BR9813349A - Processo para a purificação de ácido tereftálico bruto de uma dispersão lìquida do mesmo que também contém impurezas selecionadas entre materiais de partida não reagidos, solventes, produtos de reações secundárias e/ou outros materiais indesejados - Google Patents
Processo para a purificação de ácido tereftálico bruto de uma dispersão lìquida do mesmo que também contém impurezas selecionadas entre materiais de partida não reagidos, solventes, produtos de reações secundárias e/ou outros materiais indesejadosInfo
- Publication number
- BR9813349A BR9813349A BR9813349-7A BR9813349A BR9813349A BR 9813349 A BR9813349 A BR 9813349A BR 9813349 A BR9813349 A BR 9813349A BR 9813349 A BR9813349 A BR 9813349A
- Authority
- BR
- Brazil
- Prior art keywords
- terephthalic acid
- solvent
- materials
- solution
- solvents
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
"PROCESSO PARA A PURIFICAçãO DE áCIDO TEREFTáLICO BRUTO DE UMA DISPERSãO LìQUIDA DO MESMO QUE TAMBéM CONTéM IMPUREZAS SELECIONADAS ENTRE MATERIAIS DE PARTIDA NãO REAGIDOS, SOLVENTES, PRODUTOS DE REAçõES SECUNDáRIAS E/OU OUTROS MATERIAIS INDESEJADOS". São fornecidos um processo e uma aparelhagem para a purificação de ácido tereftálico bruto de uma dispersão líquida do mesmo que também contém impurezas selecionadas entre materiais de partida não reagidos, solventes, produtos de reações secundárias e/ou outros materiais indesejados. O processo compreende as etapas de filtração da dispersão para formar uma torta de filtro de ácido tereftálico bruto, dissolução da torta do filtro em um solvente para cristalização seletiva a uma temperatura elevada para formar uma solução, cristalização do ácido tereftálico purificado da solução no solvente de cristalização por redução da pressão e da temperatura da solução e separação do dito ácido tereftálico purificado cristalizado da solução. De acordo com a invenção, o solvente é não aquoso, não corrosivo e essencialmente não reativo com ácido tereftálico. Preferencialmente, o solvente para cristalização seletiva é N-metil pirrolidona ou N,N-dimetil acetamida. O processo e a aparelhagem produzem ácido tereftálico purificado que tem uma pureza desejada para uso na formação de resina de poliéster e outros produtos a uma velocidade economicamente atraente e a condição de operação de gravidade reduzida que requerem um menor investimento de capital e um processamento simplificado.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/962,030 US5840968A (en) | 1995-06-07 | 1997-10-31 | Method and apparatus for preparing purified terephthalic acid |
PCT/US1998/022942 WO1999023055A1 (en) | 1997-10-31 | 1998-10-29 | Method and apparatus for preparing purified terephthalic acid |
Publications (2)
Publication Number | Publication Date |
---|---|
BR9813349A true BR9813349A (pt) | 2000-08-22 |
BR9813349B1 BR9813349B1 (pt) | 2010-08-24 |
Family
ID=25505339
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI9813349-7A BR9813349B1 (pt) | 1997-10-31 | 1998-10-29 | processo para a purificaÇço de Ácido tereftÁlico bruto de uma dispersço lÍquida do mesmo que tambÉm contÉm impurezas selecionadas entre materiais de partida nço reagidos, solventes, produtos de reaÇÕes secundÁrias e/ou outros materiais indesejados. |
Country Status (17)
Country | Link |
---|---|
US (1) | US5840968A (pt) |
EP (1) | EP1030829B1 (pt) |
JP (1) | JP4381600B2 (pt) |
KR (1) | KR100603723B1 (pt) |
CN (1) | CN1127471C (pt) |
AR (1) | AR017765A1 (pt) |
AU (1) | AU1286899A (pt) |
BR (1) | BR9813349B1 (pt) |
CA (1) | CA2307783C (pt) |
DE (1) | DE69835229T2 (pt) |
ES (1) | ES2263227T3 (pt) |
ID (1) | ID21201A (pt) |
MY (1) | MY119529A (pt) |
RU (1) | RU2213725C2 (pt) |
TR (1) | TR200001138T2 (pt) |
TW (1) | TW505627B (pt) |
WO (1) | WO1999023055A1 (pt) |
