AR092069A1 - Proceso para la produccion de un material de espinela - Google Patents

Proceso para la produccion de un material de espinela

Info

Publication number
AR092069A1
AR092069A1 ARP130102807A ARP130102807A AR092069A1 AR 092069 A1 AR092069 A1 AR 092069A1 AR P130102807 A ARP130102807 A AR P130102807A AR P130102807 A ARP130102807 A AR P130102807A AR 092069 A1 AR092069 A1 AR 092069A1
Authority
AR
Argentina
Prior art keywords
powder
compound
dissolved
microwave treatment
solution
Prior art date
Application number
ARP130102807A
Other languages
English (en)
Original Assignee
Csir
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Csir filed Critical Csir
Publication of AR092069A1 publication Critical patent/AR092069A1/es

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Nickelates
    • C01G53/42—Nickelates containing alkali metals, e.g. LiNiO2
    • C01G53/44—Nickelates containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/54—Nickelates containing alkali metals, e.g. LiNiO2 containing manganese of the type [Mn2O4]-, e.g. Li(NixMn2-x)O4, Li(MyNixMn2-x-y)O4
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B1/00—Single-crystal growth directly from the solid state
    • C30B1/02—Single-crystal growth directly from the solid state by thermal treatment, e.g. strain annealing
    • C30B1/04—Isothermal recrystallisation
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/16—Oxides
    • C30B29/22—Complex oxides
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B30/00—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions
    • C30B30/02—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions using electric fields, e.g. electrolysis
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/30—Three-dimensional structures
    • C01P2002/32—Three-dimensional structures spinel-type (AB2O4)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C01P2002/54—Solid solutions containing elements as dopants one element only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/74—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by peak-intensities or a ratio thereof only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Metallurgy (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

Un proceso para la producción de un material de espinela de óxido de litio-manganeso-níquel incluye mantener una solución que comprende un compuesto de litio disuelto, un compuesto de manganeso disuelto, un compuesto de níquel disuelto, un ácido hidroxicarboxílico, un alcohol polihidroxi, y, en forma opcional, un compuesto metálico adicional, a una temperatura elevada T₁, en donde T₁ se encuentra por debajo del punto de ebullición de la solución, hasta que la solución se gelifica. El gel se mantiene a una temperatura elevada hasta que se enciende y se quema para formar un polvo de Li-Mn-Ni-O. El polvo de Li-Mn-Ni-O se calcina para quemar el carbono y/u otras impurezas presentes en el polvo. El polvo calcinado resultante se somete en forma opcional a tratamiento de microondas, a fin de obtener un polvo tratado el cual se hibrida para cristalizar el polvo. El material hibridado resultante se somete en forma opcional al tratamiento de microondas. Se lleva a cabo por lo menos un tratamiento de microondas. De ese modo, se obtiene el material de espinela de óxido de litio-manganeso-níquel.
ARP130102807A 2012-08-10 2013-08-07 Proceso para la produccion de un material de espinela AR092069A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ZA201206016 2012-08-10

Publications (1)

Publication Number Publication Date
AR092069A1 true AR092069A1 (es) 2015-03-18

Family

ID=49304034

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP130102807A AR092069A1 (es) 2012-08-10 2013-08-07 Proceso para la produccion de un material de espinela

Country Status (10)

