BR112012015219B1 - Processo para iniciar um catalisador de óxido de etileno altamente seletivo - Google Patents

Processo para iniciar um catalisador de óxido de etileno altamente seletivo Download PDF

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Publication number
BR112012015219B1
BR112012015219B1 BR112012015219-0A BR112012015219A BR112012015219B1 BR 112012015219 B1 BR112012015219 B1 BR 112012015219B1 BR 112012015219 A BR112012015219 A BR 112012015219A BR 112012015219 B1 BR112012015219 B1 BR 112012015219B1
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BR
Brazil
Prior art keywords
temperature
catalyst
moderator
fact
hours
Prior art date
Application number
BR112012015219-0A
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English (en)
Portuguese (pt)
Other versions
BR112012015219A2 (pt
Inventor
Rizkalla Nabil
B. Castagnola Norma
Desai Girish
Original Assignee
Scientific Design Company, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
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Application filed by Scientific Design Company, Inc. filed Critical Scientific Design Company, Inc.
Publication of BR112012015219A2 publication Critical patent/BR112012015219A2/pt
Publication of BR112012015219B1 publication Critical patent/BR112012015219B1/pt

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/32Manganese, technetium or rhenium
    • B01J23/36Rhenium
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00Aliphatic unsaturated hydrocarbons
    • C07C11/02Alkenes
    • C07C11/04Ethene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D303/00Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02Compounds containing oxirane rings
    • C07D303/04Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Epoxy Compounds (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
BR112012015219-0A 2009-12-23 2010-12-20 Processo para iniciar um catalisador de óxido de etileno altamente seletivo BR112012015219B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US28971909P 2009-12-23 2009-12-23
US61/289,719 2009-12-23
PCT/US2010/061192 WO2011079056A2 (en) 2009-12-23 2010-12-20 A process for initiating a highly selective ethylene oxide catalyst

Publications (2)

Publication Number Publication Date
BR112012015219A2 BR112012015219A2 (pt) 2015-09-22
BR112012015219B1 true BR112012015219B1 (pt) 2018-04-03

Family

ID=44152005

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012015219-0A BR112012015219B1 (pt) 2009-12-23 2010-12-20 Processo para iniciar um catalisador de óxido de etileno altamente seletivo

Country Status (12)

Country Link
US (1) US8487123B2 (enExample)
EP (1) EP2521718B1 (enExample)
JP (1) JP2013515730A (enExample)
KR (1) KR101815664B1 (enExample)
CN (1) CN102666515B (enExample)
BR (1) BR112012015219B1 (enExample)
CA (1) CA2784603C (enExample)
IN (1) IN2012DN05077A (enExample)
MX (1) MX2012007440A (enExample)
RU (1) RU2538969C2 (enExample)
TW (1) TWI485142B (enExample)
WO (1) WO2011079056A2 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012141942A1 (en) * 2011-04-11 2012-10-18 Dow Technology Investments Llc Process for conditioning a high efficiency ethylene oxide catalyst
CN104203931A (zh) * 2011-10-18 2014-12-10 哈桑·伊萨·阿拉哈迈迪 具有添加缓和剂的环氧化方法
CN104884443B (zh) * 2012-12-31 2017-07-04 科学设计公司 用于环氧乙烷催化剂的启动方法
CN105008339B (zh) * 2013-01-11 2017-09-12 科学设计公司 具有后调节步骤的环氧化工艺
EP3087061B1 (en) * 2013-12-23 2018-04-11 Scientific Design Company Inc. Epoxidation process
WO2019055773A1 (en) 2017-09-15 2019-03-21 MultiPhase Solutions, Inc. GAS PHASE CHROMATOGRAPHY OF SELECTIVE HALOGEN DETECTION FOR ONLINE ANALYSIS AND CONTROL OF SELECTIVE OXIDATION CHEMICAL PRODUCTION PROCESSES
CN114057670B (zh) * 2020-07-29 2024-06-07 中国石油化工股份有限公司 一种用于启动乙烯环氧化工艺的方法
CN114057669B (zh) * 2020-07-29 2023-12-08 中国石油化工股份有限公司 一种乙烯环氧化恒温开车方法
CN114436998A (zh) * 2020-11-05 2022-05-06 中国石油化工股份有限公司 一种乙烯环氧化开车方法
CA3214971A1 (en) * 2021-04-08 2022-10-13 Shell Internationale Research Maatschappij B.V. Moderator and catalyst performance optimization for epoxidation of ethylene

