ATE342758T1 - Druckwechseladsorptionsverfahren zur wasserstoffreinigung - Google Patents

Druckwechseladsorptionsverfahren zur wasserstoffreinigung

Info

Publication number
ATE342758T1
ATE342758T1 AT98400075T AT98400075T ATE342758T1 AT E342758 T1 ATE342758 T1 AT E342758T1 AT 98400075 T AT98400075 T AT 98400075T AT 98400075 T AT98400075 T AT 98400075T AT E342758 T1 ATE342758 T1 AT E342758T1
Authority
AT
Austria
Prior art keywords
swing adsorption
pressure swing
adsorption process
hydrogen purification
lithium
Prior art date
Application number
AT98400075T
Other languages
English (en)
Inventor
Dominique Plee
Original Assignee
Ceca Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ceca Sa filed Critical Ceca Sa
Application granted granted Critical
Publication of ATE342758T1 publication Critical patent/ATE342758T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B01J20/186—Chemical treatments in view of modifying the properties of the sieve, e.g. increasing the stability or the activity, also decreasing the activity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B01D2253/1085—Zeolites characterized by a silicon-aluminium ratio
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/102—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/502—Carbon monoxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S95/00—Gas separation: processes
    • Y10S95/90—Solid sorbent
    • Y10S95/902—Molecular sieve

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
AT98400075T 1997-01-24 1998-01-16 Druckwechseladsorptionsverfahren zur wasserstoffreinigung ATE342758T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9700784A FR2758739B1 (fr) 1997-01-24 1997-01-24 Perfectionnement dans les procedes psa de purification de l'hydrogene

Publications (1)

Publication Number Publication Date
ATE342758T1 true ATE342758T1 (de) 2006-11-15

Family

ID=9502956

Family Applications (1)

Application Number Title Priority Date Filing Date
AT98400075T ATE342758T1 (de) 1997-01-24 1998-01-16 Druckwechseladsorptionsverfahren zur wasserstoffreinigung

Country Status (10)

Country Link
US (1) US6464756B1 (de)
EP (1) EP0855209B1 (de)
JP (1) JP4382885B2 (de)
AT (1) ATE342758T1 (de)
CA (1) CA2224945C (de)
DE (1) DE69836159T2 (de)
DK (1) DK0855209T3 (de)
ES (1) ES2276451T3 (de)
FR (1) FR2758739B1 (de)
PT (1) PT855209E (de)