Country Link
US (1) US9834854B2 (es)
EP (1) EP2882690B1 (es)
JP (1) JP6316812B2 (es)
KR (1) KR102085903B1 (es)
CN (1) CN104703920A (es)
AR (1) AR092069A1 (es)
BR (1) BR112015002884B1 (es)
CA (1) CA2880876C (es)
WO (1) WO2014024075A1 (es)
ZA (1) ZA201501121B (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DK3164363T3 (da) 2014-07-03 2020-11-23 Csir Fremstilling af et lagdelt lithium-mangan-nikkel-kobolt-oxidmateriale
US9979011B2 (en) * 2014-09-26 2018-05-22 The United States Of America As Represented By The Secretary Of The Army LixMn2O4-y(C1z) spinal cathode material, method of preparing the same, and rechargeable lithium and li-ion electrochemical systems containing the same
BR112017009040B1 (pt) * 2014-10-31 2022-06-14 Csir Produção de um material de espinélio
US10505188B2 (en) * 2015-03-03 2019-12-10 The Government Of The United States As Represented By The Secretary Of The Army “B” and “O” site doped AB2O4 spinel cathode material, method of preparing the same, and rechargeable lithium and Li-ion electrochemical systems containing the same
CN108604673B (zh) * 2015-12-22 2022-02-08 Csir公司 尖晶石材料
CN105576231A (zh) * 2016-02-25 2016-05-11 江南大学 一种具有尖晶石结构的高电压锂离子电池正极材料及其制备方法
EP3435158A4 (en) 2016-03-24 2019-01-30 Fujifilm Corporation ACTIVE RADIATIVE OR RADIATIVE COMPOSITION, METHOD FOR CLEANING AN ACTIVE RADIATION-SENSITIVE OR RADIATION-SENSITIVE COMPOSITION, STRUCTURE-FORMING METHOD, AND METHOD FOR PRODUCING AN ELECTRONIC DEVICE
EP3435157B1 (en) 2016-03-24 2021-01-06 FUJIFILM Corporation Active light sensitive or radiation sensitive composition, method for producing active light sensitive or radiation sensitive composition, pattern forming method, and electronic device producing method
WO2017164018A1 (ja) 2016-03-24 2017-09-28 富士フイルム株式会社 感活性光線性又は感放射線性組成物、感活性光線性又は感放射線性組成物の精製方法、感活性光線性又は感放射線性組成物の製造方法、パターン形成方法、及び電子デバイスの製造方法
US10516156B2 (en) * 2016-05-25 2019-12-24 The Government Of The United States As Represented By The Secretary Of The Army Chlorinated lithium manganese oxide spinel cathode material with charge transfer catalyst coating, method of preparing the same, and Li electrochemical cell containing the same
KR101963251B1 (ko) * 2017-10-17 2019-03-29 한국과학기술연구원 양극 활물질 제조방법 및 이를 이용한 이차전지
CN114369863B (zh) * 2021-12-08 2023-02-14 中国科学院地球化学研究所 一种高温高压下制备锰铝榴石单晶的方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2221213B (en) * 1988-07-12 1991-09-04 Csir Synthesizing lithium manganese oxide
CN1042377C (zh) * 1996-05-10 1999-03-03 中国科学院物理研究所 一种合成锂离子电池中正极材料的方法
DE69701063T2 (de) * 1996-06-27 2000-07-13 Honjo Chem Kk Verfahren zur Herstellung von Lithium-Mangan-Oxid mit Spinelstruktur
JP2973299B2 (ja) * 1996-06-27 1999-11-08 本荘ケミカル株式会社 スピネル型構造を有するリチウム−マンガン複合酸化物の製造方法
JP3411488B2 (ja) * 1997-12-01 2003-06-03 本荘ケミカル株式会社 リチウムイオン二次電池用正極活物質の製造方法
JP2000281355A (ja) * 1999-03-29 2000-10-10 Nippon Chem Ind Co Ltd リチウム複合酸化物の製造方法
JP4726896B2 (ja) * 2005-04-28 2011-07-20 日産自動車株式会社 非水電解質リチウムイオン電池用正極材料およびこれを用いた電池
US8496855B2 (en) * 2009-07-27 2013-07-30 Samsung Electronics Co., Ltd. Cathode active material, cathode including cathode active material, and lithium battery including cathode
JP2011210463A (ja) * 2010-03-29 2011-10-20 Jx Nippon Mining & Metals Corp リチウムイオン電池用正極活物質の製造方法

Also Published As

Publication number Publication date
KR102085903B1 (ko) 2020-03-06
EP2882690A1 (en) 2015-06-17
ZA201501121B (en) 2016-01-27
BR112015002884A2 (pt) 2019-10-08
EP2882690B1 (en) 2016-10-12
WO2014024075A1 (en) 2014-02-13
JP2015525734A (ja) 2015-09-07
BR112015002884B1 (pt) 2021-06-08
JP6316812B2 (ja) 2018-04-25
US20150197872A1 (en) 2015-07-16
CA2880876C (en) 2020-07-07
US9834854B2 (en) 2017-12-05
CN104703920A (zh) 2015-06-10
KR20150056542A (ko) 2015-05-26
CA2880876A1 (en) 2014-02-13

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