Family Cites Families (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2279469A (en) * 1942-04-14 Process of making olefin oxides
SE321462B (enExample) 1962-10-10 1970-03-09 Halcon International Inc
GB1170663A (en) * 1967-03-22 1969-11-12 Shell Int Research Process for preparing Silver Catalysts
US3702259A (en) * 1970-12-02 1972-11-07 Shell Oil Co Chemical production of metallic silver deposits
US4761394A (en) * 1986-10-31 1988-08-02 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4766105A (en) * 1986-10-31 1988-08-23 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4908343A (en) * 1987-02-20 1990-03-13 Union Carbide Chemicals And Plastics Company Inc. Catalyst composition for oxidation of ethylene to ethylene oxide
US5057481A (en) * 1987-02-20 1991-10-15 Union Carbide Chemicals And Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
CA1339317C (en) 1988-07-25 1997-08-19 Ann Marie Lauritzen Process for producing ethylene oxide
US4874879A (en) * 1988-07-25 1989-10-17 Shell Oil Company Process for starting-up an ethylene oxide reactor
DE68925767T2 (de) * 1988-08-30 1996-08-14 Union Carbide Corp Katalysatoren für die Herstellung von Ethylenoxid und Verfahren zur deren Herstellung
US5187140A (en) * 1989-10-18 1993-02-16 Union Carbide Chemicals & Plastics Technology Corporation Alkylene oxide catalysts containing high silver content
US5102848A (en) * 1990-09-28 1992-04-07 Union Carbide Chemicals & Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US5155242A (en) * 1991-12-05 1992-10-13 Shell Oil Company Process for starting-up an ethylene oxide reactor
US5407888A (en) * 1992-05-12 1995-04-18 Basf Aktiengesellschaft Silver catalyst
US6492065B2 (en) * 1997-12-05 2002-12-10 Victor Company Of Japan, Limited Hologram color filter, production method of the same hologram color filter and space light modulating apparatus using the same hologram color filter
US6008388A (en) * 1998-04-16 1999-12-28 Arco Chemical Technology, L.P. Epoxidation process
JP4042332B2 (ja) 2001-02-27 2008-02-06 三菱化学株式会社 レニウム含有触媒を用いるオレフィンオキシドの製造方法
MX257124B (es) * 2002-06-28 2008-05-14 Shell Int Research Metodo para iniciar un proceso de epoxidacion, catalizador y proceso de epoxidacion de una olefina.
AU2003243757A1 (en) 2002-06-28 2004-01-19 Shell Oil Company A method for improving the selectivity of a catalyst and a process for the epoxidation of an olefin
MX245604B (es) * 2002-06-28 2007-05-04 Shell Int Research Metodo para iniciar un proceso de epoxidacion y proceso de epoxidacion de una olefina.
US6992209B2 (en) * 2002-12-09 2006-01-31 Battelle Memorial Institute Methods of forming alpha, beta-unsaturated acids and esters
CA2540563C (en) * 2003-09-29 2013-01-08 Union Carbide Chemicals & Plastics Technology Corporation A process for the production of alkylene oxide using a gas-phase promoter system
US8791280B2 (en) * 2005-08-10 2014-07-29 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparation of catalyst carrier and its use in catalyst preparation
US7696368B2 (en) 2007-05-11 2010-04-13 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Start-up of high selectivity catalysts in olefin oxide plants
US7553980B2 (en) * 2007-09-26 2009-06-30 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst
CN102056909B (zh) * 2008-05-07 2014-03-05 国际壳牌研究有限公司 环氧化工艺的开车方法及环氧乙烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或链烷醇胺的制备方法

Also Published As

Publication number Publication date
KR101815664B1 (ko) 2018-01-05
CA2784603A1 (en) 2011-06-30
EP2521718B1 (en) 2014-07-02
CN102666515B (zh) 2015-05-20
WO2011079056A3 (en) 2011-11-17
TW201139392A (en) 2011-11-16
US20110152549A1 (en) 2011-06-23
CN102666515A (zh) 2012-09-12
CA2784603C (en) 2018-06-12
KR20120108029A (ko) 2012-10-04
TWI485142B (zh) 2015-05-21
US8487123B2 (en) 2013-07-16
RU2538969C2 (ru) 2015-01-10
JP2013515730A (ja) 2013-05-09
BR112012015219A2 (pt) 2015-09-22
RU2012131369A (ru) 2014-01-27
EP2521718A4 (en) 2013-06-19
EP2521718A2 (en) 2012-11-14
MX2012007440A (es) 2012-07-23
IN2012DN05077A (enExample) 2015-10-09
WO2011079056A2 (en) 2011-06-30

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B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]
B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 9A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2545 DE 15-10-2019 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.