BR112023002512A2 - Processo para purificação de glicol recuperado a partir da reciclagem química de resíduo de poliéster - Google Patents
Processo para purificação de glicol recuperado a partir da reciclagem química de resíduo de poliésterInfo
- Publication number
- BR112023002512A2 BR112023002512A2 BR112023002512A BR112023002512A BR112023002512A2 BR 112023002512 A2 BR112023002512 A2 BR 112023002512A2 BR 112023002512 A BR112023002512 A BR 112023002512A BR 112023002512 A BR112023002512 A BR 112023002512A BR 112023002512 A2 BR112023002512 A2 BR 112023002512A2
- Authority
- BR
- Brazil
- Prior art keywords
- stream
- component
- ethylene glycol
- distillation column
- chemical recycling
- Prior art date
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title abstract 22
- 238000000034 method Methods 0.000 title abstract 6
- 229920000728 polyester Polymers 0.000 title abstract 4
- 238000004064 recycling Methods 0.000 title abstract 3
- 239000000126 substance Substances 0.000 title abstract 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title abstract 2
- 239000002699 waste material Substances 0.000 title abstract 2
- 238000004821 distillation Methods 0.000 abstract 6
- 238000009835 boiling Methods 0.000 abstract 1
- -1 polyethylene terephthalate Polymers 0.000 abstract 1
- 229920000139 polyethylene terephthalate Polymers 0.000 abstract 1
- 239000005020 polyethylene terephthalate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/128—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis
- C07C29/1285—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis of esters of organic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J11/00—Recovery or working-up of waste materials
- C08J11/04—Recovery or working-up of waste materials of polymers
- C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
- C08J11/18—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material
- C08J11/22—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with organic oxygen-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/095—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of organic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/20—Dihydroxylic alcohols
- C07C31/202—Ethylene glycol
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
- C07C69/80—Phthalic acid esters
- C07C69/82—Terephthalic acid esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
Abstract
PROCESSO PARA PURIFICAÇÃO DE GLICOL RECUPERADO A PARTIR DA RECICLAGEM QUÍMICA DE RESÍDUO DE POLIÉSTER. Um processo para purificar etilenoglicol de grau poliéster a partir de etilenoglicol bruto contendo pelo menos um primeiro componente e um segundo componente que têm um ponto de ebulição abaixo do etilenoglicol que inclui (a) fornecer uma corrente de etilenoglicol bruto por despolimerização de tereftalato de polietileno em um processo de reciclagem química; (b) introduzir a corrente de etilenoglicol bruto em uma primeira coluna de destilação para destilar o primeiro componente e remover o primeiro componente do processo; (c) retirar uma primeira corrente da porção inferior da primeira coluna de destilação e alimentar a primeira corrente em uma segunda coluna de destilação para destilar o segundo componente e remover o segundo componente do processo; (d) retirar uma segunda corrente da porção inferior da segunda coluna de destilação e alimentar a segunda corrente em uma terceira coluna de destilação; e (e) recuperar etilenoglicol de grau poliéster da terceira coluna de destilação.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US202063063479P | 2020-08-10 | 2020-08-10 | |
PCT/US2021/045147 WO2022035725A1 (en) | 2020-08-10 | 2021-08-09 | Process for purification of recovered glycol from chemical recycling of waste polyester |
Publications (1)
Publication Number | Publication Date |
---|---|
BR112023002512A2 true BR112023002512A2 (pt) | 2023-04-04 |
Family
ID=80247348
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112023002512A BR112023002512A2 (pt) | 2020-08-10 | 2021-08-09 | Processo para purificação de glicol recuperado a partir da reciclagem química de resíduo de poliéster |
Country Status (11)
Country | Link |
---|---|
US (1) | US20230312864A1 (pt) |
EP (1) | EP4192805A1 (pt) |
JP (1) | JP2023537393A (pt) |
KR (1) | KR20230074720A (pt) |
CN (1) | CN116033967A (pt) |
AU (1) | AU2021325856A1 (pt) |
BR (1) | BR112023002512A2 (pt) |
CA (1) | CA3188894A1 (pt) |
GB (1) | GB2612252A (pt) |
MX (1) | MX2023001634A (pt) |
WO (1) | WO2022035725A1 (pt) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2023193942A1 (de) * | 2022-04-04 | 2023-10-12 | Evonik Operations Gmbh | Verbessertes verfahren zur depolymerisierung von polyethylenterephthalat |
WO2023193941A1 (de) * | 2022-04-04 | 2023-10-12 | Evonik Operations Gmbh | Verbessertes verfahren zur depolymerisierung von polyethylenterephthalat |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4830712A (en) * | 1987-09-29 | 1989-05-16 | Union Carbide Corporation | Process for refining ethylene glycol |
JPH062687B2 (ja) * | 1988-12-09 | 1994-01-12 | ユニオン、カーバイド、コーポレーション | エチレングリコールを精製する方法 |
DE19629042C2 (de) * | 1996-07-19 | 1999-02-25 | Cet Umwelttechnik Entwicklungs | Verfahren zur Gewinnung von Terephthalsäure und Ethylenglykol, insbesondere aus Polyethylenterephthalat-Abfällen und Vorrichtung zur Durchführung des Verfahrens |
DE60042656D1 (de) * | 1999-10-22 | 2009-09-10 | Teijin Ltd | Verfahren zur abtrennung und rückgewinnung von dimethylterephthalat und ethylenglykol aus polyesterabfällen |
JP3808672B2 (ja) * | 1999-11-26 | 2006-08-16 | 東洋製罐株式会社 | 回収ポリエチレンテレフタレート粉砕品からのテレフタル酸の工業的回収方法 |
CN101928201B (zh) * | 2009-06-26 | 2013-04-10 | 上海焦化有限公司 | 一种煤制乙二醇粗产品的提纯工艺 |
US20190202764A1 (en) * | 2016-05-23 | 2019-07-04 | Shell Oil Company | Process for the separation of glycols |
GB201710508D0 (en) * | 2017-06-30 | 2017-08-16 | Johnson Matthey Davy Technologies Ltd | Process |
EA202190121A1 (ru) * | 2018-06-25 | 2021-06-07 | 9449710 Канада Инк. | Получение сложных эфиров терефталевой кислоты |
-
2021
- 2021-08-09 CA CA3188894A patent/CA3188894A1/en active Pending
- 2021-08-09 GB GB2301887.2A patent/GB2612252A/en active Pending
- 2021-08-09 JP JP2023509575A patent/JP2023537393A/ja active Pending
- 2021-08-09 BR BR112023002512A patent/BR112023002512A2/pt unknown
- 2021-08-09 US US18/020,571 patent/US20230312864A1/en active Pending
- 2021-08-09 CN CN202180056468.0A patent/CN116033967A/zh active Pending
- 2021-08-09 WO PCT/US2021/045147 patent/WO2022035725A1/en active Application Filing
- 2021-08-09 MX MX2023001634A patent/MX2023001634A/es unknown
- 2021-08-09 KR KR1020237008594A patent/KR20230074720A/ko unknown
- 2021-08-09 EP EP21856491.2A patent/EP4192805A1/en active Pending
- 2021-08-09 AU AU2021325856A patent/AU2021325856A1/en active Pending
Also Published As
Publication number | Publication date |
---|---|
JP2023537393A (ja) | 2023-08-31 |
US20230312864A1 (en) | 2023-10-05 |
WO2022035725A1 (en) | 2022-02-17 |
MX2023001634A (es) | 2023-03-08 |
AU2021325856A1 (en) | 2023-03-09 |
KR20230074720A (ko) | 2023-05-31 |
CN116033967A (zh) | 2023-04-28 |
GB2612252A (en) | 2023-04-26 |
EP4192805A1 (en) | 2023-06-14 |
GB202301887D0 (en) | 2023-03-29 |
CA3188894A1 (en) | 2022-02-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06W | Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette] |