BR112017014298B1 - Método para preparar um concentrado de café, e, concentrado de café - Google Patents
Método para preparar um concentrado de café, e, concentrado de café Download PDFInfo
- Publication number
- BR112017014298B1 BR112017014298B1 BR112017014298-8A BR112017014298A BR112017014298B1 BR 112017014298 B1 BR112017014298 B1 BR 112017014298B1 BR 112017014298 A BR112017014298 A BR 112017014298A BR 112017014298 B1 BR112017014298 B1 BR 112017014298B1
- Authority
- BR
- Brazil
- Prior art keywords
- coffee
- extraction
- primary
- extract
- concentrate
- Prior art date
Links
- 239000012141 concentrate Substances 0.000 title claims abstract description 76
- 238000000034 method Methods 0.000 title claims abstract description 58
- 235000013353 coffee beverage Nutrition 0.000 claims abstract description 177
- 235000016213 coffee Nutrition 0.000 claims abstract description 168
- 238000000605 extraction Methods 0.000 claims abstract description 133
- 239000000284 extract Substances 0.000 claims abstract description 66
- 238000012546 transfer Methods 0.000 claims abstract description 15
- 239000007787 solid Substances 0.000 claims description 49
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 37
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 claims description 27
- 239000007788 liquid Substances 0.000 claims description 26
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 claims description 22
- 241000533293 Sesbania emerus Species 0.000 claims description 22
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 claims description 22
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 claims description 19
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 claims description 19
- 235000001368 chlorogenic acid Nutrition 0.000 claims description 19
- 229940074393 chlorogenic acid Drugs 0.000 claims description 19
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 claims description 19
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 claims description 19
- CHWNEIVBYREQRF-UHFFFAOYSA-N 4-Ethyl-2-methoxyphenol Chemical compound CCC1=CC=C(O)C(OC)=C1 CHWNEIVBYREQRF-UHFFFAOYSA-N 0.000 claims description 18
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- 239000003550 marker Substances 0.000 claims description 14
- DBERHVIZRVGDFO-UHFFFAOYSA-N Acetoxyacetone Chemical compound CC(=O)COC(C)=O DBERHVIZRVGDFO-UHFFFAOYSA-N 0.000 claims description 13
- 238000001704 evaporation Methods 0.000 claims description 11
- 230000008020 evaporation Effects 0.000 claims description 11
- GWTUHAXUUFROTF-UHFFFAOYSA-N pseudochlorogenic acid Natural products C1C(O)C(O)C(O)CC1(C(O)=O)OC(=O)C=CC1=CC=C(O)C(O)=C1 GWTUHAXUUFROTF-UHFFFAOYSA-N 0.000 claims description 11
- -1 1-caffeoylquinic acid lactone Chemical class 0.000 claims description 10
- GWTUHAXUUFROTF-NCZKRNLISA-N 1-O-caffeoylquinic acid Natural products O[C@@H]1C[C@@](C[C@@H](O)[C@@H]1O)(OC(=O)C=Cc2ccc(O)c(O)c2)C(=O)O GWTUHAXUUFROTF-NCZKRNLISA-N 0.000 claims description 9
- 238000011084 recovery Methods 0.000 claims description 8
- WQOXQRCZOLPYPM-UHFFFAOYSA-N dimethyl disulfide Chemical compound CSSC WQOXQRCZOLPYPM-UHFFFAOYSA-N 0.000 claims description 6
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- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims 1
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- 238000004458 analytical method Methods 0.000 description 7
- 230000001953 sensory effect Effects 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
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- 239000011521 glass Substances 0.000 description 4
- 150000002596 lactones Chemical class 0.000 description 4
- 235000014666 liquid concentrate Nutrition 0.000 description 4
- IFMRCDUHXWRGLW-UHFFFAOYSA-N methoxysulfinyl methyl sulfite Chemical compound S(=O)(OC)OS(=O)OC IFMRCDUHXWRGLW-UHFFFAOYSA-N 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- AAWZDTNXLSGCEK-LNVDRNJUSA-N (3r,5r)-1,3,4,5-tetrahydroxycyclohexane-1-carboxylic acid Chemical compound O[C@@H]1CC(O)(C(O)=O)C[C@@H](O)C1O AAWZDTNXLSGCEK-LNVDRNJUSA-N 0.000 description 3
- CWVRJTMFETXNAD-GMZLATJGSA-N 5-Caffeoyl quinic acid Natural products O[C@H]1C[C@](O)(C[C@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-GMZLATJGSA-N 0.000 description 3
- 235000007460 Coffea arabica Nutrition 0.000 description 3
- 230000000875 corresponding effect Effects 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
