BR112018012553A2 - tratamento de superfície da fase gasosa para tratar fibra de carbono, e, processo contínuo para fabricar fibra de carbono. - Google Patents
tratamento de superfície da fase gasosa para tratar fibra de carbono, e, processo contínuo para fabricar fibra de carbono.Info
- Publication number
- BR112018012553A2 BR112018012553A2 BR112018012553A BR112018012553A BR112018012553A2 BR 112018012553 A2 BR112018012553 A2 BR 112018012553A2 BR 112018012553 A BR112018012553 A BR 112018012553A BR 112018012553 A BR112018012553 A BR 112018012553A BR 112018012553 A2 BR112018012553 A2 BR 112018012553A2
- Authority
- BR
- Brazil
- Prior art keywords
- carbon fiber
- surface treatment
- gas phase
- nitrogen
- continuous process
- Prior art date
Links
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title abstract 7
- 229920000049 Carbon (fiber) Polymers 0.000 title abstract 5
- 239000004917 carbon fiber Substances 0.000 title abstract 5
- 238000004381 surface treatment Methods 0.000 title abstract 3
- 238000010924 continuous production Methods 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 6
- 229910052757 nitrogen Inorganic materials 0.000 abstract 3
- 239000000835 fiber Substances 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
- D01F11/12—Chemical after-treatment of artificial filaments or the like during manufacture of carbon with inorganic substances ; Intercalation
- D01F11/128—Nitrides, nitrogen carbides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
- D01F11/12—Chemical after-treatment of artificial filaments or the like during manufacture of carbon with inorganic substances ; Intercalation
- D01F11/122—Oxygen, oxygen-generating compounds
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/34—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxygen, ozone or ozonides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
- D06M11/60—Ammonia as a gas or in solution
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/40—Fibres of carbon
Abstract
um tratamento de superfície da fase gasosa para tratar fibra de carbono incluindo (a) expor uma fibra de carbono a uma atmosfera de oxidação gasosa para formar uma fibra de carbono modificada com uma superfície da fibra oxidada; seguido por (b) expor a superfície da fibra oxidada a uma atmosfera contendo nitrogênio gasoso para formar uma fibra de carbono modificada com uma superfície enriquecida com nitrogênio, em que a superfície enriquecida com nitrogênio apresenta um aumento na razão de nitrogênio da superfície para carbono da superfície (n/c) comparado à superfície da fibra de carbono antes da exposição a (a). etapas (a) e (b) são realizadas continuamente sem nenhum tratamento de superfície intermediário adicional.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201562270656P | 2015-12-22 | 2015-12-22 | |
US62/270,656 | 2015-12-22 | ||
PCT/US2016/067574 WO2017112598A1 (en) | 2015-12-22 | 2016-12-19 | Process for gas phase surface treatment |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112018012553A2 true BR112018012553A2 (pt) | 2018-12-04 |
BR112018012553B1 BR112018012553B1 (pt) | 2022-12-06 |
Family
ID=57822036
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112018012553-9A BR112018012553B1 (pt) | 2015-12-22 | 2016-12-19 | Tratamento de superfície da fase gasosa para tratar fibra de carbono contínua, e, processo contínuo para fabricar fibra de carbono |
Country Status (12)
Country | Link |
---|---|
US (2) | US10060053B2 (pt) |
EP (1) | EP3394331B1 (pt) |
JP (1) | JP7092671B2 (pt) |
KR (1) | KR20180094081A (pt) |
CN (1) | CN108431311B (pt) |
AU (1) | AU2016377496B2 (pt) |
BR (1) | BR112018012553B1 (pt) |
CA (1) | CA3009340A1 (pt) |
ES (1) | ES2899079T3 (pt) |
MX (1) | MX2018007275A (pt) |
