BR112012019114A2 - processo e instalação para refrigerar ácido sulfúrico. - Google Patents

processo e instalação para refrigerar ácido sulfúrico.

Info

Publication number
BR112012019114A2
BR112012019114A2 BR112012019114A BR112012019114A BR112012019114A2 BR 112012019114 A2 BR112012019114 A2 BR 112012019114A2 BR 112012019114 A BR112012019114 A BR 112012019114A BR 112012019114 A BR112012019114 A BR 112012019114A BR 112012019114 A2 BR112012019114 A2 BR 112012019114A2
Authority
BR
Brazil
Prior art keywords
acid
water
heat exchanger
steam
sulfuric acid
Prior art date
Application number
BR112012019114A
Other languages
English (en)
Other versions
BR112012019114B1 (pt
Inventor
Karl-Heinz Daum
Wolfram Schalk
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj filed Critical Outotec Oyj
Publication of BR112012019114A2 publication Critical patent/BR112012019114A2/pt
Publication of BR112012019114B1 publication Critical patent/BR112012019114B1/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/80Apparatus
    • C01B17/806Absorbers; Heat exchangers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/765Multi-stage SO3-conversion
    • C01B17/7655Multi-stage SO3-conversion with intermediate absorption
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01KSTEAM ENGINE PLANTS; STEAM ACCUMULATORS; ENGINE PLANTS NOT OTHERWISE PROVIDED FOR; ENGINES USING SPECIAL WORKING FLUIDS OR CYCLES
    • F01K17/00Using steam or condensate extracted or exhausted from steam engine plant
    • F01K17/06Returning energy of steam, in exchanged form, to process, e.g. use of exhaust steam for drying solid fuel or plant
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01KSTEAM ENGINE PLANTS; STEAM ACCUMULATORS; ENGINE PLANTS NOT OTHERWISE PROVIDED FOR; ENGINES USING SPECIAL WORKING FLUIDS OR CYCLES
    • F01K23/00Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids
    • F01K23/02Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids the engine cycles being thermally coupled
    • F01K23/06Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids the engine cycles being thermally coupled combustion heat from one cycle heating the fluid in another cycle
    • F01K23/064Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids the engine cycles being thermally coupled combustion heat from one cycle heating the fluid in another cycle in combination with an industrial process, e.g. chemical, metallurgical
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/16Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged in parallel spaced relation
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/26Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with two or more fluidised beds, e.g. reactor and regeneration installations

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Sorption Type Refrigeration Machines (AREA)
  • Treating Waste Gases (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

processo e instalação para refreigerar ácido sulfúrico. ao refrigerar ácido que é retirado a partir de um aparelho de absorção (2) de uma instalação de ácido sulfúrico, o ácido é bombeado a partir de um tanque de bomba de ácido (9) em um trocador de calor (13) e, subsequentemente, fornecido de novo ao aparelho de absorção (2), em que água como meio de transporte de calor é aquecida no trocador de calor como o calor do ácido e é pelo menos parcialmente convertida em vapor, e em que a água é separada do vapor. prevê-se que o ácido é fornecido a um espaço de concha (12) do trocador de calor e a água é fornecida para aquecer os elementos de transferência dispostos no espaço de concha (12) e pelo menos parcialmente convertida em vapor, que o vapor gerado no trocador de calor (13) é separado a partir da água em um tambor de vapor (22), e que a água assim obtida é recirculada para o trocador de calor por meio de uma bomba (7).
BR112012019114-4A 2010-02-01 2011-01-11 processo e instalação para refrigerar ácido sulfúrico BR112012019114B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102010006541.2A DE102010006541B4 (de) 2010-02-01 2010-02-01 Verfahren und Anlage zum Abkühlen von Säure
PCT/EP2011/000074 WO2011091950A2 (en) 2010-02-01 2011-01-11 Process and plant for cooling acid

Publications (2)

Publication Number Publication Date
BR112012019114A2 true BR112012019114A2 (pt) 2016-09-13
BR112012019114B1 BR112012019114B1 (pt) 2019-11-12

Family

ID=44243155

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012019114-4A BR112012019114B1 (pt) 2010-02-01 2011-01-11 processo e instalação para refrigerar ácido sulfúrico

Country Status (17)

Country Link
US (1) US8906133B2 (pt)
EP (1) EP2531446B1 (pt)
KR (1) KR101687052B1 (pt)
CN (1) CN102741159B (pt)
AP (1) AP2012006435A0 (pt)
AU (1) AU2011209094B2 (pt)
BR (1) BR112012019114B1 (pt)
CL (1) CL2012002119A1 (pt)
DE (1) DE102010006541B4 (pt)
EA (1) EA021625B1 (pt)
EG (1) EG26895A (pt)
ES (1) ES2514667T3 (pt)
MA (1) MA34022B1 (pt)
MX (1) MX2012008670A (pt)
PL (1) PL2531446T3 (pt)
WO (1) WO2011091950A2 (pt)
ZA (1) ZA201204830B (pt)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JOP20200123A1 (ar) * 2010-01-20 2017-06-16 Mecs Inc استرجاع الطاقة في تصنيع حمض السلفريك
BR112014030687B1 (pt) * 2012-06-06 2021-03-30 Haldor Tops0E A/S Processo para a conversão de so2 em so3 e instalação de referido processo
EA031910B1 (ru) * 2013-10-24 2019-03-29 Оутотек (Финлэнд) Ой Способ эксплуатации сернокислотной установки
TR201905939T4 (tr) 2014-12-19 2019-05-21 Outotec Finland Oy Gelişmiş enerji tasarruflu sülfürik asit üretimine yönelik proses ve tesis.
WO2017001463A1 (en) * 2015-07-02 2017-01-05 Haldor Topsøe A/S Process for production of sulfuric acid
BR102016003690B1 (pt) * 2016-02-22 2022-08-30 Nc Engenharia, Industria E Comercio Ltda Método e equipamento para resfriar ácido sulfúrico
CN107764103A (zh) * 2016-08-22 2018-03-06 宜兴市宏塍净化给排水制造有限公司 废硫酸冷却塔
ES2951905T3 (es) 2017-07-06 2023-10-25 Topsoe As Un método para el enfriamiento entre lechos en plantas de ácido sulfúrico de gas húmedo
JP2019067994A (ja) * 2017-10-04 2019-04-25 トヨタ自動車株式会社 積層基板とその製造方法
WO2021056089A1 (pt) * 2019-09-27 2021-04-01 Clark Solutions Llc Trocador de calor multifluído tamponado de segurança e processo de troca térmica multifluído tamponado de segurança

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2766442A (en) * 1952-11-26 1956-10-09 Jr William H Meyer Leak detection apparatus
US4123107A (en) * 1977-02-03 1978-10-31 Freeport Minerals Company Integrated sulfur mining - sulfuric acid production system
US4576813A (en) * 1983-07-05 1986-03-18 Monsanto Company Heat recovery from concentrated sulfuric acid
US4996038A (en) * 1983-07-05 1991-02-26 Monsanto Company Heat recovery from concentrated sulfuric acid
US5130112A (en) * 1990-03-23 1992-07-14 Monsanto Company Method for recovering high grade process energy from a contact sulfuric acid process
DE10128032A1 (de) * 2001-06-08 2002-12-12 Outokumpu Oy Verfahren zum Schutz gegen Korrossion eines Stahlteils aus austenitischem oder halbaustenitischem Stahl bei der Herstellung von Schwefelsäure
DE10128774A1 (de) 2001-06-13 2002-12-19 Outokumpu Oy Plattenwärmeaustauscher mit anodischem Korrosionsschutz
DE102004022506B4 (de) * 2004-05-05 2012-06-21 Outokumpu Oyj Verfahren und Anlage zur Herstellung von Schwefelsäure aus schwefeldioxidreichen Gasen
DE102005008109A1 (de) * 2005-02-21 2006-08-24 Outokumpu Technology Oy Verfahren und Anlage zur Herstellung von Schwefelsäure

Also Published As

Publication number Publication date
US8906133B2 (en) 2014-12-09
US20130000869A1 (en) 2013-01-03
EA021625B1 (ru) 2015-07-30
EA201290649A1 (ru) 2013-03-29
WO2011091950A3 (en) 2011-10-27
BR112012019114B1 (pt) 2019-11-12
AP2012006435A0 (en) 2012-08-31
CL2012002119A1 (es) 2012-11-30
DE102010006541A1 (de) 2011-09-29
ZA201204830B (en) 2013-09-25
EP2531446A2 (en) 2012-12-12
CN102741159B (zh) 2014-11-19
CN102741159A (zh) 2012-10-17
MX2012008670A (es) 2012-08-23
ES2514667T3 (es) 2014-10-28
DE102010006541B4 (de) 2016-03-17
MA34022B1 (fr) 2013-02-01
EP2531446B1 (en) 2014-09-03
KR101687052B1 (ko) 2016-12-15
WO2011091950A2 (en) 2011-08-04
EG26895A (en) 2014-12-03
AU2011209094B2 (en) 2013-11-14
KR20120139707A (ko) 2012-12-27
AU2011209094A1 (en) 2012-07-26
PL2531446T3 (pl) 2015-04-30

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Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06T Formal requirements before examination [chapter 6.20 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 11/01/2011, OBSERVADAS AS CONDICOES LEGAIS. (CO) 20 (VINTE) ANOS CONTADOS A PARTIR DE 11/01/2011, OBSERVADAS AS CONDICOES LEGAIS

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 11A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2652 DE 03-11-2021 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.