AU655627B2 - Thermoplastic resins containing coated additives - Google Patents
Thermoplastic resins containing coated additives Download PDFInfo
- Publication number
- AU655627B2 AU655627B2 AU11239/92A AU1123992A AU655627B2 AU 655627 B2 AU655627 B2 AU 655627B2 AU 11239/92 A AU11239/92 A AU 11239/92A AU 1123992 A AU1123992 A AU 1123992A AU 655627 B2 AU655627 B2 AU 655627B2
- Authority
- AU
- Australia
- Prior art keywords
- composition according
- polyarylene ether
- reinforcing agent
- functionalized
- thermoplastic resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 229920005992 thermoplastic resin Polymers 0.000 title claims abstract description 21
- 239000000654 additive Substances 0.000 title description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 50
- 229920000412 polyarylene Polymers 0.000 claims abstract description 29
- 239000000203 mixture Substances 0.000 claims abstract description 26
- 239000012744 reinforcing agent Substances 0.000 claims abstract description 24
- 239000011248 coating agent Substances 0.000 claims abstract description 11
- 238000000576 coating method Methods 0.000 claims abstract description 11
- 239000007787 solid Substances 0.000 claims abstract 2
- 239000000835 fiber Substances 0.000 claims description 24
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 10
- 229920010524 Syndiotactic polystyrene Polymers 0.000 claims description 8
- 150000002170 ethers Chemical class 0.000 claims description 8
- 239000003365 glass fiber Substances 0.000 claims description 6
- 229920001577 copolymer Polymers 0.000 claims description 4
- 239000007822 coupling agent Substances 0.000 claims description 4
- 239000011521 glass Substances 0.000 claims description 4
- 229920001519 homopolymer Polymers 0.000 claims description 4
- 238000004513 sizing Methods 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 229910052582 BN Inorganic materials 0.000 claims description 3
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 3
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 3
- 239000004917 carbon fiber Substances 0.000 claims description 3
- 239000000919 ceramic Substances 0.000 claims description 3
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 3
- 239000000178 monomer Substances 0.000 claims description 3
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical compound [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 claims description 3
- 241000531908 Aramides Species 0.000 claims description 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 2
- 239000004952 Polyamide Substances 0.000 claims description 2
- 150000001412 amines Chemical class 0.000 claims description 2
- XQJHRCVXRAJIDY-UHFFFAOYSA-N aminophosphine Chemical compound PN XQJHRCVXRAJIDY-UHFFFAOYSA-N 0.000 claims description 2
- 229920003235 aromatic polyamide Polymers 0.000 claims description 2
- 229920002647 polyamide Polymers 0.000 claims description 2
- 229920000515 polycarbonate Polymers 0.000 claims description 2
- 239000004417 polycarbonate Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 239000004793 Polystyrene Substances 0.000 claims 1
- 125000001142 dicarboxylic acid group Chemical group 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 229920002223 polystyrene Polymers 0.000 claims 1
- 229920005989 resin Polymers 0.000 description 8
- 239000011347 resin Substances 0.000 description 8
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000000376 reactant Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- -1 poly(2,6-dimethyl-1,4-phenylene) Polymers 0.000 description 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000806 elastomer Substances 0.000 description 2
- XEOCKQIQXJNTER-UHFFFAOYSA-N gold palladium platinum Chemical compound [Pd].[Pd].[Pd].[Pd].[Pd].[Pt].[Pt].[Pt].[Pt].[Pt].[Pt].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au].[Au] XEOCKQIQXJNTER-UHFFFAOYSA-N 0.000 description 2
- 229920005669 high impact polystyrene Polymers 0.000 description 2
- 239000004797 high-impact polystyrene Substances 0.000 description 2
- 238000010348 incorporation Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 229920001955 polyphenylene ether Polymers 0.000 description 2
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- HIDBROSJWZYGSZ-UHFFFAOYSA-N 1-phenylpyrrole-2,5-dione Chemical compound O=C1C=CC(=O)N1C1=CC=CC=C1 HIDBROSJWZYGSZ-UHFFFAOYSA-N 0.000 description 1
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- 229930185605 Bisphenol Natural products 0.000 description 1
- 239000004604 Blowing Agent Substances 0.000 description 1
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- 239000004642 Polyimide Substances 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- 239000002174 Styrene-butadiene Substances 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- MTAZNLWOLGHBHU-UHFFFAOYSA-N butadiene-styrene rubber Chemical compound C=CC=C.C=CC1=CC=CC=C1 MTAZNLWOLGHBHU-UHFFFAOYSA-N 0.000 description 1
- 229960001701 chloroform Drugs 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000012718 coordination polymerization Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 239000011256 inorganic filler Substances 0.000 description 1
- 229910003475 inorganic filler Inorganic materials 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 150000001451 organic peroxides Chemical class 0.000 description 1
- 150000002918 oxazolines Chemical class 0.000 description 1
- 238000005691 oxidative coupling reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920001721 polyimide Polymers 0.000 description 1
- 229920006380 polyphenylene oxide Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000011342 resin composition Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000011115 styrene butadiene Substances 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/24—Coatings containing organic materials
- C03C25/26—Macromolecular compounds or prepolymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/48—Polymers modified by chemical after-treatment
- C08G65/485—Polyphenylene oxides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
- C08J5/08—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials glass fibres
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Reinforced Plastic Materials (AREA)
- Hydrogenated Pyridines (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polyamides (AREA)
- Laminated Bodies (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US66046191A | 1991-02-26 | 1991-02-26 | |
| US660461 | 1991-02-26 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU1123992A AU1123992A (en) | 1992-08-27 |
| AU655627B2 true AU655627B2 (en) | 1995-01-05 |
Family
ID=24649629
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU11239/92A Ceased AU655627B2 (en) | 1991-02-26 | 1992-02-25 | Thermoplastic resins containing coated additives |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5426171A (enExample) |
| EP (1) | EP0501625B1 (enExample) |
| JP (1) | JP3198465B2 (enExample) |
| KR (1) | KR100206398B1 (enExample) |
| AT (1) | ATE141628T1 (enExample) |
| AU (1) | AU655627B2 (enExample) |
| CA (1) | CA2061798A1 (enExample) |
| DE (1) | DE69212863T2 (enExample) |
| TW (1) | TW224981B (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0736364B1 (en) * | 1994-10-20 | 2001-07-25 | Idemitsu Petrochemical Co., Ltd. | Styrene resin pellets and product of molding thereof |
| DE10016280A1 (de) * | 2000-04-03 | 2001-10-04 | Basf Ag | Schlagzähe thermoplastische Formmassen aus syndiotaktischem Polystyrol, Glasfasern und Acrylat-Schlagzähmodifier |
| JP2003185064A (ja) * | 2001-12-19 | 2003-07-03 | Ge Plastics Japan Ltd | 配管部材 |
| US6894102B2 (en) * | 2002-05-20 | 2005-05-17 | General Electric | Syndiotactic polystyrene blends |
| JP4007877B2 (ja) | 2002-08-07 | 2007-11-14 | 日本ジーイープラスチックス株式会社 | ワイヤ・ケーブル被覆材用樹脂組成物 |
| DE102010030615A1 (de) * | 2010-06-28 | 2011-12-29 | Sgl Carbon Se | Verbundwerkstoff, Verfahren zum Herstellen eines Verbundwerkstoffes und Verwendung des Verbundwerkstoffes |
| US20220049093A1 (en) * | 2019-02-28 | 2022-02-17 | Idemitsu Kosan Co.,Ltd. | Resin composition and molded body of same |
| JP2020186314A (ja) * | 2019-05-14 | 2020-11-19 | 旭化成株式会社 | 樹脂用充填材および熱可塑性樹脂組成物 |
| CN115916906B (zh) * | 2020-08-27 | 2024-09-13 | 出光兴产株式会社 | 热塑性树脂组合物 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU446200B2 (en) * | 1968-09-05 | 1970-09-24 | Dow Corning Corporation | Reinforced polystyrene and its copolymers |
| AU612152B2 (en) * | 1987-06-12 | 1991-07-04 | E.I. Du Pont De Nemours And Company | Composites |
| AU614539B2 (en) * | 1987-09-18 | 1991-09-05 | Yvan Landler | Composite material and process for the production thereof |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3375228A (en) * | 1967-05-10 | 1968-03-26 | Gen Electric | Hot capping of polyphenylene ethers |
| JPS4926700B1 (enExample) * | 1970-08-21 | 1974-07-11 | ||
| US3881977A (en) * | 1972-11-15 | 1975-05-06 | Us Air Force | Treatment of graphite fibers |
| NL8301284A (nl) * | 1983-04-12 | 1984-11-01 | Gen Electric | Polymeermengsel dat een polyfenyleenether en eventueel een polystyreen en/of een met rubber gemodificeerd polystyreen bevat en daaruit gevormde voorwerpen. |
| US4654405A (en) * | 1985-12-05 | 1987-03-31 | Borg-Warner Chemicals, Inc. | Carboxylated phenylene ether resins |
| DE3780383T2 (de) * | 1986-09-10 | 1992-12-17 | Mitsubishi Gas Chemical Co | Polyphenyleneaetherharzzusammensetzung. |
| GB2204888A (en) * | 1987-05-18 | 1988-11-23 | Textilver Sa | Fibre reinforced matrix |
| IT1223326B (it) * | 1987-10-28 | 1990-09-19 | Montedipe Spa | Composizioni termoplastiche a base di polimeri sindiotattici dello stirene e polifenileneteri |
| JPH01135868A (ja) * | 1987-11-24 | 1989-05-29 | Mitsubishi Gas Chem Co Inc | 樹脂組成物 |
-
1992
- 1992-02-07 AT AT92301065T patent/ATE141628T1/de not_active IP Right Cessation
- 1992-02-07 DE DE69212863T patent/DE69212863T2/de not_active Expired - Fee Related
- 1992-02-07 EP EP92301065A patent/EP0501625B1/en not_active Expired - Lifetime
- 1992-02-18 JP JP07942092A patent/JP3198465B2/ja not_active Expired - Fee Related
- 1992-02-24 KR KR1019920002771A patent/KR100206398B1/ko not_active Expired - Fee Related
- 1992-02-25 CA CA002061798A patent/CA2061798A1/en not_active Abandoned
- 1992-02-25 AU AU11239/92A patent/AU655627B2/en not_active Ceased
- 1992-02-25 TW TW081101403A patent/TW224981B/zh active
-
1993
- 1993-11-05 US US08/147,363 patent/US5426171A/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU446200B2 (en) * | 1968-09-05 | 1970-09-24 | Dow Corning Corporation | Reinforced polystyrene and its copolymers |
| AU612152B2 (en) * | 1987-06-12 | 1991-07-04 | E.I. Du Pont De Nemours And Company | Composites |
| AU614539B2 (en) * | 1987-09-18 | 1991-09-05 | Yvan Landler | Composite material and process for the production thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| KR100206398B1 (ko) | 1999-07-01 |
| TW224981B (enExample) | 1994-06-11 |
| KR920016557A (ko) | 1992-09-25 |
| DE69212863T2 (de) | 1997-03-06 |
| CA2061798A1 (en) | 1992-08-27 |
| JPH0586296A (ja) | 1993-04-06 |
| EP0501625A1 (en) | 1992-09-02 |
| AU1123992A (en) | 1992-08-27 |
| JP3198465B2 (ja) | 2001-08-13 |
| DE69212863D1 (de) | 1996-09-26 |
| EP0501625B1 (en) | 1996-08-21 |
| US5426171A (en) | 1995-06-20 |
| ATE141628T1 (de) | 1996-09-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK14 | Patent ceased section 143(a) (annual fees not paid) or expired |