ATE107535T1 - Gaschromatographische methode zur trennung von wasserstoffisotopen. - Google Patents
Gaschromatographische methode zur trennung von wasserstoffisotopen.Info
- Publication number
- ATE107535T1 ATE107535T1 AT87302742T AT87302742T ATE107535T1 AT E107535 T1 ATE107535 T1 AT E107535T1 AT 87302742 T AT87302742 T AT 87302742T AT 87302742 T AT87302742 T AT 87302742T AT E107535 T1 ATE107535 T1 AT E107535T1
- Authority
- AT
- Austria
- Prior art keywords
- hydrogen
- isotops
- separation
- gas chromatographic
- chromatographic method
- Prior art date
Links
- 239000007789 gas Substances 0.000 title abstract 2
- 239000001257 hydrogen Substances 0.000 title abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 title abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title 1
- 238000004587 chromatography analysis Methods 0.000 title 1
- 238000000926 separation method Methods 0.000 title 1
- 230000000155 isotopic effect Effects 0.000 abstract 2
- 238000004440 column chromatography Methods 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002808 molecular sieve Substances 0.000 abstract 1
- 238000012856 packing Methods 0.000 abstract 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D59/00—Separation of different isotopes of the same chemical element
- B01D59/22—Separation by extracting
- B01D59/24—Separation by extracting by solvent extraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D59/00—Separation of different isotopes of the same chemical element
- B01D59/22—Separation by extracting
- B01D59/26—Separation by extracting by sorption, i.e. absorption, adsorption, persorption
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B4/00—Hydrogen isotopes; Inorganic compounds thereof prepared by isotope exchange, e.g. NH3 + D2 → NH2D + HD
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/025—Gas chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/3007—Control of physical parameters of the fluid carrier of temperature same temperature for whole column
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/3023—Control of physical parameters of the fluid carrier of temperature using cryogenic fluids
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/3084—Control of physical parameters of the fluid carrier of temperature ovens
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/16—Injection
- G01N30/20—Injection using a sampling valve
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Biochemistry (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Hydrogen, Water And Hydrids (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/861,336 US4732581A (en) | 1986-05-08 | 1986-05-08 | Gas chromatographic method for separating hydrogen isotopes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE107535T1 true ATE107535T1 (de) | 1994-07-15 |
Family
ID=25335525
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT87302742T ATE107535T1 (de) | 1986-05-08 | 1987-03-30 | Gaschromatographische methode zur trennung von wasserstoffisotopen. |
| AT91120674T ATE113861T1 (de) | 1986-05-08 | 1987-03-30 | Gaschromatographische methode zur trennung von wasserstoffisotopen. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT91120674T ATE113861T1 (de) | 1986-05-08 | 1987-03-30 | Gaschromatographische methode zur trennung von wasserstoffisotopen. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4732581A (enExample) |
| EP (2) | EP0486070B1 (enExample) |