Families Citing this family (70)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1082286B1 (en) * | 1998-05-29 | 2005-02-23 | GTC Technology, Inc | Method for preparing purified terephthalic acid and isophthalic acid from mixed xylenes |
US6291707B1 (en) * | 1999-03-12 | 2001-09-18 | Tsong-Dar Vincent Lin | Process of purifying and producing high purity aromatic polycarboxylic acids and derivatives thereof |
US6392091B2 (en) * | 1998-11-24 | 2002-05-21 | Tsong-Dar Vincent Lin | Process of purifying and producing high purity aromatic polycarboxylic acids |
JP2003510247A (ja) * | 1998-11-24 | 2003-03-18 | ディー ヴィンセント リン,ティー | 高純度芳香族ポリカルボン酸及びその誘導体の精製及び製造過程 |
EP1212277B1 (en) | 1999-08-30 | 2004-04-21 | Mossi & Ghisolfi International S.A. | An integrated process for the production of 2,6-naphthalene dicarboxylic acid |
US6649263B2 (en) | 2001-11-16 | 2003-11-18 | Honeywell International Inc. | Polyester resin and industrial yarn process |
DE10206168A1 (de) * | 2002-02-14 | 2003-08-21 | Guehring Joerg | Kupplung für mudular aufgebaute Werkzeughalterarme |
US7276625B2 (en) * | 2002-10-15 | 2007-10-02 | Eastman Chemical Company | Process for production of a carboxylic acid/diol mixture suitable for use in polyester production |
US7132566B2 (en) * | 2003-09-22 | 2006-11-07 | Eastman Chemical Company | Process for the purification of a crude carboxylic acid slurry |
US7074954B2 (en) * | 2002-12-09 | 2006-07-11 | Eastman Chemical Company | Process for the oxidative purification of terephthalic acid |
BR0316462A (pt) * | 2002-12-09 | 2005-10-11 | Eastman Chem Co | Processos para reduzir uma suspensão de ácido carboxìlico purificado, para purificar um produto de oxidação em estágios, para produzir um produto de ácido carboxìlico purificado, e, suspensão de ácido carboxìlico purificado |
US7161027B2 (en) | 2002-12-09 | 2007-01-09 | Eastman Chemical Company | Process for the oxidative purification of terephthalic acid |
WO2004063135A1 (ja) * | 2003-01-10 | 2004-07-29 | Mitsubishi Chemical Corporation | 芳香族カルボン酸の製造方法およびテレフタル酸の製造方法 |
US7193109B2 (en) * | 2003-03-06 | 2007-03-20 | Eastman Chemical Company | Process for production of a carboxylic acid/diol mixture suitable for use in polyester production |
US20050059709A1 (en) * | 2003-09-15 | 2005-03-17 | Meythaler Jay M. | Treatment of a neuropathy with rapid release aminopyridine |
US7214760B2 (en) * | 2004-01-15 | 2007-05-08 | Eastman Chemical Company | Process for production of a carboxylic acid/diol mixture suitable for use in polyester production |
US7307188B2 (en) * | 2004-04-09 | 2007-12-11 | Gtc Technology, Inc. | Purification of carboxylic acids by complexation with selective solvents |
US20050288527A1 (en) * | 2004-06-28 | 2005-12-29 | Cook William L | Method for preparing free-flowing crystalline material |
US7589231B2 (en) | 2004-09-02 | 2009-09-15 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7381836B2 (en) | 2004-09-02 | 2008-06-03 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7568361B2 (en) | 2004-09-02 | 2009-08-04 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7741515B2 (en) | 2004-09-02 | 2010-06-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7572936B2 (en) | 2004-09-02 | 2009-08-11 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7692036B2 (en) | 2004-11-29 | 2010-04-06 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7692037B2 (en) | 2004-09-02 | 2010-04-06 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7910769B2 (en) | 2004-09-02 | 2011-03-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7507857B2 (en) | 2004-09-02 | 2009-03-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7504535B2 (en) | 2004-09-02 | 2009-03-17 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7582793B2 (en) | 2004-09-02 | 2009-09-01 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7683210B2 (en) | 2004-09-02 | 2010-03-23 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7741516B2 (en) | 2005-05-19 | 2010-06-22 | Eastman Chemical Company | Process to enrich a carboxylic acid composition |