TW (1) | TWI699466B (pt) |
WO (1) | WO2017112598A1 (pt) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111286816B (zh) * | 2018-12-10 | 2022-11-29 | 天津工业大学 | 一种具有平滑表面的聚丙烯腈基碳纤维的制备方法 |
CN110528277A (zh) * | 2019-08-21 | 2019-12-03 | 大同新成新材料股份有限公司 | 一种碳纤维的表面处理方法 |
CN115710817A (zh) * | 2022-10-07 | 2023-02-24 | 河南师范大学 | 一种臭氧辅助激光制备高缺陷多孔碳纤维的方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA1018716A (en) * | 1972-12-22 | 1977-10-11 | Kureha Kagaku Kogyo Kabushiki Kaisha | Process for the surface treatment of carbon fibres |
JPS5116219B2 (pt) * | 1972-12-22 | 1976-05-22 | ||
JPS5116220B2 (pt) * | 1972-12-22 | 1976-05-22 | ||
US4507272A (en) * | 1983-05-09 | 1985-03-26 | Hitco | Method of purifying partially carbonized pan material prior to carbonization |
US4608402A (en) * | 1985-08-09 | 1986-08-26 | E. I. Du Pont De Nemours And Company | Surface treatment of pitch-based carbon fibers |
JP2514637B2 (ja) * | 1986-09-20 | 1996-07-10 | 日機装 株式会社 | 気相成長炭素繊維の表面処理方法 |
JPS6385167A (ja) * | 1986-09-22 | 1988-04-15 | 東レ株式会社 | 表面改質炭素繊維とその製造方法 |
JPS6468570A (en) * | 1987-09-03 | 1989-03-14 | Asahi Chemical Ind | Surface modification of carbon fiber |
JP3656864B2 (ja) * | 1996-02-14 | 2005-06-08 | 東レ株式会社 | 炭素繊維およびその製造方法ならびにその炭素繊維を使用したプリプレグ |
JP2001207377A (ja) * | 2000-01-28 | 2001-08-03 | Toho Rayon Co Ltd | 表面改質された炭素繊維 |
JP4986453B2 (ja) | 2005-12-31 | 2012-07-25 | キョーラク株式会社 | 車両用空調ダクト |
JP2011017100A (ja) * | 2009-07-09 | 2011-01-27 | Toray Ind Inc | 炭素繊維の製造方法 |
CN103215692B (zh) * | 2013-03-26 | 2015-05-13 | 北京化工大学 | 一种高碳收率聚丙烯腈基碳纤维的制备方法 |
CN103806274B (zh) * | 2014-03-03 | 2015-09-16 | 哈尔滨工业大学 | 一种碳纤维表面接枝聚合物的方法 |
PT3117777T (pt) | 2014-03-12 | 2020-06-17 | Integral Geometry Science Inc | Método de tomografia de dispersão e dispositivo de tomografia de dispersão |
KR101563892B1 (ko) * | 2014-04-09 | 2015-10-30 | 인하대학교 산학협력단 | 수소저장용 활성탄소섬유 |
-
2016
- 2016-12-19 ES ES16826805T patent/ES2899079T3/es active Active
- 2016-12-19 US US15/382,832 patent/US10060053B2/en active Active
- 2016-12-19 WO PCT/US2016/067574 patent/WO2017112598A1/en active Application Filing
- 2016-12-19 MX MX2018007275A patent/MX2018007275A/es active IP Right Grant
- 2016-12-19 CN CN201680075389.3A patent/CN108431311B/zh active Active
- 2016-12-19 EP EP16826805.0A patent/EP3394331B1/en active Active
- 2016-12-19 BR BR112018012553-9A patent/BR112018012553B1/pt active IP Right Grant
- 2016-12-19 CA CA3009340A patent/CA3009340A1/en not_active Abandoned
- 2016-12-19 KR KR1020187020185A patent/KR20180094081A/ko active IP Right Grant
- 2016-12-19 AU AU2016377496A patent/AU2016377496B2/en active Active
- 2016-12-19 JP JP2018532441A patent/JP7092671B2/ja active Active
- 2016-12-22 TW TW105142627A patent/TWI699466B/zh not_active IP Right Cessation
-
2018
- 2018-07-25 US US16/045,470 patent/US20180327935A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
TWI699466B (zh) | 2020-07-21 |
WO2017112598A1 (en) | 2017-06-29 |
US20170175298A1 (en) | 2017-06-22 |
EP3394331A1 (en) | 2018-10-31 |
MX2018007275A (es) | 2018-09-06 |
ES2899079T3 (es) | 2022-03-10 |
US20180327935A1 (en) | 2018-11-15 |
KR20180094081A (ko) | 2018-08-22 |
AU2016377496A1 (en) | 2018-06-14 |
US10060053B2 (en) | 2018-08-28 |
CN108431311A (zh) | 2018-08-21 |
TW201736655A (zh) | 2017-10-16 |
AU2016377496B2 (en) | 2020-05-21 |
JP7092671B2 (ja) | 2022-06-28 |
BR112018012553B1 (pt) | 2022-12-06 |
CN108431311B (zh) | 2021-06-25 |
CA3009340A1 (en) | 2017-06-29 |
EP3394331B1 (en) | 2021-09-01 |
JP2018538459A (ja) | 2018-12-27 |
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Legal Events
Date | Code | Title | Description |
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B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 19/12/2016, OBSERVADAS AS CONDICOES LEGAIS |