| JP (1) | JPS6312329A (enExample) |
| AT (2) | ATE107535T1 (enExample) |
| CA (1) | CA1271142A (enExample) |
| DE (2) | DE3750100T2 (enExample) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3717456C1 (de) * | 1987-05-23 | 1988-07-21 | Eberhard Gerstel | Gaschromatograph und Verfahren zur gaschromatographischen Trennung |
| LU86902A1 (fr) * | 1987-05-27 | 1988-06-13 | Euratom | Procede et dispositif de purification d'un gaz contenant des isotopes d'hydrogene |
| US4780116A (en) * | 1987-11-20 | 1988-10-25 | Cheh Christopher H | Low temperature preparative gas chromatography apparatus |
| US4992083A (en) * | 1988-11-19 | 1991-02-12 | Kernforschungsanlage Juelich Gesellschaft Mit Beschrenkter Haftung | Apparatus for intermediate enrichment of trace substances from a gas stream in a cold trap, and chromatography arrangement provided therewith |
| US4994096A (en) * | 1989-05-09 | 1991-02-19 | Hewlett-Packard Co. | Gas chromatograph having integrated pressure programmer |
| US4948389A (en) * | 1989-05-22 | 1990-08-14 | Hewlett-Packard Company | Gas chromatograph having cyro blast coolings |
| US5032151A (en) * | 1990-01-17 | 1991-07-16 | Hewlett-Packard Company | System and method for automated cool on-column injection with column diameters less than 530 μm |
| US5083450A (en) * | 1990-05-18 | 1992-01-28 | Martin Marietta Energy Systems, Inc. | Gas chromatograph-mass spectrometer (gc/ms) system for quantitative analysis of reactive chemical compounds |
| EP0576715A1 (en) * | 1992-07-03 | 1994-01-05 | European Atomic Energy Community (Euratom) | A method for purifying a stream of hydrogen isotopes from impurities |
| US5319955A (en) * | 1992-08-21 | 1994-06-14 | United States Department Of Energy | Tritium monitor |
| CA2110343C (en) * | 1992-12-14 | 1999-08-24 | Christopher Huk-Shi Cheh | Gas chromatographic method |
| US5637787A (en) * | 1994-05-31 | 1997-06-10 | Shimadzu Corporation | Gas chromatograph |
| JP3424432B2 (ja) * | 1996-04-03 | 2003-07-07 | 株式会社島津製作所 | ガスクロマトグラフ装置 |
| CN1192235C (zh) * | 2000-06-20 | 2005-03-09 | 科学技术振兴事业团 | 氢离子的分离方法和分析方法以及离子层析装置 |
| JP2002035528A (ja) * | 2000-07-26 | 2002-02-05 | Japan Atom Energy Res Inst | ガス分離装置 |
| US6514316B1 (en) * | 2001-08-22 | 2003-02-04 | Mt Systems, Llc | System for improving the maximum operating temperature and lifetime of chromatographic columns |
| NO319447B1 (no) * | 2002-07-05 | 2005-08-15 | Scatec As | Fremgangsmate for separasjon av isotoper |
| JP2005211757A (ja) * | 2004-01-28 | 2005-08-11 | National Institutes Of Natural Sciences | 水素同位体の分離方法、及び水素同位体の分離装置 |
| DE602005001927T2 (de) * | 2005-02-25 | 2008-04-10 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Gaschromatographievorrichtung |
| CN102553439B (zh) * | 2010-12-14 | 2014-12-10 | 中国科学院金属研究所 | 一种热致循环吸附法氢同位素分离用色谱柱及其制备 |
| CN102921191A (zh) * | 2011-09-27 | 2013-02-13 | 哈尔滨工业大学 | 一种多通路逆流分级高效分离纯化系统及其使用方法 |
| GB2586100B (en) * | 2012-07-06 | 2021-04-28 | Waters Technologies Corp | Techniques for thermally insulating a liquid chromatographic column |
| US11185795B2 (en) | 2012-07-06 | 2021-11-30 | Waters Technologies Corporation | Techniques for thermally insulating a chromatographic column |
| CN106693704B (zh) * | 2017-02-15 | 2019-06-04 | 中国工程物理研究院材料研究所 | 一种置换色谱氢同位素富集分离方法 |
| CN106693703B (zh) * | 2017-02-15 | 2018-01-02 | 中国工程物理研究院材料研究所 | 一种置换色谱氢同位素分离装置 |
| CN107051205B (zh) * | 2017-02-15 | 2019-02-12 | 中国工程物理研究院材料研究所 | 一种低温钯置换分离方法 |
