AT52974B - Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid. - Google Patents

Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid.

Info

Publication number
AT52974B
AT52974B AT52974DA AT52974B AT 52974 B AT52974 B AT 52974B AT 52974D A AT52974D A AT 52974DA AT 52974 B AT52974 B AT 52974B
Authority
AT
Austria
Prior art keywords
disulfonic acid
dimethylphenylbenzylammonium
preparation
desc
halomethyl
Prior art date
Application number
Other languages
German (de)
Original Assignee
Hoechst Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Ag filed Critical Hoechst Ag
Application granted granted Critical
Publication of AT52974B publication Critical patent/AT52974B/en

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

   <Desc/Clms Page number 1> 
 



  Verfahren zur Darstellung einer Dimethylphenylbenzylammoniumdisulfosäure. 



   Es wurde gefunden, dass eine für   Druckereizwecke sehr   wertvolle Dimethylphenyl-   benzylammoniumdisulfosäure   entsteht, wenn man auf die Methylbenzylailindisulfosäure, welche man gemäss dem Verfahren des D. R. P. Nr.   69777   erhält, durch Sulfurieren von   Methylbenzylanilin   erhält, Halogenmethyl oder Dimethylsulfat einwirken lässt. 



   Es ist zwar bekannt, dass sich Ammoniumverbindungen aus tertiären Basen und   Halogenalkylen erhalten lassen.   Dieses Verfahren versagt jedoch bereits bei Aminen von sehr geringer Basizität. Im vorliegenden Falle sind die basischen Eigenschaften durch die beiden Sulfogruppen   überhaupt   verschwunden. Die Ausführbarkeit des Verfahrens war also nicht vorauszusehen. 



   Beispiel : Eine Lösung von 400 Teilen des neutralen Natronsalzes der Methylbenzylanilindisulfosäure, welche man durch Sulfurieren von   Methylbenzylanilin   erhält, wird 
 EMI1.1 
 

**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.



   <Desc / Clms Page number 1>
 



  Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid.



   It has been found that dimethylphenylbenzylammonium disulfonic acid, which is very valuable for printing purposes, is formed when halomethyl or dimethyl sulfate is allowed to act on methylbenzylbenzyl disulfonic acid, which is obtained by sulfurizing methylbenzylaniline according to the method of D. R. P. No. 69777.



   It is known that ammonium compounds can be obtained from tertiary bases and haloalkylenes. However, this process fails even with amines of very low basicity. In the present case, the basic properties have disappeared altogether due to the two sulfo groups. The feasibility of the procedure could not be foreseen.



   Example: A solution of 400 parts of the neutral sodium salt of methylbenzylaniline disulfonic acid, which is obtained by sulfurizing methylbenzylaniline, is used
 EMI1.1
 

** WARNING ** End of DESC field may overlap beginning of CLMS **.

Claims (1)

PATENT-ANSPRUCH : Verfahren zur Darstellung einer Dimethylphenylbenzylamoniumdisulfosäure, darin bestehend, dass man die Methyibenzyianitindisulfosäure in Form ihrer Salze mit Halogenmethyl oder Dimethylsulfat vereinigt. **WARNUNG** Ende CLMS Feld Kannt Anfang DESC uberlappen**. PATENT CLAIM: Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid, which consists in combining the methyl benzyianitine disulfonic acid in the form of its salts with halomethyl or dimethyl sulfate. ** WARNING ** End of CLMS field may overlap beginning of DESC **.
AT52974D 1910-03-22 1911-03-18 Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid. AT52974B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE52974X 1910-03-22

Publications (1)

Publication Number Publication Date
AT52974B true AT52974B (en) 1912-04-10

Family

ID=5627474

Family Applications (1)

Application Number Title Priority Date Filing Date
AT52974D AT52974B (en) 1910-03-22 1911-03-18 Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid.

Country Status (1)

Country Link
AT (1) AT52974B (en)

Similar Documents

Publication Publication Date Title
AT52974B (en) Process for the preparation of a dimethylphenylbenzylammonium disulfonic acid.
DE977642C (en) Wetting agents
DE952981C (en) Process for the production of surface-active polyoxalkylated N- (tert-alkyl) -amines
AT107314B (en) Process for the synthetic production of ammonia from the elements.
AT52976B (en) Process for the preparation of a dimethylbenzylphenylammonium monosulfonic acid.
DE714105C (en) Water-soluble impregnation agent for wood
AT72939B (en) Process for the production of a paint composition.
DE216581C (en) Process for the preparation of a pure water-soluble, neutral salt-like compound from lactalbumin
AT76930B (en) Process for the production of soap and soap emulsions.
DE648539C (en) Process for the production of coarsely crystalline ammonium sulfate
AT73580B (en) Process for the preparation of boroformates of alkalis.
AT117846B (en) Process for the production of a cleaning compound.
AT117442B (en) Process for precipitating viscose solutions.
AT97693B (en) Method of gluing paper in fabric.
AT111249B (en) Process for the preparation of complex antimony compounds.
AT54593B (en) Process for preventing boiler corrosion and the formation of scale in steam generators.
AT160531B (en) Process for improving aqueous emulsions of natural or synthetic rubber and the articles and coatings made therefrom.
AT71175B (en) Process for the preparation of salizyloyl theobromine.
AT73446B (en) Process for the production of highly concentrated, viscous emulsion masses from asphalt, tar, pitch, resins, balsams, oils, paraffins and other hydrocarbons, cresols and other water-insoluble or sparingly soluble substances or mixtures thereof.
DE952021C (en) Process for breaking petroleum emulsions
AT18569B (en) Process for the production of antiseptic bezw. metal soap solutions with a preservative effect.
AT119775B (en) Process for the electrolytic production of protective layers from lead peroxide on electrical conductors connected as anode.
AT62216B (en) Process for the simultaneous production of ammonium phosphate and ammonium nitrate.
AT72451B (en) Process for the production of highly concentrated, viscous emulsion masses from asphalt, tar, pitch, resins, balsams, oils, paraffins and other hydrocarbons, cresols and other water-insoluble or sparingly soluble substances or mixtures thereof.
AT72460B (en) Process for the production of concentrated acetic acid from dilute, aqueous solutions.