ATE432766T1 - Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid - Google Patents

Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid

Info

Publication number
ATE432766T1
ATE432766T1 AT06841526T AT06841526T ATE432766T1 AT E432766 T1 ATE432766 T1 AT E432766T1 AT 06841526 T AT06841526 T AT 06841526T AT 06841526 T AT06841526 T AT 06841526T AT E432766 T1 ATE432766 T1 AT E432766T1
Authority
AT
Austria
Prior art keywords
conditions
purification
concentration
reacting
ethylene oxide
Prior art date
Application number
AT06841526T
Other languages
English (en)
Inventor
Dominicus Maria Rekers
Mathias Jozef Paul Slapak
Original Assignee
Shell Int Research
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Int Research filed Critical Shell Int Research
Application granted granted Critical
Publication of ATE432766T1 publication Critical patent/ATE432766T1/de

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093Microreactors, e.g. miniaturised or microfabricated reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B81MICROSTRUCTURAL TECHNOLOGY
    • B81BMICROSTRUCTURAL DEVICES OR SYSTEMS, e.g. MICROMECHANICAL DEVICES
    • B81B7/00Microstructural systems; Auxiliary parts of microstructural devices or systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00783Laminate assemblies, i.e. the reactor comprising a stack of plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00822Metal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00831Glass
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00833Plastic
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00835Comprising catalytically active material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00858Aspects relating to the size of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00858Aspects relating to the size of the reactor
    • B01J2219/0086Dimensions of the flow channels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00867Microreactors placed in series, on the same or on different supports
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00869Microreactors placed in parallel, on the same or on different supports
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00871Modular assembly
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00873Heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00905Separation
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23CMETHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN  A CARRIER GAS OR AIR 
    • F23C2900/00Special features of, or arrangements for combustion apparatus using fluid fuels or solid fuels suspended in air; Combustion processes therefor
    • F23C2900/03001Miniaturized combustion devices using fluid fuels

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Epoxy Compounds (AREA)
  • Incineration Of Waste (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Treatments Of Macromolecular Shaped Articles (AREA)
AT06841526T 2005-12-22 2006-12-20 Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid ATE432766T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP05257995 2005-12-22
PCT/EP2006/070030 WO2007071739A1 (en) 2005-12-22 2006-12-20 Microchannel apparatus for unit operations following ethylene oxide production

Publications (1)

Publication Number Publication Date
ATE432766T1 true ATE432766T1 (de) 2009-06-15

Family

ID=37898787

Family Applications (1)

Application Number Title Priority Date Filing Date
AT06841526T ATE432766T1 (de) 2005-12-22 2006-12-20 Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid

Country Status (10)

Country Link
EP (4) EP1976625B1 (de)
JP (4) JP2009520762A (de)
KR (4) KR20080080372A (de)
CN (4) CN101384352A (de)
AT (1) ATE432766T1 (de)
CA (4) CA2634417A1 (de)
DE (1) DE602006007180D1 (de)
EA (2) EA200870100A1 (de)
TW (4) TW200740519A (de)
WO (4) WO2007071741A1 (de)

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US7294734B2 (en) 2003-05-02 2007-11-13 Velocys, Inc. Process for converting a hydrocarbon to an oxygenate or a nitrile
CN101023068B (zh) 2004-08-12 2013-02-13 万罗赛斯公司 使用微通道工艺技术将乙烯转化成环氧乙烷的方法
US7750170B2 (en) 2005-12-22 2010-07-06 Shell Oil Company Process for mixing an oxidant having explosive potential with a hydrocarbon
US8100996B2 (en) 2008-04-09 2012-01-24 Velocys, Inc. Process for upgrading a carbonaceous material using microchannel process technology
US9908093B2 (en) 2008-04-09 2018-03-06 Velocys, Inc. Process for converting a carbonaceous material to methane, methanol and/or dimethyl ether using microchannel process technology
WO2010009021A2 (en) * 2008-07-14 2010-01-21 Velocys Inc. Process for making ethylene oxide using microchannel process technology
EP2300447A1 (de) 2008-07-14 2011-03-30 Basf Se Verfahren zur herstellung von ethylenoxid
CA2739325C (en) 2008-10-10 2018-11-27 Velocys Inc. Process and apparatus employing microchannel process technology
EP2223741A1 (de) * 2009-02-13 2010-09-01 Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO Mikrofluidisches System mit einem Stapel von Verfahrensmodulen und Wärmetauschermodule
US8524927B2 (en) 2009-07-13 2013-09-03 Velocys, Inc. Process for making ethylene oxide using microchannel process technology
US8968695B2 (en) * 2009-08-10 2015-03-03 Idt International Co., Ltd. Method of producing nano-size graphene-based material and an equipment for producing the same
TWI493141B (zh) * 2010-03-29 2015-07-21 Guan Bang Chen 微管路之觸媒燃燒器
US9676623B2 (en) 2013-03-14 2017-06-13 Velocys, Inc. Process and apparatus for conducting simultaneous endothermic and exothermic reactions
CN103386334A (zh) * 2013-08-07 2013-11-13 苏州扬清芯片科技有限公司 一种微流控芯片的制冷方法
DE102015111614A1 (de) * 2015-07-17 2017-01-19 Karlsruher Institut für Technologie Mikrostrukturreaktor zur Durchführung exothermer, heterogen katalysierter Reaktionen mit effizienter Verdampfungskühlung
CN106316783A (zh) * 2016-08-23 2017-01-11 张英 一种1,2‑己二醇的气液管道式制备方法
JP6732672B2 (ja) * 2017-02-03 2020-07-29 株式会社ガスター 浴湯熱暖房システム
JP6838983B2 (ja) * 2017-02-03 2021-03-03 株式会社ガスター 放熱ユニット 暖房システム
EP3770145A1 (de) 2019-07-24 2021-01-27 Basf Se Verfahren zur kontinuierlichen herstellung von acrolein oder acrylsäure als zielprodukt aus propen

Family Cites Families (21)

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US4760200A (en) * 1985-12-31 1988-07-26 Union Carbide Corporation Process for the production of alkylene glycols
US6126723A (en) * 1994-07-29 2000-10-03 Battelle Memorial Institute Microcomponent assembly for efficient contacting of fluid
US5811062A (en) * 1994-07-29 1998-09-22 Battelle Memorial Institute Microcomponent chemical process sheet architecture
US5914091A (en) * 1996-02-15 1999-06-22 Atmi Ecosys Corp. Point-of-use catalytic oxidation apparatus and method for treatment of voc-containing gas streams
US6616909B1 (en) * 1998-07-27 2003-09-09 Battelle Memorial Institute Method and apparatus for obtaining enhanced production rate of thermal chemical reactions
US6875247B2 (en) * 2000-06-06 2005-04-05 Battelle Memorial Institute Conditions for fluid separations in microchannels, capillary-driven fluid separations, and laminated devices capable of separating fluids
CA2446503C (en) * 2001-04-30 2009-11-24 Battelle Memorial Institute Apparatus and method for separation/purification of fluids utilizing rapidly cycled thermal swing
US6713036B1 (en) * 2001-05-07 2004-03-30 Uop Llc Process for mixing and reacting two or more fluids
US7014835B2 (en) * 2002-08-15 2006-03-21 Velocys, Inc. Multi-stream microchannel device
US6652627B1 (en) * 2002-10-30 2003-11-25 Velocys, Inc. Process for separating a fluid component from a fluid mixture using microchannel process technology
US7294734B2 (en) * 2003-05-02 2007-11-13 Velocys, Inc. Process for converting a hydrocarbon to an oxygenate or a nitrile
DE602004009681T2 (de) * 2003-05-16 2008-08-14 Velocys, Inc., Plain City Verfahren zur erzeugung einer emulsion durch verwendung einer mikrokanalverfahrentechnologie
AU2004241941B2 (en) * 2003-05-16 2010-05-13 Velocys Inc. Oxidation process using microchannel technology and novel catalyst useful in same
US7470408B2 (en) * 2003-12-18 2008-12-30 Velocys In situ mixing in microchannels
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Also Published As

Publication number Publication date
JP2009520767A (ja) 2009-05-28
WO2007071737A1 (en) 2007-06-28
EP1979087A1 (de) 2008-10-15
CA2634366A1 (en) 2007-06-28
WO2007071744A1 (en) 2007-06-28
CN101384349A (zh) 2009-03-11
WO2007071741A1 (en) 2007-06-28
CA2634440A1 (en) 2007-06-28
EA200870101A1 (ru) 2008-12-30
TW200740518A (en) 2007-11-01
EP1976625B1 (de) 2009-06-03
KR20080080182A (ko) 2008-09-02
DE602006007180D1 (de) 2009-07-16
EP1981632A1 (de) 2008-10-22
JP2009520764A (ja) 2009-05-28
JP2009520762A (ja) 2009-05-28
CN101384351A (zh) 2009-03-11
CA2634417A1 (en) 2007-06-28
CN101384350A (zh) 2009-03-11
KR20080080372A (ko) 2008-09-03
KR20080080183A (ko) 2008-09-02
CN101384352A (zh) 2009-03-11
EP1976625A1 (de) 2008-10-08
TW200735958A (en) 2007-10-01
CA2634409A1 (en) 2007-06-28
JP2009520943A (ja) 2009-05-28
EA200870100A1 (ru) 2008-12-30
WO2007071739A1 (en) 2007-06-28
KR20080080184A (ko) 2008-09-02
TW200740519A (en) 2007-11-01
TW200803973A (en) 2008-01-16
EP1973645A1 (de) 2008-10-01

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