BR112012014186A2 - formulação, artigo de compósito, e, processo de fabricação - Google Patents
formulação, artigo de compósito, e, processo de fabricaçãoInfo
- Publication number
- BR112012014186A2 BR112012014186A2 BR112012014186A BR112012014186A BR112012014186A2 BR 112012014186 A2 BR112012014186 A2 BR 112012014186A2 BR 112012014186 A BR112012014186 A BR 112012014186A BR 112012014186 A BR112012014186 A BR 112012014186A BR 112012014186 A2 BR112012014186 A2 BR 112012014186A2
- Authority
- BR
- Brazil
- Prior art keywords
- modified resin
- temperature
- resin system
- processes
- formulation
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
- B29C70/02—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising combinations of reinforcements, e.g. non-specified reinforcements, fibrous reinforcing inserts and fillers, e.g. particulate fillers, incorporated in matrix material, forming one or more layers and with or without non-reinforced or non-filled layers
- B29C70/021—Combinations of fibrous reinforcement and non-fibrous material
- B29C70/025—Combinations of fibrous reinforcement and non-fibrous material with particular filler
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
- B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
- B29C70/28—Shaping operations therefor
- B29C70/30—Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core
- B29C70/34—Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core and shaping or impregnating by compression, i.e. combined with compressing after the lay-up operation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
- B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
- B29C70/28—Shaping operations therefor
- B29C70/40—Shaping or impregnating by compression not applied
- B29C70/42—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles
- B29C70/44—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using isostatic pressure, e.g. pressure difference-moulding, vacuum bag-moulding, autoclave-moulding or expanding rubber-moulding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
- B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
- B29C70/28—Shaping operations therefor
- B29C70/40—Shaping or impregnating by compression not applied
- B29C70/42—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles
- B29C70/44—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using isostatic pressure, e.g. pressure difference-moulding, vacuum bag-moulding, autoclave-moulding or expanding rubber-moulding
- B29C70/443—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using isostatic pressure, e.g. pressure difference-moulding, vacuum bag-moulding, autoclave-moulding or expanding rubber-moulding and impregnating by vacuum or injection
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
- B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
- B29C70/28—Shaping operations therefor
- B29C70/40—Shaping or impregnating by compression not applied
- B29C70/42—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles
- B29C70/46—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using matched moulds, e.g. for deforming sheet moulding compounds [SMC] or prepregs
- B29C70/48—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using matched moulds, e.g. for deforming sheet moulding compounds [SMC] or prepregs and impregnating the reinforcements in the closed mould, e.g. resin transfer moulding [RTM], e.g. by vacuum
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F279/00—Macromolecular compounds obtained by polymerising monomers on to polymers of monomers having two or more carbon-to-carbon double bonds as defined in group C08F36/00
- C08F279/02—Macromolecular compounds obtained by polymerising monomers on to polymers of monomers having two or more carbon-to-carbon double bonds as defined in group C08F36/00 on to polymers of conjugated dienes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
- C08G59/38—Epoxy compounds containing three or more epoxy groups together with di-epoxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L55/00—Compositions of homopolymers or copolymers, obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in groups C08L23/00 - C08L53/00
- C08L55/04—Polyadducts obtained by the diene synthesis
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2063/00—Use of EP, i.e. epoxy resins or derivatives thereof, as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/06—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
- B29K2105/16—Fillers
- B29K2105/165—Hollow fillers, e.g. microballoons or expanded particles
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2207/00—Properties characterising the ingredient of the composition
- C08L2207/53—Core-shell polymer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Composite Materials (AREA)
- Medicinal Chemistry (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Reinforced Plastic Materials (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Casting Or Compression Moulding Of Plastics Or The Like (AREA)
- Inorganic Chemistry (AREA)
Abstract
formulação, artigo de compósito, e, processo de fabricação. formas de realização da invenção são direcionadas a sistemas de resina modificada para uso em processos de infusão de resina líquida (lri), variações de processos de lri e outros processos adequados. em uma forma de realização, o sistema de resina modificada inclui uma nova combinação de pelo menos uma resina de base, uma quantidade de partículas dentro deuma faixa predeterminada e uma quantidade de material termoplástico dentro de uma faixa predeterminada em que, quando combinado, o sistema de resina modificada tem uma viscosidade média abaixo de uma viscosidade média limiar em uma temperatura específica e um alto nível de dureza. o sistema de resina modificada pode incluir adicionalmente um agente de cura e outros componentes adequados. o sistema de resina modificada foi experimentalmente mostrado para exibir uma morfologia única, controlável e constante que pode ser pelo menos parcialmente responsável por comunicar uma dureza e resistência ao dano necessários a um compósito acabado sem impactar adversamente propriedades tais como viscosidade, limite de armazenamento, temperatura de cura, temperatura de transição vítrea ou módulo de tração do sistema de resina modificada.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB0922599.6 | 2009-12-23 | ||
GB0922599A GB0922599D0 (en) | 2009-12-23 | 2009-12-23 | Modified resin systems for liquid resin infusion applications, prepreg autoclave applications and hybrids thereof |
PCT/GB2010/002324 WO2011077094A1 (en) | 2009-12-23 | 2010-12-22 | Modified resin systems for liquid resin infusion applications & process methods related thereto |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112012014186A2 true BR112012014186A2 (pt) | 2016-05-31 |
BR112012014186B1 BR112012014186B1 (pt) | 2019-10-08 |
Family
ID=41716940
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112012014186-4A BR112012014186B1 (pt) | 2009-12-23 | 2010-12-22 | Sistema de resina modificada para infusão de resina líquida, e, processo de fabricação |
Country Status (13)
Country | Link |
---|---|
US (2) | US20110151232A1 (pt) |
EP (1) | EP2516139B1 (pt) |
JP (1) | JP5808057B2 (pt) |
KR (1) | KR101703378B1 (pt) |
CN (1) | CN103025508B (pt) |
AU (1) | AU2010334587B2 (pt) |
BR (1) | BR112012014186B1 (pt) |
CA (1) | CA2785279C (pt) |
ES (1) | ES2576133T3 (pt) |
GB (1) | GB0922599D0 (pt) |
MY (1) | MY160836A (pt) |
TW (1) | TWI517966B (pt) |
WO (1) | WO2011077094A1 (pt) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6207396B2 (ja) * | 2010-11-09 | 2017-10-04 | サイテク・テクノロジー・コーポレーシヨン | 二次強化用適合性キャリヤー |
US9879722B2 (en) * | 2013-03-11 | 2018-01-30 | Bell Helicopter Textron Inc. | Low shear modulus transition shim for elastomeric bearing bonding in torsional applications |
JP6720181B2 (ja) * | 2014-12-18 | 2020-07-08 | サイテック インダストリーズ インコーポレイテッド | 「液体樹脂注入に適した製造方法及び硬化性組成物」 |
CA2995200A1 (en) * | 2015-08-10 | 2017-02-16 | Cytec Industries Inc. | Prepreg material capable of providing lightning strike protection and burn-through resistance |
BR112018012124B1 (pt) * | 2015-12-16 | 2022-08-09 | Cytec Industries Inc | Métodos para infusão de resina e para fabricação de uma estrutura compósita |
PL3405337T3 (pl) | 2016-01-20 | 2023-11-27 | Zephyros Inc. | Termoplastyczne materiały epoksydowe z fazą rdzeń-otoczka |
JP6354884B1 (ja) * | 2017-03-13 | 2018-07-11 | 横浜ゴム株式会社 | シアネートエステル樹脂組成物およびプリプレグ |
CN107263887A (zh) * | 2017-07-04 | 2017-10-20 | 西安飞机工业(集团)有限责任公司 | 一种真空辅助定位装置及定位方法 |
GB201717639D0 (en) * | 2017-10-26 | 2017-12-13 | Cytec Ind Inc | Resin compositions and resin infusion process |
CN109986813A (zh) * | 2017-12-29 | 2019-07-09 | 北京金风科创风电设备有限公司 | 风力发电机组叶片内、外补强模具及其制备方法 |
EP4101878A4 (en) | 2020-02-03 | 2024-02-28 | Toray Industries | MOLDING MATERIAL AND FIBER REINFORCED COMPOSITE MATERIAL |
US11930565B1 (en) * | 2021-02-05 | 2024-03-12 | Mainstream Engineering Corporation | Carbon nanotube heater composite tooling apparatus and method of use |
JPWO2022176773A1 (pt) | 2021-02-18 | 2022-08-25 |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3035310A (en) * | 1956-01-23 | 1962-05-22 | Republic Aviat Corp | Method of making reinforced synthetic resin forming tool |
US4656208A (en) * | 1985-02-19 | 1987-04-07 | Hercules Incorporated | Thermosetting epoxy resin compositions and thermosets therefrom |
EP0228450B1 (en) * | 1985-06-26 | 1990-10-10 | The Dow Chemical Company | Rubber-modified epoxy compounds |
ES2088781T3 (es) * | 1990-01-19 | 1996-09-16 | Minnesota Mining & Mfg | Composicion termoendurecible. |
US5266610A (en) * | 1991-03-11 | 1993-11-30 | Ici Composites Inc. | Toughened cocontinuous resin system |
EP0525418B1 (en) * | 1991-07-30 | 2002-11-20 | Cytec Technology Corp. | Toughened, fiber-reinforced thermosetting resin matrix prepregs and composites made therefrom |
GB9616455D0 (en) * | 1996-08-05 | 1996-09-25 | Short Brothers Plc | Apparatus and method for forming a fibre reinforced resin composite component |
FR2753978B1 (fr) * | 1996-09-30 | 1999-05-14 | Inst Francais Du Petrole | Composition thermodurcissable, ses utilisations et preforme souple depliable comprenant cette composition |
CN1103350C (zh) * | 1999-06-11 | 2003-03-19 | 中国科学院化学研究所 | 一种环氧树脂复合物及其制备方法 |
US6537470B1 (en) * | 2000-09-01 | 2003-03-25 | Honeywell International Inc. | Rapid densification of porous bodies (preforms) with high viscosity resins or pitches using a resin transfer molding process |
GB2401081B (en) * | 2000-10-03 | 2005-06-01 | Structural Polymer Systems Ltd | Moulding material |
JP3874108B2 (ja) * | 2002-08-13 | 2007-01-31 | 信越化学工業株式会社 | エポキシ樹脂組成物 |
CN101242947B (zh) * | 2005-07-05 | 2010-08-11 | 快步科技私人有限公司 | 利用流体密度和压力生产复合材料部件的方法及生产系统 |
JP5307544B2 (ja) * | 2005-08-24 | 2013-10-02 | ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェン | 改善された耐衝撃性を有するエポキシ組成物 |
JP4983228B2 (ja) * | 2005-11-29 | 2012-07-25 | 味の素株式会社 | 多層プリント配線板の絶縁層用樹脂組成物 |
WO2008127556A1 (en) * | 2007-04-17 | 2008-10-23 | Hexcel Corporation | Pre-impregnated composite materials with improved performance |
GB0619401D0 (en) * | 2006-10-02 | 2006-11-08 | Hexcel Composites Ltd | Composite materials with improved performance |
ES2523142T3 (es) * | 2007-04-17 | 2014-11-21 | Hexcel Corporation | Material compuesto con mezcla de partículas termoplásticas |
GB0717507D0 (en) | 2007-09-07 | 2007-10-17 | Cytec Tech Corp | Composite materials and their use |
GB2460050A (en) * | 2008-05-14 | 2009-11-18 | Hexcel Composites Ltd | Epoxy composite |
GB2464085A (en) * | 2008-06-07 | 2010-04-07 | Hexcel Composites Ltd | Improved Conductivity of Resin Materials and Composite Materials |
WO2011025873A1 (en) * | 2009-08-31 | 2011-03-03 | Cytec Technology Corp. | High performance adhesive compositions |
-
2009
- 2009-12-23 GB GB0922599A patent/GB0922599D0/en not_active Ceased
-
2010
- 2010-12-09 US US12/963,823 patent/US20110151232A1/en not_active Abandoned
- 2010-12-22 ES ES10799119.2T patent/ES2576133T3/es active Active
- 2010-12-22 WO PCT/GB2010/002324 patent/WO2011077094A1/en active Application Filing
- 2010-12-22 CN CN201080059036.7A patent/CN103025508B/zh active Active
- 2010-12-22 BR BR112012014186-4A patent/BR112012014186B1/pt active IP Right Grant
- 2010-12-22 MY MYPI2012002370A patent/MY160836A/en unknown
- 2010-12-22 EP EP10799119.2A patent/EP2516139B1/en active Active
- 2010-12-22 KR KR1020127018919A patent/KR101703378B1/ko active IP Right Grant
- 2010-12-22 JP JP2012545433A patent/JP5808057B2/ja active Active
- 2010-12-22 CA CA2785279A patent/CA2785279C/en active Active
- 2010-12-22 AU AU2010334587A patent/AU2010334587B2/en active Active
- 2010-12-22 TW TW099145371A patent/TWI517966B/zh active
-
2017
- 2017-07-18 US US15/653,098 patent/US10836118B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
CA2785279A1 (en) | 2011-06-30 |
EP2516139B1 (en) | 2016-03-16 |
US10836118B2 (en) | 2020-11-17 |
GB0922599D0 (en) | 2010-02-10 |
WO2011077094A9 (en) | 2012-12-13 |
BR112012014186B1 (pt) | 2019-10-08 |
KR101703378B1 (ko) | 2017-02-06 |
KR20120108002A (ko) | 2012-10-04 |
JP2013515806A (ja) | 2013-05-09 |
AU2010334587B2 (en) | 2014-10-09 |
TW201136752A (en) | 2011-11-01 |
TWI517966B (zh) | 2016-01-21 |
AU2010334587A1 (en) | 2012-06-07 |
MY160836A (en) | 2017-03-31 |
EP2516139A1 (en) | 2012-10-31 |
JP5808057B2 (ja) | 2015-11-10 |
US20110151232A1 (en) | 2011-06-23 |
CN103025508B (zh) | 2015-11-25 |
WO2011077094A1 (en) | 2011-06-30 |
CA2785279C (en) | 2017-09-05 |
ES2576133T3 (es) | 2016-07-05 |
US20170326819A1 (en) | 2017-11-16 |
CN103025508A (zh) | 2013-04-03 |
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