Families Citing this family (42)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2782461B1 (fr) 1998-08-21 2000-09-22 Air Liquide Procede psa utilisant une zeolithe faujasite contenant des cations metalliques en tant qu'adsorbant
FR2782507B1 (fr) * 1998-08-21 2000-09-29 Air Liquide Procede de fabrication de particules de zeolite x echangee par des cations metalliques
FR2782460B1 (fr) * 1998-08-21 2000-09-22 Air Liquide Procede psa utilisant un adsorbant agglomere constitue d'une phase zeolitique et d'un liant
FR2783439B1 (fr) * 1998-09-23 2000-10-20 Air Liquide Particules d'adsorbant ellipsoidales et leur utilisation dans un procede de production de gaz
US6302943B1 (en) 1999-11-02 2001-10-16 Air Products And Chemicals, Inc. Optimum adsorbents for H2 recovery by pressure and vacuum swing absorption
DE60129626T2 (de) 2000-04-20 2008-05-21 Tosoh Corp., Shinnanyo Verfahren zum Reinigen von einem Wasserstoff enthaltenden Gasgemisch
JP2000202281A (ja) * 2000-04-20 2000-07-25 Air Water Inc 選択的窒素吸着剤およびそれを用いた空気分離方法
FR2811241B1 (fr) * 2000-07-07 2002-12-13 Ceca Sa Procede pour la purification de melanges gazeux a base d'hydrogene utilisant une zeolite x au calcium
US6596256B1 (en) * 2000-08-28 2003-07-22 The Boc Group, Inc. Synthesis of low silicon sodium X zeolite
CA2432909C (en) 2000-12-25 2007-01-23 Sumitomo Seika Chemicals Co., Ltd. Method for separating hydrogen gas
FR2832077B1 (fr) * 2001-11-12 2004-08-27 Air Liquide Adsorbant zeolitique au baryum et calcium pour la purification de gaz, en particulier de l'air
FR2832141B1 (fr) * 2001-11-14 2004-10-01 Ceca Sa Procede de purification de gaz de synthese
FR2835445B1 (fr) 2002-02-07 2004-11-19 Air Liquide Utilisation d'un adsorbant sous forme de mousse solide pour la purification ou la separation de gaz
US6605136B1 (en) * 2002-07-10 2003-08-12 Air Products And Chemicals, Inc. Pressure swing adsorption process operation and optimization
US7175751B2 (en) * 2003-05-01 2007-02-13 Ovonic Fuel Cell Company Llc Method and apparatus for electrorefining impure hydrogen
CN1315563C (zh) * 2003-06-06 2007-05-16 四川天一科技股份有限公司 从混合气体中脱除乙烯、二氧化碳的吸附分离法
US7404846B2 (en) 2005-04-26 2008-07-29 Air Products And Chemicals, Inc. Adsorbents for rapid cycle pressure swing adsorption processes
US20080011163A1 (en) * 2006-07-17 2008-01-17 Mcclain Michael S Sorbent porous polymeric composite materials
KR100896455B1 (ko) * 2007-07-09 2009-05-14 한국에너지기술연구원 압력변동흡착장치 및 이를 이용한 수소 정제 방법
WO2010102038A1 (en) 2009-03-04 2010-09-10 Xerox Corporation Electronic devices comprising structured organic films
JP2011032128A (ja) * 2009-07-31 2011-02-17 Jx Nippon Oil & Energy Corp 水素の精製方法、水素の出荷設備、及び水素ステーション
US9567425B2 (en) 2010-06-15 2017-02-14 Xerox Corporation Periodic structured organic films
US8697322B2 (en) 2010-07-28 2014-04-15 Xerox Corporation Imaging members comprising structured organic films
US8257889B2 (en) 2010-07-28 2012-09-04 Xerox Corporation Imaging members comprising capped structured organic film compositions
US8318892B2 (en) 2010-07-28 2012-11-27 Xerox Corporation Capped structured organic film compositions
US8119315B1 (en) 2010-08-12 2012-02-21 Xerox Corporation Imaging members for ink-based digital printing comprising structured organic films
US8119314B1 (en) 2010-08-12 2012-02-21 Xerox Corporation Imaging devices comprising structured organic films
US8759473B2 (en) 2011-03-08 2014-06-24 Xerox Corporation High mobility periodic structured organic films
US8353574B1 (en) 2011-06-30 2013-01-15 Xerox Corporation Ink jet faceplate coatings comprising structured organic films
US8247142B1 (en) 2011-06-30 2012-08-21 Xerox Corporation Fluorinated structured organic film compositions
US8313560B1 (en) 2011-07-13 2012-11-20 Xerox Corporation Application of porous structured organic films for gas separation
US8377999B2 (en) 2011-07-13 2013-02-19 Xerox Corporation Porous structured organic film compositions
US8410016B2 (en) 2011-07-13 2013-04-02 Xerox Corporation Application of porous structured organic films for gas storage
US8372566B1 (en) 2011-09-27 2013-02-12 Xerox Corporation Fluorinated structured organic film photoreceptor layers
US8460844B2 (en) 2011-09-27 2013-06-11 Xerox Corporation Robust photoreceptor surface layer
US8529997B2 (en) 2012-01-17 2013-09-10 Xerox Corporation Methods for preparing structured organic film micro-features by inkjet printing
US8765340B2 (en) 2012-08-10 2014-07-01 Xerox Corporation Fluorinated structured organic film photoreceptor layers containing fluorinated secondary components
US8906462B2 (en) 2013-03-14 2014-12-09 Xerox Corporation Melt formulation process for preparing structured organic films
JP6331937B2 (ja) * 2014-10-01 2018-05-30 日本ポリプロ株式会社 オレフィン重合体の製造方法
CN107486146B (zh) * 2017-09-06 2020-10-23 洛阳建龙微纳新材料股份有限公司 一种混合阳离子LiCa-LSX分子筛制法及应用
FR3076828A1 (fr) 2018-01-15 2019-07-19 Arkema France Procede de preparation de zeolithes en continu au moyen d'ultrasons
CN112758892B (zh) * 2021-01-05 2021-12-17 西南化工研究设计院有限公司 一种变压吸附提纯氢气系统及其方法

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3839847A (en) * 1972-07-05 1974-10-08 Hydrocarbon Research Inc Cryogenic hydrogen adsorption system
DE2729558C3 (de) * 1977-06-30 1983-12-08 Bergwerksverband Gmbh, 4300 Essen Adsorptions/Desorptionsverfahren zur Gewinnung von Wasserstoff
USRE31014E (en) * 1981-03-30 1982-08-17 Air Products And Chemicals, Inc. Separation of multicomponent gas mixtures
DE3143993A1 (de) * 1981-11-05 1983-05-11 Bayer Ag, 5090 Leverkusen Molekularsieb-zeolith fuer die gewinnung von wasserstoff mit der druckwechsel-adsorptions-technik
JPS60103002A (ja) * 1983-11-01 1985-06-07 Kawasaki Steel Corp 吸着法を使用して一酸化炭素、二酸化炭素、水素及び窒素ガスを含む混合ガス中の一酸化炭素及び水素を精製する方法
JPS60139337A (ja) * 1983-12-27 1985-07-24 Toyo Soda Mfg Co Ltd 一酸化炭素吸着剤
JPS61247612A (ja) * 1985-04-23 1986-11-04 Mitsubishi Heavy Ind Ltd Ｃｏ吸着分離方法
US4859217A (en) * 1987-06-30 1989-08-22 Uop Process for separating nitrogen from mixtures thereof with less polar substances
JPH0779940B2 (ja) * 1987-09-16 1995-08-30 日本酸素株式会社 吸着分離法
JPH07166B2 (ja) * 1987-09-24 1995-01-11 三菱重工業株式会社 Ｃｏ吸着分離方法
US5234472A (en) * 1987-11-16 1993-08-10 The Boc Group Plc Separation of gas mixtures including hydrogen
US4943304A (en) * 1989-04-06 1990-07-24 Air Products And Chemicals, Inc. Process for the purification of bulk gases using chabazite adsorbents
US5174979A (en) * 1989-10-06 1992-12-29 Uop Mixed ion-exchanged zeolites and processes for the use thereof in gas separations
US5220797A (en) * 1990-09-28 1993-06-22 The Boc Group, Inc. Argon recovery from argon-oxygen-decarburization process waste gases
US5133785A (en) * 1991-02-26 1992-07-28 Air Products And Chemicals, Inc. Separation of multicomponent gas mixtures by selective adsorption
US5152813A (en) * 1991-12-20 1992-10-06 Air Products And Chemicals, Inc. Nitrogen adsorption with a Ca and/or Sr exchanged lithium X-zeolite
US5266102A (en) * 1992-09-23 1993-11-30 Air Products And Chemicals, Inc. O2 VSA process with low O2 capacity adsorbents
US5258060A (en) * 1992-09-23 1993-11-02 Air Products And Chemicals, Inc. Adsorptive separation using diluted adsorptive phase
US5551257A (en) * 1992-10-01 1996-09-03 The Boc Group, Inc. Production of ultrahigh purity nitrogen
US5268023A (en) * 1992-10-05 1993-12-07 Air Products And Chemicals, Inc. Nitrogen adsorption with highly Li exchanged X-zeolites with low Si/Al ratio
US5464467A (en) * 1994-02-14 1995-11-07 The Boc Group, Inc. Adsorptive separation of nitrogen from other gases
IL112027A (en) * 1994-02-14 1999-03-12 Boc Group Inc A method for separating nitrogen from other gases
JP3462560B2 (ja) * 1994-03-04 2003-11-05 日本パイオニクス株式会社 水素ガスの精製方法
US5573745A (en) * 1994-05-12 1996-11-12 Air Products And Chemicals, Inc. High micropore volume low silica EMT-containing metallosilicates
US5616170A (en) * 1995-08-11 1997-04-01 The Boc Group, Inc. Adsorptive separation of nitrogen from other gases
US5674311A (en) * 1995-10-20 1997-10-07 Praxair Technology, Inc. Adsorption process and system using multilayer adsorbent beds

Also Published As

Publication number Publication date
JPH10212103A (ja) 1998-08-11
FR2758739B1 (fr) 1999-02-26
DE69836159T2 (de) 2007-11-29
CA2224945A1 (fr) 1998-07-24
ES2276451T3 (es) 2007-06-16
PT855209E (pt) 2007-02-28
FR2758739A1 (fr) 1998-07-31
DK0855209T3 (da) 2007-02-19
DE69836159D1 (de) 2006-11-30
US6464756B1 (en) 2002-10-15
JP4382885B2 (ja) 2009-12-16
EP0855209A1 (de) 1998-07-29
EP0855209B1 (de) 2006-10-18
CA2224945C (fr) 2006-06-20

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