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- 239000007789 gas Substances 0.000 description 3
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- 238000004519 manufacturing process Methods 0.000 description 3
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- 238000009283 thermal hydrolysis Methods 0.000 description 3
- 230000009466 transformation Effects 0.000 description 3
- 239000003039 volatile agent Substances 0.000 description 3
- 239000012224 working solution Substances 0.000 description 3
- GWTUHAXUUFROTF-AVXJPILUSA-N (3r,5r)-1-[(e)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy-3,4,5-trihydroxycyclohexane-1-carboxylic acid Chemical compound C1[C@@H](O)C(O)[C@H](O)CC1(C(O)=O)OC(=O)\C=C\C1=CC=C(O)C(O)=C1 GWTUHAXUUFROTF-AVXJPILUSA-N 0.000 description 2
- GWTUHAXUUFROTF-JUHZACGLSA-N 1-O-caffeoylquinic acid Chemical class [C@H]1(C[C@@](C(=O)O)(C[C@@H](O)[C@@H]1O)OC(=O)/C=C/C1=CC=C(O)C(O)=C1)O GWTUHAXUUFROTF-JUHZACGLSA-N 0.000 description 2
- 235000002187 Coffea robusta Nutrition 0.000 description 2
- AAWZDTNXLSGCEK-UHFFFAOYSA-N Cordycepinsaeure Natural products OC1CC(O)(C(O)=O)CC(O)C1O AAWZDTNXLSGCEK-UHFFFAOYSA-N 0.000 description 2
- 208000033962 Fontaine progeroid syndrome Diseases 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- AAWZDTNXLSGCEK-ZHQZDSKASA-N Quinic acid Natural products O[C@H]1CC(O)(C(O)=O)C[C@H](O)C1O AAWZDTNXLSGCEK-ZHQZDSKASA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000004809 Teflon Substances 0.000 description 2
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- 238000002474 experimental method Methods 0.000 description 2
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- CWVRJTMFETXNAD-KJOPMHRFSA-N (1r,3s,4s,5s)-3-[(e)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy-1,4,5-trihydroxycyclohexane-1-carboxylic acid Chemical compound O[C@H]1[C@@H](O)C[C@](O)(C(O)=O)C[C@@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-KJOPMHRFSA-N 0.000 description 1
- OCKGFTQIICXDQW-ZEQRLZLVSA-N 5-[(1r)-1-hydroxy-2-[4-[(2r)-2-hydroxy-2-(4-methyl-1-oxo-3h-2-benzofuran-5-yl)ethyl]piperazin-1-yl]ethyl]-4-methyl-3h-2-benzofuran-1-one Chemical compound C1=C2C(=O)OCC2=C(C)C([C@@H](O)CN2CCN(CC2)C[C@H](O)C2=CC=C3C(=O)OCC3=C2C)=C1 OCKGFTQIICXDQW-ZEQRLZLVSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
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- MYRTYDVEIRVNKP-UHFFFAOYSA-N divinylbenzene Substances C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 1
- 238000002451 electron ionisation mass spectrometry Methods 0.000 description 1
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- 238000010828 elution Methods 0.000 description 1
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- 238000013467 fragmentation Methods 0.000 description 1
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- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 238000010191 image analysis Methods 0.000 description 1
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- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
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- IDOWTHOLJBTAFI-UHFFFAOYSA-N phenmedipham Chemical compound COC(=O)NC1=CC=CC(OC(=O)NC=2C=C(C)C=CC=2)=C1 IDOWTHOLJBTAFI-UHFFFAOYSA-N 0.000 description 1
- 238000000252 photodiode array detection Methods 0.000 description 1
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- 238000012545 processing Methods 0.000 description 1
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- 230000000630 rising effect Effects 0.000 description 1
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- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
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- 238000012358 sourcing Methods 0.000 description 1
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- 230000003068 static effect Effects 0.000 description 1
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- 238000004885 tandem mass spectrometry Methods 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- QAIPRVGONGVQAS-DUXPYHPUSA-N trans-caffeic acid Chemical group OC(=O)\C=C\C1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-DUXPYHPUSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/28—Drying or concentrating coffee extract
- A23F5/285—Drying or concentrating coffee extract by evaporation, e.g. drying in thin layers, foam drying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/243—Liquid, semi-liquid or non-dried semi-solid coffee extract preparations; Coffee gels; Liquid coffee in solid capsules
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/04—Methods of roasting coffee
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/04—Methods of roasting coffee
- A23F5/06—Methods of roasting coffee of roasting extracted coffee ; Caramelisation of coffee extract
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/26—Extraction of water-soluble constituents
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Tea And Coffee (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP15150046 | 2015-01-02 | ||
EP15150046.9 | 2015-01-02 | ||
PCT/NL2015/050913 WO2016108688A1 (en) | 2015-01-02 | 2015-12-28 | Liquid espresso concentrate |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112017014298A2 BR112017014298A2 (pt) | 2018-03-06 |
BR112017014298B1 true BR112017014298B1 (pt) | 2021-11-16 |
Family
ID=52130187
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112017014298-8A BR112017014298B1 (pt) | 2015-01-02 | 2015-12-28 | Método para preparar um concentrado de café, e, concentrado de café |
Country Status (15)
Country | Link |
---|---|
US (1) | US9968110B2 (zh) |
EP (1) | EP3240432B1 (zh) |
JP (1) | JP6920992B2 (zh) |
KR (1) | KR20170101984A (zh) |
CN (1) | CN107404896B (zh) |
AU (1) | AU2015372676B2 (zh) |
BR (1) | BR112017014298B1 (zh) |
CA (1) | CA2972747C (zh) |
ES (1) | ES2740777T3 (zh) |
MX (1) | MX2017008806A (zh) |
PL (1) | PL3240432T3 (zh) |
RU (1) | RU2731286C2 (zh) |
SG (1) | SG11201705427WA (zh) |
UA (1) | UA122679C2 (zh) |
WO (1) | WO2016108688A1 (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU2015372675B2 (en) * | 2015-01-02 | 2020-04-30 | Koninklijke Douwe Egberts B.V. | Liquid espresso concentrate |
CN108003027B (zh) * | 2017-12-25 | 2021-07-06 | 北京微医智慧信息技术有限责任公司 | 1-o-咖啡酰奎宁酸、其衍生物、制备方法及其用途 |
GB2574850B (en) * | 2018-06-20 | 2022-12-14 | Douwe Egberts Bv | Method of beverage extraction and apparatus therefor |
JP7431748B2 (ja) | 2018-11-29 | 2024-02-15 | サントリーホールディングス株式会社 | コーヒー抽出液の製造方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2420615A (en) * | 1944-03-16 | 1947-05-13 | Harry Sachs | Manufacture of concentrated coffee extract |
US3821434A (en) * | 1970-07-01 | 1974-06-28 | Niro Atomizer As | Method for producing a coffee concentrate |
US3810766A (en) * | 1972-04-03 | 1974-05-14 | Gen Foods Corp | Method of extracting roasted coffee |
NL191402C (nl) * | 1977-10-06 | 1995-07-17 | Sara Lee De Nv | Werkwijze voor de primaire extractie van gemalen gebrande koffie. |
JPS58220653A (ja) * | 1982-06-17 | 1983-12-22 | Ajinomoto General Food Kk | コ−ヒ−エキスの製造方法 |
DE4038526A1 (de) * | 1990-12-03 | 1992-06-04 | Jacobs Suchard Ag | Verfahren zur herstellung von loeslichem kaffee |
NL1030178C2 (nl) * | 2005-10-12 | 2007-04-13 | Sara Lee De Nv | Werkwijze voor het bereiden van een koffie-extract, alsmede het daarmee te verkrijgen extract. |
RU2532851C2 (ru) * | 2009-04-28 | 2014-11-10 | Као Корпорейшн | Концентрированный экстракт кофе |
AU2012290763C1 (en) * | 2011-08-01 | 2016-06-02 | Koninklijke Douwe Egberts B.V. | Process for the production of a liquid coffee concentrate |
BR112014032684B1 (pt) | 2012-06-29 | 2020-10-13 | Koninklijke Douwe Egberts B.V | sistema |
BR112015018591B8 (pt) * | 2013-02-05 | 2021-09-14 | Douwe Egberts Bv | Processo para a produção de um concentrado de café líquido, e, concentrado de café líquido |
AU2015372675B2 (en) * | 2015-01-02 | 2020-04-30 | Koninklijke Douwe Egberts B.V. | Liquid espresso concentrate |
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2015
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BR112017014298A2 (pt) | 2018-03-06 |
EP3240432B1 (en) | 2019-06-19 |
AU2015372676A1 (en) | 2017-07-20 |
MX2017008806A (es) | 2017-10-19 |
EP3240432A1 (en) | 2017-11-08 |
WO2016108688A1 (en) | 2016-07-07 |
CN107404896A (zh) | 2017-11-28 |
US20170295815A1 (en) | 2017-10-19 |
RU2731286C2 (ru) | 2020-09-01 |
AU2015372676B2 (en) | 2020-04-30 |
CN107404896B (zh) | 2021-10-01 |
JP6920992B2 (ja) | 2021-08-18 |
UA122679C2 (uk) | 2020-12-28 |
CA2972747C (en) | 2022-07-19 |
PL3240432T3 (pl) | 2020-02-28 |
SG11201705427WA (en) | 2017-08-30 |
RU2017127269A (ru) | 2019-02-04 |
US9968110B2 (en) | 2018-05-15 |
JP2018500040A (ja) | 2018-01-11 |
RU2017127269A3 (zh) | 2019-07-17 |
KR20170101984A (ko) | 2017-09-06 |
CA2972747A1 (en) | 2016-07-07 |
ES2740777T3 (es) | 2020-02-06 |
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