status (14)

Country Link
US (1) US6326508B1 (pt)
EP (1) EP0937707B1 (pt)
JP (2) JP4974313B2 (pt)
KR (1) KR100587189B1 (pt)
CN (1) CN1131205C (pt)
BG (1) BG64552B1 (pt)
BR (1) BRPI9900414B1 (pt)
DE (1) DE69906848T2 (pt)
ES (1) ES2197578T3 (pt)
RO (1) RO122146B1 (pt)
RU (1) RU2230733C2 (pt)
TR (1) TR199900385A2 (pt)
TW (1) TW422830B (pt)
ZA (1) ZA991401B (pt)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
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US6395142B1 (en) 1999-10-14 2002-05-28 Chemcycles, Inc. Method and apparatus for purifying low grade acetonitrile and other constituents from hazardous waste
US6706474B1 (en) * 2000-06-27 2004-03-16 Board Of Trustees Of The University Of Illinois Nucleic acid enzyme biosensors for ions
WO2002006212A2 (en) * 2000-07-18 2002-01-24 The Standard Oil Company Process for the purification and recovery of acetonitrile
US6890719B2 (en) * 2002-05-10 2005-05-10 The Board Of Trustess Of The University Of Illinois Fluorescence based biosensor
WO2005044783A2 (en) 2003-11-04 2005-05-19 Lonza Ag Acetonitrile recycling process
US7892734B2 (en) * 2005-08-11 2011-02-22 The Board Of Trustees Of The University Of Illinois Aptamer based colorimetric sensor systems
WO2007109500A1 (en) * 2006-03-16 2007-09-27 The Board Of Trustees Of The University Of Illinois Lateral flow devices
WO2008089248A2 (en) * 2007-01-19 2008-07-24 The Board Of Trustees Of The University Of Illinois Amphiphilic substances and triggered liberation from lipid vesicles
US8058415B2 (en) * 2007-04-24 2011-11-15 The Board Of Trustees Of The University Of Illinois Aptamer- and nucleic acid enzyme-based systems for simultaneous detection of multiple analytes
WO2009012309A2 (en) * 2007-07-16 2009-01-22 The Board Of Trustees Of The University Of Illinois Nucleic acid based fluorescent sensor for divalent copper ion detection
US8568690B2 (en) * 2007-07-31 2013-10-29 The Board Of Trustees Of The University Of Illinois MRI contrast agents and high-throughput screening by MRI
US8367416B2 (en) 2007-08-10 2013-02-05 The Board Of Trustees Of The University Of Illinois Nucleic acid based fluorescent sensor for mercury detection
US20090090894A1 (en) * 2007-10-05 2009-04-09 Bin Wang Separation and extraction system
US20100105039A1 (en) * 2008-06-03 2010-04-29 Yi Lu Label-free colorimetric detection
US8062893B2 (en) 2008-10-10 2011-11-22 The Board Of Trustees Of The University Of Illinois Fluorescent sensor for mercury
CN101570497B (zh) * 2009-06-15 2012-10-24 天津市康科德科技有限公司 科研用高纯有机溶剂乙腈的提纯方法
CN102666519B (zh) * 2009-12-24 2016-01-13 昭和电工株式会社 环氧化合物的制造方法
US8815156B2 (en) 2010-07-19 2014-08-26 Andalyze, Inc. Sensor housing and reagent chemistry
CN102527213B (zh) * 2011-12-15 2014-06-25 惠生工程（中国）有限公司 一种乙腈精制工艺的尾气处理方法
CN102746189B (zh) * 2012-07-24 2014-10-29 国药集团化学试剂有限公司 一种色谱纯乙腈的制备方法
US10336690B2 (en) 2014-02-24 2019-07-02 Honeywell International Inc. Methods and systems for processing an acetonitrile waste stream
CN109499085A (zh) * 2014-06-11 2019-03-22 英尼奥斯欧洲股份公司 丙烯腈回收的乙腈移除步骤中的污染减轻
CN106892843A (zh) * 2015-12-17 2017-06-27 英尼奥斯欧洲股份公司 回收塔控制
KR102142550B1 (ko) * 2016-12-16 2020-08-07 주식회사 엘지화학 미반응 단량체를 포함하는 혼합용액으로부터 미반응 단량체의 분리방법
CN109663379A (zh) * 2017-10-13 2019-04-23 抚顺伊科思新材料有限公司 一种节能乙腈法裂解碳五分离方法
CN111056975A (zh) * 2019-11-29 2020-04-24 南通醋酸化工股份有限公司 一种产品乙腈中去除丙酮的方法
WO2022051659A1 (en) 2020-09-03 2022-03-10 Ascend Performance Materials Operations Llc Process for recovering acetonitrile
MX2023002685A (es) 2020-09-04 2023-04-03 Ascend Performance Mat Operations Llc Proceso de separacion de acetonitrilo.

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3201451A (en) * 1962-03-23 1965-08-17 Standard Oil Co Purification of acetonitrile
US3936360A (en) * 1971-04-07 1976-02-03 The Standard Oil Company Process for distillation and recovery of olefinic nitriles
US4166008A (en) * 1977-07-29 1979-08-28 The Standard Oil Company Process for recovery of olefinic nitriles
US4328075A (en) * 1979-12-10 1982-05-04 Standard Oil Company Removal of cyanides from acetonitrile
KR850001603B1 (ko) * 1980-12-03 1985-10-24 아사히 가세이 고오교오 가부시기가이샤 불포화 니트릴의 제조법
US4334965A (en) * 1980-12-31 1982-06-15 Standard Oil Company Process for recovery of olefinic nitriles
US4362603A (en) * 1981-01-02 1982-12-07 The Standard Oil Company Continuous acetonitrile recovery process
DE69307701T2 (de) * 1992-05-21 1997-05-15 Cryodyne Tech Inc Verfahren zur reinigung von acetonitril
US5426208A (en) * 1992-05-21 1995-06-20 Cryodyne Technologies, Inc. Method of purification of acetonitrile
JPH08231487A (ja) * 1995-02-28 1996-09-10 Asahi Chem Ind Co Ltd アクリロニトリルの製造方法
KR100498803B1 (ko) * 1996-10-23 2005-07-01 솔루티아인코포레이티드 아크릴로니트릴의 정제방법
DE69707848T2 (de) * 1997-07-08 2002-04-04 Standard Oil The Company Chica Verfahren zur Reinigung von Acetonitril
US5840955A (en) * 1997-11-25 1998-11-24 Sockell; Edward J. Waste minimization and product recovery process

Also Published As

Publication number Publication date
EP0937707B1 (en) 2003-04-16
DE69906848D1 (de) 2003-05-22
CN1231282A (zh) 1999-10-13
DE69906848T2 (de) 2003-10-30
JP2009102388A (ja) 2009-05-14
TW422830B (en) 2001-02-21
ZA991401B (en) 1999-08-23
TR199900385A3 (tr) 1999-09-21
US6326508B1 (en) 2001-12-04
TR199900385A2 (xx) 1999-09-21
EP0937707A3 (en) 2000-07-26
ES2197578T3 (es) 2004-01-01
CN1131205C (zh) 2003-12-17
JPH11286473A (ja) 1999-10-19
BRPI9900414B1 (pt) 2015-03-31
JP4974313B2 (ja) 2012-07-11
KR100587189B1 (ko) 2006-06-08
BG103188A (en) 1999-12-30
RO122146B1 (ro) 2009-01-30
EP0937707A2 (en) 1999-08-25
KR19990072776A (ko) 1999-09-27
BG64552B1 (bg) 2005-07-29
RU2230733C2 (ru) 2004-06-20

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