US7919652B2 (en) * | 2005-05-19 | 2011-04-05 | Eastman Chemical Company | Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone |
US7897809B2 (en) * | 2005-05-19 | 2011-03-01 | Eastman Chemical Company | Process to produce an enrichment feed |
US7834208B2 (en) * | 2005-05-19 | 2010-11-16 | Eastman Chemical Company | Process to produce a post catalyst removal composition |
US20060264662A1 (en) * | 2005-05-19 | 2006-11-23 | Gibson Philip E | Esterification of an enriched composition |
US7432395B2 (en) * | 2005-05-19 | 2008-10-07 | Eastman Chemical Company | Enriched carboxylic acid composition |
US7557243B2 (en) | 2005-05-19 | 2009-07-07 | Eastman Chemical Company | Enriched terephthalic acid composition |
US20060264656A1 (en) * | 2005-05-19 | 2006-11-23 | Fujitsu Limited | Enrichment process using compounds useful in a polyester process |
US7880031B2 (en) * | 2005-05-19 | 2011-02-01 | Eastman Chemical Company | Process to produce an enrichment feed |
US7884231B2 (en) * | 2005-05-19 | 2011-02-08 | Eastman Chemical Company | Process to produce an enriched composition |
US20060264664A1 (en) * | 2005-05-19 | 2006-11-23 | Parker Kenny R | Esterification of an exchange solvent enriched composition |
US7304178B2 (en) * | 2005-05-19 | 2007-12-04 | Eastman Chemical Company | Enriched isophthalic acid composition |
US7884232B2 (en) | 2005-06-16 | 2011-02-08 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7355068B2 (en) * | 2006-01-04 | 2008-04-08 | Eastman Chemical Company | Oxidation system with internal secondary reactor |
US20070179312A1 (en) * | 2006-02-02 | 2007-08-02 | O'meadhra Ruairi Seosamh | Process for the purification of a crude carboxylic axid slurry |
US8697906B2 (en) * | 2006-03-01 | 2014-04-15 | Grupo Petrotemex, S.A. De C.V. | Methods and apparatus for producing a low-moisture carboxylic acid wet cake |
US8173835B2 (en) * | 2006-03-01 | 2012-05-08 | Grupo Petrotemex, S.A. De C.V. | Method and apparatus for drying carboxylic acid |
US7888529B2 (en) | 2006-03-01 | 2011-02-15 | Eastman Chemical Company | Process to produce a post catalyst removal composition |
US8614350B2 (en) | 2008-01-15 | 2013-12-24 | Eastman Chemical Company | Carboxylic acid production process employing solvent from esterification of lignocellulosic material |
US8455680B2 (en) | 2008-01-15 | 2013-06-04 | Eastman Chemical Company | Carboxylic acid production process employing solvent from esterification of lignocellulosic material |
BRPI1006621A2 (pt) * | 2009-04-24 | 2016-04-19 | INVISTA Technologies S à r l | "método de resfriar uma corrente de água-mãe" |
KR20130110151A (ko) * | 2010-08-23 | 2013-10-08 | 소니 주식회사 | 유기 박막의 형성 방법 및 형성 장치, 및 유기 디바이스의 제조 방법 |
CN102234226A (zh) * | 2010-09-02 | 2011-11-09 | 华东理工大学 | 一种从碱减量废液中回收提纯对苯二甲酸的方法 |
CN102179063A (zh) * | 2011-03-23 | 2011-09-14 | 苏州汇通色谱分离纯化有限公司 | 高压液-液萃取方法 |
CN103030554B (zh) * | 2011-09-30 | 2015-04-08 | 中国石油化工股份有限公司 | 溶剂置换粗对苯二甲酸氧化浆料的方法 |
CN103121943B (zh) * | 2011-11-18 | 2015-08-12 | 中国石油化工股份有限公司 | 提纯粗间苯二甲酸氧化浆料的方法 |
RU2475475C1 (ru) * | 2011-12-26 | 2013-02-20 | Открытое акционерное общество "Каустик" (ОАО "Каустик") | Способ получения диамида терефталевой кислоты |
US9024059B2 (en) | 2011-12-29 | 2015-05-05 | Uop Llc | Process for producing terephthalic acid |
US9156765B2 (en) | 2011-12-29 | 2015-10-13 | Uop Llc | Process for oxidizing alkyl-aromatic compounds |
US8697905B2 (en) | 2011-12-29 | 2014-04-15 | Uop Llc | Process for producing terephthalic acid |
US8759571B2 (en) | 2011-12-29 | 2014-06-24 | Uop Llc | Process for oxidizing alkyl-aromatic compounds |
US9085522B2 (en) | 2011-12-29 | 2015-07-21 | Uop Llc | Process for producing terephthalic acid |
US8927764B2 (en) | 2011-12-29 | 2015-01-06 | Uop Llc | Process for producing terephthalic acid |
US9150484B2 (en) | 2011-12-29 | 2015-10-06 | Uop Llc | Process for producing terephthalic acid |
US9045408B2 (en) | 2011-12-29 | 2015-06-02 | Uop Llc | Process for oxidizing alkyl-aromatic compounds |
CN108623065B (zh) * | 2017-03-22 | 2020-08-25 | 天华化工机械及自动化研究设计院有限公司 | Pta精制单元母液的回收利用方法 |
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MX2023013755A (es) | 2021-05-20 | 2023-12-04 | Carbios | Proceso para degradar un producto de plastico que comprende al menos un poliester. |
CN116368120A (zh) * | 2021-07-19 | 2023-06-30 | 株式会社Lg化学 | 用于合成再生塑料的单体组合物、其制备方法以及使用其的再生塑料、模制品、增塑剂组合物 |
KR20240101673A (ko) | 2021-11-16 | 2024-07-02 | 까르비오 | 에스테라제의 신규 용도 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB818211A (en) * | 1955-11-08 | 1959-08-12 | Hoechst Ag | Manufacture of pure terephthalic acid |
US3931305A (en) * | 1973-08-20 | 1976-01-06 | Standard Oil Company | Terephthalic acid recovery by continuous flash crystallization |
US4380662A (en) * | 1981-03-16 | 1983-04-19 | Labofina, S.A. | Process for the purification of terephthalic acid |
US5159109A (en) * | 1990-06-25 | 1992-10-27 | Amoco Corporation | Purification of organic polycarboxylic acids |
EP0551596B1 (en) * | 1991-12-03 | 1996-05-15 | Mitsubishi Chemical Corporation | Process for producing naphtalenedicarboxylic acid |
US5767311A (en) * | 1995-06-07 | 1998-06-16 | Glitsch International, Inc. | Method and apparatus for preparing purified terephtalic acid |
-
1997
- 1997-10-31 US US08/962,030 patent/US5840968A/en not_active Expired - Lifetime
-
1998
- 1998-10-29 KR KR1020007004687A patent/KR100603723B1/ko not_active IP Right Cessation
- 1998-10-29 CN CN98810798A patent/CN1127471C/zh not_active Expired - Fee Related
- 1998-10-29 CA CA002307783A patent/CA2307783C/en not_active Expired - Fee Related
- 1998-10-29 WO PCT/US1998/022942 patent/WO1999023055A1/en active IP Right Grant
- 1998-10-29 ES ES98956315T patent/ES2263227T3/es not_active Expired - Lifetime
- 1998-10-29 DE DE69835229T patent/DE69835229T2/de not_active Expired - Lifetime
- 1998-10-29 RU RU2000113847/04A patent/RU2213725C2/ru not_active IP Right Cessation
- 1998-10-29 ID IDP981421A patent/ID21201A/id unknown
- 1998-10-29 BR BRPI9813349-7A patent/BR9813349B1/pt not_active IP Right Cessation
- 1998-10-29 AU AU12868/99A patent/AU1286899A/en not_active Abandoned
- 1998-10-29 TR TR2000/01138T patent/TR200001138T2/xx unknown
- 1998-10-29 JP JP2000518932A patent/JP4381600B2/ja not_active Expired - Fee Related
- 1998-10-29 EP EP98956315A patent/EP1030829B1/en not_active Expired - Lifetime
- 1998-10-30 MY MYPI98004967A patent/MY119529A/en unknown
- 1998-10-30 AR ARP980105476A patent/AR017765A1/es not_active Application Discontinuation
-
1999
- 1999-02-22 TW TW087118140A patent/TW505627B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
KR20010031634A (ko) | 2001-04-16 |
JP4381600B2 (ja) | 2009-12-09 |
TR200001138T2 (tr) | 2000-09-21 |
AU1286899A (en) | 1999-05-24 |
CA2307783C (en) | 2008-12-30 |
DE69835229D1 (de) | 2006-08-24 |
BR9813349B1 (pt) | 2010-08-24 |
RU2213725C2 (ru) | 2003-10-10 |
MY119529A (en) | 2005-06-30 |
WO1999023055A1 (en) | 1999-05-14 |
US5840968A (en) | 1998-11-24 |
KR100603723B1 (ko) | 2006-07-26 |
JP2001521917A (ja) | 2001-11-13 |
AR017765A1 (es) | 2001-10-24 |
EP1030829B1 (en) | 2006-07-12 |
ID21201A (id) | 1999-05-06 |
CN1278239A (zh) | 2000-12-27 |
CN1127471C (zh) | 2003-11-12 |
DE69835229T2 (de) | 2006-11-23 |
ES2263227T3 (es) | 2006-12-01 |
CA2307783A1 (en) | 1999-05-14 |
EP1030829A4 (en) | 2003-01-02 |
EP1030829A1 (en) | 2000-08-30 |
TW505627B (en) | 2002-10-11 |
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B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
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B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2385 DE 20-09-2016 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |