AU2012250560B2 - Lignin production from lignocellulosic biomass - Google Patents

Lignin production from lignocellulosic biomass Download PDF

Info

Publication number
AU2012250560B2
AU2012250560B2 AU2012250560A AU2012250560A AU2012250560B2 AU 2012250560 B2 AU2012250560 B2 AU 2012250560B2 AU 2012250560 A AU2012250560 A AU 2012250560A AU 2012250560 A AU2012250560 A AU 2012250560A AU 2012250560 B2 AU2012250560 B2 AU 2012250560B2
Authority
AU
Australia
Prior art keywords
pressure
lignin
temperature
bar
lignocellulosic biomass
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
AU2012250560A
Other languages
English (en)
Other versions
AU2012250560A1 (en
Inventor
Krishnan V. IYER
Kiran KADAM
Michel A. Simard
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Renmatix Inc
Original Assignee
Renmatix Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Renmatix Inc filed Critical Renmatix Inc
Publication of AU2012250560A1 publication Critical patent/AU2012250560A1/en
Application granted granted Critical
Publication of AU2012250560B2 publication Critical patent/AU2012250560B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/16Sulfur-containing compounds
    • C04B24/18Lignin sulfonic acid or derivatives thereof, e.g. sulfite lye
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07GCOMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G1/00Lignin; Lignin derivatives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08HDERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H6/00Macromolecular compounds derived from lignin, e.g. tannins, humic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08HDERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00Macromolecular compounds derived from lignocellulosic materials
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L97/00Compositions of lignin-containing materials
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10Feedstock materials
    • C10G2300/1011Biomass
    • C10G2300/1014Biomass of vegetal origin
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/54Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00Technologies relating to oil refining and petrochemical industry
    • Y02P30/20Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Ceramic Engineering (AREA)
  • Structural Engineering (AREA)
  • Processing Of Solid Wastes (AREA)
  • Paper (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
AU2012250560A 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass Active AU2012250560B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161482425P 2011-05-04 2011-05-04
US61/482,425 2011-05-04
PCT/US2012/036566 WO2012151509A2 (en) 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass

Publications (2)

Publication Number Publication Date
AU2012250560A1 AU2012250560A1 (en) 2013-11-07
AU2012250560B2 true AU2012250560B2 (en) 2015-11-19

Family

ID=47090420

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2012250560A Active AU2012250560B2 (en) 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass

Country Status (13)

Country Link
US (2) US8317928B1 (enExample)
EP (1) EP2705074B1 (enExample)
JP (1) JP5905570B2 (enExample)
KR (1) KR101425765B1 (enExample)
CN (1) CN103502320B (enExample)
AU (1) AU2012250560B2 (enExample)
BR (1) BR112013028146A2 (enExample)
CA (1) CA2834856C (enExample)
PH (1) PH12013502197A1 (enExample)
RU (1) RU2508301C1 (enExample)
SG (1) SG194704A1 (enExample)
WO (1) WO2012151509A2 (enExample)
ZA (1) ZA201309031B (enExample)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2526225B1 (en) 2010-01-19 2019-10-02 Renmatix, Inc. Production of fermentable sugars and lignin from biomass using supercritical fluids
CA2816250C (en) 2010-11-01 2020-01-14 Reac Fuel Ab Process for controlled liquefaction of a biomass feedstock by treatment in hot compressed water
US8801859B2 (en) 2011-05-04 2014-08-12 Renmatix, Inc. Self-cleaning apparatus and method for thick slurry pressure control
JP5967730B2 (ja) * 2011-05-04 2016-08-10 レンマティックス, インコーポレイテッドRenmatix, Inc. リグノセルロース系バイオマスからのリグニンの製造
WO2013070160A1 (en) * 2011-11-08 2013-05-16 Reac Fuel Ab Liquefaction of biomass at low ph
US8759498B2 (en) 2011-12-30 2014-06-24 Renmatix, Inc. Compositions comprising lignin
FI20125362L (fi) * 2012-03-29 2013-09-30 Upm Kymmene Corp Ligniini sekä menetelmä ja järjestelmä ligniinin käsittelemiseksi
BR112014025714A8 (pt) * 2012-04-30 2018-02-06 Renmatix Inc Processo que envolve a liquefação de uma calda de biomassa por meio de tratamento em água comprimida quente (hcw)
US9222040B2 (en) * 2012-06-07 2015-12-29 General Electric Company System and method for slurry handling
US10018416B2 (en) 2012-12-04 2018-07-10 General Electric Company System and method for removal of liquid from a solids flow
CA2896791C (en) * 2013-01-25 2021-03-23 Ren Fuel K2B Ab Compositions of biomass materials for refining
US10059730B2 (en) 2013-03-15 2018-08-28 Renmatix, Inc. High purity lignin, lignin compositions, and higher structured lignin
US9255187B2 (en) * 2013-03-15 2016-02-09 Synergy Horizon Limited Method for production of dry hydrolytic lignin
KR101479676B1 (ko) * 2013-05-23 2015-01-08 씨제이제일제당 주식회사 저분자 리그닌 유도체의 제조방법
US9784121B2 (en) 2013-12-11 2017-10-10 General Electric Company System and method for continuous solids slurry depressurization
US9702372B2 (en) 2013-12-11 2017-07-11 General Electric Company System and method for continuous solids slurry depressurization
KR20170063716A (ko) 2014-09-26 2017-06-08 렌매틱스, 인코포레이티드. 다환방향족 화합물을 제조하고 수집하기 위한 방법 및 다환방향족 화합물을 포함하는 제품
SG10202003336XA (en) 2014-09-26 2020-05-28 Renmatix Inc Cellulose-containing compositions and methods of making same
RU2686832C2 (ru) 2014-11-12 2019-04-30 Ренмэтикс, Инк. Способ коалесценции вещества
FI127740B (en) 2015-05-29 2019-01-15 Upm Kymmene Corp A method and an apparatus for forming a lignin fraction, a lignin composition and its use
FI127960B (fi) * 2015-05-29 2019-06-14 Upm Kymmene Corp Menetelmä raakaligniinin pesemiseksi, liukoinen hiilihydraattia sisältävä fraktio, kiintoainefraktio ja niiden käyttö
GB2546243B (en) 2015-12-23 2018-07-11 Aerothermal Green Energy Ltd Biomass, thermal pressure hydrolysis and anaerobic digestion
BR112019017106A2 (pt) 2017-02-16 2020-04-28 Sweetwater Energy, Inc. formação de zona de alta pressão para pré-tratamento
CN111465609A (zh) * 2017-09-07 2020-07-28 瑞恩麦特克斯有限公司 聚合物中的抗氧化剂稳定剂
AU2020412611A1 (en) 2019-12-22 2022-07-14 Apalta Patents OÜ Methods of making specialized lignin and lignin products from biomass

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5041192A (en) * 1988-09-16 1991-08-20 University Of South Florida Supercritical delignification of wood
US6180845B1 (en) * 1999-10-07 2001-01-30 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Transforming biomass to hydrocarbon mixtures in near-critical or supercritical water
US20080032344A1 (en) * 2006-08-07 2008-02-07 John Allan Fallavollita Process for recovery of holocellulose and near-native lignin from biomass
US20100069626A1 (en) * 2008-07-16 2010-03-18 Sriya Innovations Nano-catalytic-solvo-thermal technology platform bio-refineries

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2156159A (en) 1938-05-17 1939-04-25 Northwood Chemical Company Process of making lignin
US2994633A (en) 1958-08-21 1961-08-01 Crossett Company Process for separating lignin solids from used neutral sulfite pulping liquors
US2997466A (en) 1958-11-04 1961-08-22 West Virginia Pulp & Paper Co Decantation of lignin
DE2737118A1 (de) 1977-08-17 1979-03-01 Projektierung Chem Verfahrenst Verfahren zur gewinnung von zuckern, gegebenenfalls cellulose und gegebenenfalls lignin aus lignocellulosischen pflanzlichen rohstoffen
CA1100266A (en) 1977-08-31 1981-05-05 Laszlo Paszner Organosolv delignification and saccharification process for lignocellulosic plant materials
US4470851A (en) 1981-03-26 1984-09-11 Laszlo Paszner High efficiency organosolv saccharification process
SU1086046A1 (ru) * 1982-07-12 1984-04-15 Ленинградская Ордена Ленина Лесотехническая Академия Им.С.М.Кирова Способ делигнификации древесины
DE3428661A1 (de) 1983-08-09 1985-03-07 Krupp Industrietechnik GmbH Werk Buckau Wolf, 4048 Grevenbroich Verfahren zur hydrolyse von lignocellulosehaltiger biomasse
CA1198703A (en) 1984-08-02 1985-12-31 Edward A. De Long Method of producing level off d p microcrystalline cellulose and glucose from lignocellulosic material
US4764596A (en) 1985-11-05 1988-08-16 Repap Technologies Inc. Recovery of lignin
CA1284637C (en) 1987-08-24 1991-06-04 George S. Faass Biomass fractionation process
DK176540B1 (da) * 2004-09-24 2008-07-21 Cambi Bioethanol Aps Fremgangsmåde til behandling af biomasse og organisk affald med henblik på at udvinde önskede biologisk baserede produkter
JP2006255676A (ja) 2005-03-18 2006-09-28 Kri Inc リグニン物質分離方法
JP2006288676A (ja) * 2005-04-11 2006-10-26 Takahiko Katayama 飲料入り容器の陳列方法
CA2615844C (en) * 2005-07-19 2015-04-21 Holm Christensen Biosystemer Aps Method and apparatus for conversion of cellulosic material to ethanol
CA2631021A1 (en) 2005-11-23 2007-10-25 Natureworks Llc Process for fractionating lignocellulosic biomass into liquid and solid products
US8784566B2 (en) * 2006-03-29 2014-07-22 Virginia Tech Intellectual Properties, Inc. Cellulose-solvent-based lignocellulose fractionation with modest reaction conditions and reagent cycling
RU2338769C1 (ru) * 2007-05-22 2008-11-20 Институт физической химии и электрохимии им. А.Н. Фрумкина Российской академии наук Способ переработки растительного сырья
US8613781B2 (en) 2007-08-08 2013-12-24 Harrison R. Cooper Lignin dewatering process
US8282738B2 (en) * 2008-07-16 2012-10-09 Renmatix, Inc. Solvo-thermal fractionation of biomass
JP5339341B2 (ja) * 2008-08-13 2013-11-13 宜章 大木 亜臨界状態による木材の繊維を線維固形分としての分離方法
JP5410060B2 (ja) * 2008-10-02 2014-02-05 株式会社Kri イオン液体によるリグノセルロース系バイオマスのセルロースとリグニンの分離化方法
KR101657100B1 (ko) * 2008-10-29 2016-09-19 삼성전자주식회사 리그노셀룰로오스계 바이오매스의 분별방법 및 분별장치
SI2421911T1 (sl) 2009-04-23 2014-10-30 Greenfield Ethanol Inc. Ločevanje reaktivne celuloze od lignocelulozne biomase z visoko vsebnostjo lignina
AU2009349861B2 (en) * 2009-07-13 2015-06-25 Versalis S.P.A. High temperature lignin separation process
CN101974161B (zh) * 2010-09-30 2012-10-31 中国科学院西双版纳热带植物园 一种溶解和快速水解木质纤维素生物质的方法及其设备和应用

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5041192A (en) * 1988-09-16 1991-08-20 University Of South Florida Supercritical delignification of wood
US6180845B1 (en) * 1999-10-07 2001-01-30 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Transforming biomass to hydrocarbon mixtures in near-critical or supercritical water
US20080032344A1 (en) * 2006-08-07 2008-02-07 John Allan Fallavollita Process for recovery of holocellulose and near-native lignin from biomass
US20100069626A1 (en) * 2008-07-16 2010-03-18 Sriya Innovations Nano-catalytic-solvo-thermal technology platform bio-refineries

Also Published As

Publication number Publication date
US8317928B1 (en) 2012-11-27
BR112013028146A2 (pt) 2017-04-25
WO2012151509A2 (en) 2012-11-08
US20120282466A1 (en) 2012-11-08
ZA201309031B (en) 2015-03-25
JP2014513740A (ja) 2014-06-05
PH12013502197A1 (en) 2014-01-13
US20120282467A1 (en) 2012-11-08
JP5905570B2 (ja) 2016-04-20
EP2705074A2 (en) 2014-03-12
WO2012151509A3 (en) 2013-03-21
CA2834856C (en) 2020-04-07
CN103502320B (zh) 2016-03-30
CN103502320A (zh) 2014-01-08
US8404051B2 (en) 2013-03-26
AU2012250560A1 (en) 2013-11-07
KR20140027376A (ko) 2014-03-06
NZ616924A (en) 2015-10-30
EP2705074A4 (en) 2014-12-03
RU2508301C1 (ru) 2014-02-27
CA2834856A1 (en) 2012-11-08
KR101425765B1 (ko) 2014-08-01
SG194704A1 (en) 2013-12-30
EP2705074B1 (en) 2017-11-01

Similar Documents

Publication Publication Date Title
AU2012250560B2 (en) Lignin production from lignocellulosic biomass
US9624449B2 (en) Biorefinery process for extraction, separation and recovery of fermentable saccharides, other useful compounds, and yield of improved lignocellulosic material from plant biomass
US10150920B2 (en) Process for producing liquid hydrocarbon
US9777223B2 (en) Process and apparatus for producing liquid hydrocarbon
US12043854B2 (en) Processes for reducing steam consumption and improving process carbon balance in biomass conversion to sugars, biochemicals, biofuels, and/or biomaterials
EP3265196A1 (en) Methods and systems for post-fermentation lignin recovery
NZ616924B2 (en) Lignin production from lignocellulosic biomass
US20240301455A1 (en) Methods and systems for optimized feeding of lignocellulosic biomass in the production of sugars, biochemicals, biofuels, and/or biomaterials

Legal Events

Date Code Title Description
FGA Letters patent sealed or granted (standard patent)