BR112022003609A2 - Método de purificação para matéria-prima biológica - Google Patents

Método de purificação para matéria-prima biológica

Info

Publication number
BR112022003609A2
BR112022003609A2 BR112022003609A BR112022003609A BR112022003609A2 BR 112022003609 A2 BR112022003609 A2 BR 112022003609A2 BR 112022003609 A BR112022003609 A BR 112022003609A BR 112022003609 A BR112022003609 A BR 112022003609A BR 112022003609 A2 BR112022003609 A2 BR 112022003609A2
Authority
BR
Brazil
Prior art keywords
fraction
raw material
acylglycerols
containing compounds
nitrogen
Prior art date
Application number
BR112022003609A
Other languages
English (en)
Other versions
BR112022003609B1 (pt
Inventor
Olli Visuri
Original Assignee
Neste Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Neste Oyj filed Critical Neste Oyj
Publication of BR112022003609A2 publication Critical patent/BR112022003609A2/pt
Publication of BR112022003609B1 publication Critical patent/BR112022003609B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/50—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids in the presence of hydrogen, hydrogen donors or hydrogen generating compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G67/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only
    • C10G67/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/005—Refining fats or fatty oils by wave energy or electric current, e.g. electrodialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/02—Refining fats or fatty oils by chemical reaction
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/12—Refining fats or fatty oils by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/02—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with glycerol
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • C12P7/6454—Glycerides by esterification
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Zoology (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Electrochemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)

Abstract

método de purificação para matéria-prima biológica. a presente invenção se refere a um método para purificação de matéria-prima biológica (70), em particular reduzindo ou removendo compostos contendo nitrogênio da mesma, e a um aparelho para o mesmo. o método compreende submeter a matéria-prima (70) a uma primeira etapa de separação (80) para obter uma primeira fração (90) compreendendo ácidos graxos livres e compostos contendo nitrogênio e coletar o resíduo (85) compreendendo acilgliceróis. a primeira fração (90) é reagida com acilglicerol (100) para obter acilgliceróis do ácido graxo livre na mesma. essa fração é ainda submetida a uma segunda etapa de separação (120) para obter uma segunda fração (125) compreendendo compostos contendo nitrogênio, a qual é dispensada como produto de resíduo. os resquícios (130) da segunda etapa de separação (120) contendo os acilgliceróis formados são coletados.
BR112022003609-4A 2019-08-30 2020-08-31 Método de purificação para matéria-prima biológica BR112022003609B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20195721A FI129823B (en) 2019-08-30 2019-08-30 Purification procedure for biological input material
FI20195721 2019-08-30
PCT/FI2020/050563 WO2021038138A1 (en) 2019-08-30 2020-08-31 Purification method for biological feedstock

Publications (2)

Publication Number Publication Date
BR112022003609A2 true BR112022003609A2 (pt) 2022-05-31
BR112022003609B1 BR112022003609B1 (pt) 2023-01-24

Family

ID=72613932

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112022003609-4A BR112022003609B1 (pt) 2019-08-30 2020-08-31 Método de purificação para matéria-prima biológica

Country Status (8)

Country Link
US (1) US20220403287A1 (pt)
EP (1) EP4022015B1 (pt)
CN (1) CN114599437A (pt)
BR (1) BR112022003609B1 (pt)
CA (1) CA3149442C (pt)
ES (1) ES2964984T3 (pt)
FI (1) FI129823B (pt)
WO (1) WO2021038138A1 (pt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4370241A2 (en) * 2021-07-12 2024-05-22 Chemtor, Lp Micromixing for high throughput microfluidic refining
EP4186968A1 (en) * 2021-11-24 2023-05-31 Neste Oyj Fat rendering
WO2023094480A1 (en) * 2021-11-24 2023-06-01 Neste Oyj Fat rendering

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2290045A1 (en) * 2009-07-27 2011-03-02 Total Petrochemicals Research Feluy A process for the production of bio-naphtha from complex mixtures of natural occurring fats and oils
ES2556788T3 (es) * 2011-04-14 2016-01-20 Alfa Laval Corporate Ab Un proceso para la esterificación autocatalítica de ácidos grasos
WO2013023086A1 (en) * 2011-08-09 2013-02-14 Sapphire Energy, Inc. Compositions of matter comprising extracted algae oil
FI127206B2 (en) 2012-04-18 2021-08-31 Upm Kymmene Corp Method for producing biofuel or biofuel components
US20140020282A1 (en) * 2012-07-23 2014-01-23 Paul Lavella, SR. Method and system for integrated biodiesel production
US9738855B2 (en) * 2013-02-04 2017-08-22 Tehnochem Process for converting low and high free fatty acid containing oils into no free fatty acid containing oils and associated systems and devices
WO2014201001A1 (en) * 2013-06-11 2014-12-18 Renewable Energy Group, Inc. Production of biodiesel and products obtained therefrom
CN108977277A (zh) * 2018-08-22 2018-12-11 金溪遥遥领先高科有限公司 一种油脂脱酸和甘油二酯油的制造方法及分子蒸馏设备

Also Published As

Publication number Publication date
CA3149442C (en) 2023-03-28
FI129823B (en) 2022-09-15
FI20195721A1 (en) 2021-03-01
ES2964984T3 (es) 2024-04-10
EP4022015A1 (en) 2022-07-06
CA3149442A1 (en) 2021-03-04
US20220403287A1 (en) 2022-12-22
BR112022003609B1 (pt) 2023-01-24
WO2021038138A1 (en) 2021-03-04
EP4022015C0 (en) 2023-09-20
CN114599437A (zh) 2022-06-07
EP4022015B1 (en) 2023-09-20

Similar Documents

Publication Publication Date Title
BR112022003609A2 (pt) Método de purificação para matéria-prima biológica
KR102342647B1 (ko) 열처리에 의한 공급원료의 정제방법
RU2011143527A (ru) Усовершенствованный способ быстрого гидролиза биомассы с высоким содержанием твердых веществ
JP5808479B2 (ja) 脂肪酸の自己触媒エステル化のための方法
JP5893750B2 (ja) 脂肪および油の脱酸
RU2010126166A (ru) Обработка жировых материалов для их очистки
DE60329977D1 (de) Destillatives verfahren zur gewinnung und auftrennung von phytosterolen und phytostanolen aus tallölpech
EP2910129A1 (de) Zusammensetzung für die enzymatische Ölentschleimung
KR20220047322A (ko) 고온 및 고압에서 지방을 가수분해하여 바이오연료를 생산하기 위한 공급물의 전처리 방법
US2835682A (en) Sterol recovery process
JP2022515784A (ja) 脂質材料を処理するための方法
EA200500051A1 (ru) Способ выделения стеролов растительного происхождения из побочных продуктов, образующихся при очистке растительного масла
US20070093662A1 (en) Method of obtaining 2-mercaptobenzothiazole
US10150934B2 (en) Method for the purification of fatty acid aklyl esters
BR112022014823A2 (pt) Processo para recuperação e purificação de oligosacarídeos do leite humano
US9045715B2 (en) Process for purifying crude fatty alcohols
EP2522650B1 (en) Process for purifying crude fatty alcohols
JP5993932B2 (ja) 植物油を分留するためのプロセス
KR20180067261A (ko) 바이오 중유를 제조하는 방법
US11370990B2 (en) Process for isolation of sterols and a fraction rich in fatty acids and resin acids
JP2006124424A (ja) 油脂の分別処理方法
BR112019019079A2 (pt) método para extração de fitoesteróis a partir do breu de resina líquida
CN104098423B (zh) 5-亚乙基-2-降冰片烯enb的生产方法
BR112012032774A2 (pt) processo e sistema para a separação de finos de ácido carboxílico
TH1801008054A (th) วิธีการ และชุดเครื่องสำหรับการผลิตผลิตภัณฑ์

Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 31/08/2020, OBSERVADAS AS CONDICOES LEGAIS