| CN107930400A (zh) * | 2017-12-07 | 2018-04-20 | 中国工程物理研究院核物理与化学研究所 | 一种氢氦分离与氢同位素浓缩耦合系统及方法 |
| WO2019157297A1 (en) * | 2018-02-08 | 2019-08-15 | Wiederin Daniel R | Inline dilution and autocalibration for icp-ms speciation analysis |
| CN112986447A (zh) * | 2021-04-23 | 2021-06-18 | 中国原子能科学研究院 | 气相色谱分析装置 |
| CN114544807B (zh) * | 2022-02-15 | 2023-06-23 | 中国工程物理研究院材料研究所 | 一种氢同位素气体中杂质分析装置及方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3043127A (en) * | 1958-12-11 | 1962-07-10 | Phillips Petroleum Co | Thermochromatography heater |
| US3011589A (en) * | 1960-03-21 | 1961-12-05 | Mark Chemical Company Inc Van | Method for producing exceptionally pure hydrogen |
| DE1241416B (de) * | 1964-05-30 | 1967-06-01 | Kernforschung Gmbh Ges Fuer | Einrichtung zum Trennen von Isotopen |
| FR1478542A (fr) * | 1966-03-14 | 1967-04-28 | Rech S Tech Et Ind Soc D | Procédé de séparation continue des isotopes de l'hydrogène d'un mélange gazeux par adsorption à contre-courant |
| US3524305A (en) * | 1967-12-26 | 1970-08-18 | Phillips Petroleum Co | Minimizing switching transients in multiple column chromatography |
| US3488921A (en) * | 1968-01-16 | 1970-01-13 | Aquitaine Petrole | Process and apparatus for isotopic enrichment |
| US3769776A (en) * | 1972-02-22 | 1973-11-06 | Atomenergi Inst For | Method for thermal activation of a surface active material |
| US3843518A (en) * | 1972-08-23 | 1974-10-22 | Exxon Research Engineering Co | Commercial chromatography for more than two components |
| IT1097473B (it) * | 1978-07-05 | 1985-08-31 | Agip Nucleare Spa | Metodo per aumentare l'efficienza di produzione in processi di separazione isotopica |
| US4276060A (en) * | 1979-05-22 | 1981-06-30 | The United States Of America As Represented By The United States Department Of Energy | Chromatographic hydrogen isotope separation |
| US4271697A (en) * | 1979-10-17 | 1981-06-09 | Phillips Petroleum Company | Chromatographic analysis |
| DE3365226D1 (en) * | 1982-03-10 | 1986-09-18 | Hitachi Ltd | Gas chromatographic apparatus |
| EP0189607B1 (en) * | 1985-02-01 | 1990-05-23 | European Atomic Energy Community (Euratom) | Method for the separation of hydrogen isotopes |
-
1986
- 1986-05-08 US US06/861,336 patent/US4732581A/en not_active Expired - Lifetime
-
1987
- 1987-02-25 CA CA000530553A patent/CA1271142A/en not_active Expired
- 1987-03-30 DE DE3750100T patent/DE3750100T2/de not_active Expired - Fee Related
- 1987-03-30 EP EP91120674A patent/EP0486070B1/en not_active Expired - Lifetime
- 1987-03-30 AT AT87302742T patent/ATE107535T1/de not_active IP Right Cessation
- 1987-03-30 DE DE3750751T patent/DE3750751T2/de not_active Expired - Fee Related
- 1987-03-30 EP EP87302742A patent/EP0245936B1/en not_active Expired - Lifetime
- 1987-03-30 AT AT91120674T patent/ATE113861T1/de not_active IP Right Cessation
- 1987-04-21 JP JP62096356A patent/JPS6312329A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| EP0486070A1 (en) | 1992-05-20 |
| ATE113861T1 (de) | 1994-11-15 |
| DE3750100D1 (de) | 1994-07-28 |
| EP0245936A3 (en) | 1990-05-02 |
| CA1271142A (en) | 1990-07-03 |
| DE3750751T2 (de) | 1995-03-16 |
| JPH0412167B2 (enExample) | 1992-03-03 |
| DE3750751D1 (de) | 1994-12-15 |
| EP0245936A2 (en) | 1987-11-19 |
| JPS6312329A (ja) | 1988-01-19 |
| US4732581A (en) | 1988-03-22 |
| DE3750100T2 (de) | 1994-10-13 |
| EP0486070B1 (en) | 1994-11-09 |
| EP0245936B1 (en) | 1994-06-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |