BR112012000296A2 - composição e método para produção de um propante cerâmico ultraleve. - Google Patents

composição e método para produção de um propante cerâmico ultraleve.

Info

Publication number
BR112012000296A2
BR112012000296A2 BR112012000296A BR112012000296A BR112012000296A2 BR 112012000296 A2 BR112012000296 A2 BR 112012000296A2 BR 112012000296 A BR112012000296 A BR 112012000296A BR 112012000296 A BR112012000296 A BR 112012000296A BR 112012000296 A2 BR112012000296 A2 BR 112012000296A2
Authority
BR
Brazil
Prior art keywords
producing
composition
ceramic proppant
ultralight ceramic
ultralight
Prior art date
Application number
BR112012000296A
Other languages
English (en)
Inventor
Huang Zhijie
Li Ying
Lin Shengming
Wu Wenzhong
Original Assignee
Prop Supply And Service Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Prop Supply And Service Llc filed Critical Prop Supply And Service Llc
Publication of BR112012000296A2 publication Critical patent/BR112012000296A2/pt

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/60—Compositions for stimulating production by acting on the underground formation
    • C09K8/62—Compositions for forming crevices or fractures
    • C09K8/66—Compositions based on water or polar solvents
    • C09K8/665—Compositions based on water or polar solvents containing inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/24—Manufacture of porcelain or white ware
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62695—Granulation or pelletising
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/009—Porous or hollow ceramic granular materials, e.g. microballoons
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/60—Compositions for stimulating production by acting on the underground formation
    • C09K8/80—Compositions for reinforcing fractures, e.g. compositions of proppants used to keep the fractures open
    • E—FIXED CONSTRUCTIONS
    • E21—EARTH DRILLING; MINING
    • E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00—Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/25—Methods for stimulating production
    • E21B43/26—Methods for stimulating production by forming crevices or fractures
    • E—FIXED CONSTRUCTIONS
    • E21—EARTH DRILLING; MINING
    • E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00—Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/25—Methods for stimulating production
    • E21B43/26—Methods for stimulating production by forming crevices or fractures
    • E21B43/267—Methods for stimulating production by forming crevices or fractures reinforcing fractures by propping
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3232—Titanium oxides or titanates, e.g. rutile or anatase
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/528—Spheres
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/5296—Constituents or additives characterised by their shapes with a defined aspect ratio, e.g. indicating sphericity
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54—Particle size related information
    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5427—Particle size related information expressed by the size of the particles or aggregates thereof millimeter or submillimeter sized, i.e. larger than 0,1 mm
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/72—Products characterised by the absence or the low content of specific components, e.g. alkali metal free alumina ceramics
    • C—CHEMISTRY; METALLURGY
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    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/77—Density
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C04B2235/9669—Resistance against chemicals, e.g. against molten glass or molten salts
    • C04B2235/9692—Acid, alkali or halogen resistance

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Structural Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Mining & Mineral Resources (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • Physics & Mathematics (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)
BR112012000296A 2009-07-25 2010-07-23 composição e método para produção de um propante cerâmico ultraleve. BR112012000296A2 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US22856209P 2009-07-25 2009-07-25
CN2010101573464A CN101880524A (zh) 2010-04-27 2010-04-27 一种超轻密度陶粒支撑剂及其制备方法
PCT/US2010/042980 WO2011014410A1 (en) 2009-07-25 2010-07-23 Composition and method for producing an ultra-lightweight ceramic proppant

Publications (1)

Publication Number Publication Date
BR112012000296A2 true BR112012000296A2 (pt) 2016-02-23

Family

ID=43052674

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012000296A BR112012000296A2 (pt) 2009-07-25 2010-07-23 composição e método para produção de um propante cerâmico ultraleve.

Country Status (9)

Country Link
US (2) US8727003B2 (pt)
EP (1) EP2459846A4 (pt)
CN (1) CN101880524A (pt)
AU (1) AU2010276638B2 (pt)
BR (1) BR112012000296A2 (pt)
CA (1) CA2751907C (pt)
MX (1) MX2012000801A (pt)
RU (2) RU2014148285A (pt)
WO (1) WO2011014410A1 (pt)

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CN102390076B (zh) * 2011-10-24 2013-11-13 江苏省宜兴彩陶工艺厂 陶瓷瓶口干粉压力成型方法
CN102718530B (zh) * 2012-06-18 2014-01-29 陕西科技大学 一种利用蓝晶石、硅线石和红柱石制备压裂支撑剂的方法
US8772207B2 (en) * 2012-06-26 2014-07-08 Brownwood Clay Holdings, Llc Spherical pellets containing common clay particulate material useful as a proppant in hydraulic fracturing of oil and gas wells
CN102718469A (zh) * 2012-06-26 2012-10-10 福建瑞合通新材料有限公司 一种水力压裂用超轻质陶瓷颗粒及其制备方法
PL400420A1 (pl) 2012-08-17 2014-03-03 Baltic Ceramics Spólka Akcyjna Lekkie proppanty ceramiczne i sposób wytwarzania lekkich proppantów ceramicznych
WO2014011066A1 (en) 2012-07-11 2014-01-16 Baltic Ceramics S.A. Light ceramic proppants and a method of manufacturing of light ceramic proppants
US20150240150A1 (en) * 2012-07-11 2015-08-27 Baltic Ceramics S.A. Light ceramic proppants and a method of manufacturing of light ceramic proppants
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RU2499773C1 (ru) * 2012-09-14 2013-11-27 Юлия Алексеевна Щепочкина Сырьевая смесь для производства керамзита
CN102899016B (zh) * 2012-09-24 2015-04-01 宜兴市腾飞陶粒制造有限公司 一种采用助熔剂制备的高强度陶粒支撑剂及其制备方法
CN102876315B (zh) * 2012-10-13 2014-06-18 山西方兴耐火材料有限公司 一种低密度陶粒支撑剂及其制备方法
CN103159464B (zh) * 2013-04-16 2014-04-30 金刚新材料股份有限公司 一种利用炉渣制备页岩气开采用压裂支撑剂的方法
US10161236B2 (en) 2013-04-24 2018-12-25 Halliburton Energy Services, Inc. Methods for fracturing subterranean formations
PL406381A1 (pl) * 2013-12-05 2015-06-08 Baltic Ceramics Spółka Akcyjna Sposób wytwarzania lekkich proppantów ceramicznych i lekkie proppanty ceramiczne
CN103484098B (zh) * 2013-09-24 2016-06-22 淄博嘉丰矿业有限公司 低密度高强度的陶粒支撑剂及其制备方法
CN103468239B (zh) * 2013-09-24 2016-07-06 淄博嘉丰矿业有限公司 以焦宝石为原料的低密高强陶粒支撑剂及其制备方法
CN103468240B (zh) * 2013-09-24 2015-06-24 淄博嘉丰矿业有限公司 以焦宝石尾矿为原料的超低密陶粒支撑剂及其制备方法
US20160230083A1 (en) 2013-09-25 2016-08-11 Board Of Regents, The University Of Texas System Lightweight Proppants for Hydraulic Fracturing
EP2853520A1 (en) * 2013-09-26 2015-04-01 Baltic Ceramics S.A. Ceramic proppants of medium strength and a method for manufacturing thereof
CN103666443B (zh) * 2013-12-13 2016-06-29 淄博嘉丰矿业有限公司 低密陶粒支撑剂及其制备方法
CN103756665B (zh) * 2014-01-25 2016-03-30 金刚新材料股份有限公司 一种以焦宝石为原料的低密度支撑剂及其制备方法
US10017687B2 (en) 2014-05-14 2018-07-10 California Institute Of Technology Ultra-light ultra-strong proppants
WO2015200665A1 (en) * 2014-06-27 2015-12-30 Imerys Oilfield Minerals, Inc. Proppant-based chemical delivery system
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US20180258343A1 (en) * 2015-09-25 2018-09-13 Imerys Oilfield Minerals, Inc. Proppants having fine, narrow particle size distribution and related methods
CN105925257B (zh) * 2016-05-10 2018-10-16 太原科技大学 一种低密度陶粒支撑剂及其制备方法
US10364660B2 (en) * 2016-06-23 2019-07-30 Halliburton Energy Services, Inc. Proppant-free channels in a propped fracture using ultra-low density, degradable particulates
US10190041B2 (en) 2016-08-02 2019-01-29 University Of Utah Research Foundation Encapsulated porous proppant
CN107033870A (zh) * 2017-04-21 2017-08-11 常州市奥普泰科光电有限公司 一种低密度高强度石油压裂支撑剂的制备方法
DE102017111849A1 (de) * 2017-05-30 2018-12-06 HÜTTENES-ALBERTUS Chemische Werke Gesellschaft mit beschränkter Haftung Verfahren zur Herstellung von Isoliermaterial oder eines isolierenden Produkts für die Feuerfestindustrie, entsprechende Isoliermaterialien und Produkte sowie Verwendungen
US20190023978A1 (en) * 2017-07-21 2019-01-24 Saint-Gobain Ceramics & Plastics, Inc. Proppants and process for making the same
CN107445645B (zh) * 2017-08-16 2020-08-25 武汉钢铁有限公司 一种以铁矿石为主要原料的陶粒涂料
CN108585787A (zh) * 2018-07-10 2018-09-28 山西富森能源科技有限公司 利用改性低铝粉煤灰和河道淤砂制作超低密度陶粒支撑剂
CN110746170A (zh) * 2019-11-12 2020-02-04 陕西科技大学 一种用于修补石窟裂隙的灌浆支撑剂及其制备与使用方法
CN111875346A (zh) * 2020-08-12 2020-11-03 贵州宝鑫实业有限公司 一种生物陶粒及其制备方法

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CN101880524A (zh) 2010-11-10
EP2459846A4 (en) 2013-08-07
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US8727003B2 (en) 2014-05-20
AU2010276638A1 (en) 2012-01-19
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US20120118574A1 (en) 2012-05-17
AU2010276638B2 (en) 2015-08-13
US20140216741A1 (en) 2014-08-07
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RU2540695C2 (ru) 2015-02-10

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