AR022562A1 - Procedimiento para el control y el monitoreo continuos de la conversion de monomeros en la polimerizacion por emulsion - Google Patents
Procedimiento para el control y el monitoreo continuos de la conversion de monomeros en la polimerizacion por emulsionInfo
- Publication number
- AR022562A1 AR022562A1 ARP000100580A ARP000100580A AR022562A1 AR 022562 A1 AR022562 A1 AR 022562A1 AR P000100580 A ARP000100580 A AR P000100580A AR P000100580 A ARP000100580 A AR P000100580A AR 022562 A1 AR022562 A1 AR 022562A1
- Authority
- AR
- Argentina
- Prior art keywords
- reactor
- qad
- amount
- monomers
- emulsion polymerization
- Prior art date
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/22—Emulsion polymerisation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/01—Processes of polymerisation characterised by special features of the polymerisation apparatus used
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
- B01J2219/0006—Temperature measurement of the heat exchange medium
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
- B01J2219/00063—Temperature measurement of the reactants
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00065—Pressure measurement
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00072—Mathematical modelling
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00162—Controlling or regulating processes controlling the pressure
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00193—Sensing a parameter
- B01J2219/00195—Sensing a parameter of the reaction system
- B01J2219/002—Sensing a parameter of the reaction system inside the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
- B01J2219/00216—Parameter value calculated by equations
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00222—Control algorithm taking actions
- B01J2219/00225—Control algorithm taking actions stopping the system or generating an alarm
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00222—Control algorithm taking actions
- B01J2219/00227—Control algorithm taking actions modifying the operating conditions
- B01J2219/00229—Control algorithm taking actions modifying the operating conditions of the reaction system
- B01J2219/00231—Control algorithm taking actions modifying the operating conditions of the reaction system at the reactor inlet
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00222—Control algorithm taking actions
- B01J2219/00227—Control algorithm taking actions modifying the operating conditions
- B01J2219/00238—Control algorithm taking actions modifying the operating conditions of the heat exchange system
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00243—Mathematical modelling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00245—Avoiding undesirable reactions or side-effects
- B01J2219/00259—Preventing runaway of the chemical reaction
- B01J2219/00261—Predicting runaway of the chemical reaction
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00245—Avoiding undesirable reactions or side-effects
- B01J2219/0027—Pressure relief
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00245—Avoiding undesirable reactions or side-effects
- B01J2219/00272—Addition of reaction inhibitor
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polymerisation Methods In General (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
Abstract
Procedimiento para el control y el monitoreo en línea de la conversion de monomeros en la polimerizacion por emulsion de un reactor, especialmente enprocedimientos de polimerizacion por emulsion contínuos y semi-contínuos a escala industrial, en donde: a) se elige a partir del momento de iniciacion to = 0 yse asigna al reactor para ese momento una capacidad calorífica original determinada Qo. b) se determina a partir del momento de iniciacion en forma contínua lacantidad de calor suministrada alreactor QIN, la entalpía de reaccion suministrada QOUT eliminada del reactor. c) se calcula la cantidad de calor QAD noeliminada de acuerdo con la siguiente ecuacion: QAD(t) = Qo + QIN(T) + QRE(t) -QOUT(t), d) se calcula la temperatura interior TADmáxima producida en el casode una reaccion adiabática espontánea a partir de la cantidad de calor (QAD(t) no eliminada y de la temperatura interior momentánea T(t) del reactor, y e) sila temperatura interior TAD máxima calculada sobrepasa la temperatura interior momentánea T(t) del reactor por un valor determinado se toman medidas que evitenun aumento ulterior de la cantidad de valor QAD no eliminada. Dichas medidas son: reduccion de la alimentacion de monomeros; aumento de la refrigeracion delreactor; incremento del aporte de iniciadores. Los aspectos de seguridad tienen un papel preponderante en el procedimiento de produccion en la industriaquímica. Normalmente los procedimientos químicos de produccion son controlados constantemente paraevitar posibles situaciones de riesgo, que podrían llevar aexplosiones o a la liberacion de productos químicos nocivos al medio ambiente y los seres vivos.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19905712A DE19905712A1 (de) | 1999-02-11 | 1999-02-11 | Verfahren zur kontinuierlichen Überwachung und Steuerung des Monomerenumsatzes bei der Emulsionspolymerisation |
Publications (1)
Publication Number | Publication Date |
---|---|
AR022562A1 true AR022562A1 (es) | 2002-09-04 |
Family
ID=7897184
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP000100580A AR022562A1 (es) | 1999-02-11 | 2000-02-10 | Procedimiento para el control y el monitoreo continuos de la conversion de monomeros en la polimerizacion por emulsion |
Country Status (16)
Country | Link |
---|---|
US (1) | US6498219B1 (es) |
EP (1) | EP1153042B1 (es) |
JP (1) | JP4705245B2 (es) |
KR (1) | KR100651091B1 (es) |
CN (1) | CN1142942C (es) |
AR (1) | AR022562A1 (es) |
AT (1) | ATE316536T1 (es) |
AU (1) | AU772839B2 (es) |
BR (1) | BR0008115B1 (es) |
CA (1) | CA2362511C (es) |
DE (2) | DE19905712A1 (es) |
ES (1) | ES2257290T3 (es) |
ID (1) | ID30021A (es) |
TR (1) | TR200102319T2 (es) |
WO (1) | WO2000047632A1 (es) |
ZA (1) | ZA200107439B (es) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6991763B2 (en) * | 2000-04-26 | 2006-01-31 | Rohm And Haas Company | Polymer process |
DE10225383A1 (de) * | 2002-06-07 | 2003-12-18 | Basf Ag | Verfahren zur Überwachung und Sicherung von exothermen Reaktionen |
US20040143053A1 (en) * | 2003-01-21 | 2004-07-22 | Wu Richard Shu-Hua | Process for preparing emulsion polymers |
EP1705193B1 (en) * | 2005-03-24 | 2008-05-14 | Rohm and Haas Company | Polymerization processes |
CN101234322B (zh) * | 2006-01-31 | 2012-04-04 | 住友化学株式会社 | 反应控制方法 |
CN106940331B (zh) * | 2017-03-21 | 2019-09-06 | 山东京博石油化工有限公司 | 间歇液相本体法制备聚丙烯的聚合转化率的测量方法 |
WO2018206480A1 (en) * | 2017-05-12 | 2018-11-15 | Mitec S.R.L. Società Di Ingegneria | Method and system for monitoring the operating conditions of a semibatch reactor |
EP3922348A1 (de) | 2020-06-09 | 2021-12-15 | Basf Se | Verfahren zur überwachung eines reaktors für eine mehrphasenreaktion |
DE102022209657A1 (de) | 2022-09-14 | 2024-03-14 | Siemens Aktiengesellschaft | Überwachung exothermer Reaktionen in einem Reaktor |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2803623A (en) * | 1951-10-29 | 1957-08-20 | Phillips Petroleum Co | Temperature control of low temperature emulsion polymerization |
DE1283197B (de) * | 1963-09-20 | 1968-11-21 | Huels Chemische Werke Ag | Verfahren zur automatischen Regelung der Umsatzverteilung in kontinuierlich durchflossenen Reaktorreihen |
US3563946A (en) * | 1968-01-08 | 1971-02-16 | Dow Chemical Co | Process for latex manufacture |
US3991258A (en) * | 1970-03-10 | 1976-11-09 | Imperial Chemical Industries Limited | Control of exothermic and endothermic chemical reactions |
JPS60248702A (ja) * | 1984-05-24 | 1985-12-09 | Mitsubishi Rayon Co Ltd | 重合反応制御方法および装置 |
JPS6274449A (ja) * | 1985-09-28 | 1987-04-06 | Toshiba Corp | 加熱反応釜の温度制御装置 |
JPH04106104A (ja) * | 1990-08-27 | 1992-04-08 | Nippon Zeon Co Ltd | 重合工程における反応制御方法及び反応制御装置 |
-
1999
- 1999-02-11 DE DE19905712A patent/DE19905712A1/de not_active Withdrawn
-
2000
- 2000-02-10 TR TR2001/02319T patent/TR200102319T2/xx unknown
- 2000-02-10 CA CA002362511A patent/CA2362511C/en not_active Expired - Fee Related
- 2000-02-10 WO PCT/EP2000/001091 patent/WO2000047632A1/de active IP Right Grant
- 2000-02-10 JP JP2000598547A patent/JP4705245B2/ja not_active Expired - Fee Related
- 2000-02-10 BR BRPI0008115-9A patent/BR0008115B1/pt not_active IP Right Cessation
- 2000-02-10 AU AU38037/00A patent/AU772839B2/en not_active Ceased
- 2000-02-10 ID IDW00200101977A patent/ID30021A/id unknown
- 2000-02-10 AR ARP000100580A patent/AR022562A1/es not_active Application Discontinuation
- 2000-02-10 EP EP00916827A patent/EP1153042B1/de not_active Expired - Lifetime
- 2000-02-10 CN CNB008036705A patent/CN1142942C/zh not_active Expired - Fee Related
- 2000-02-10 ES ES00916827T patent/ES2257290T3/es not_active Expired - Lifetime
- 2000-02-10 KR KR1020017010101A patent/KR100651091B1/ko not_active IP Right Cessation
- 2000-02-10 DE DE50012127T patent/DE50012127D1/de not_active Expired - Lifetime
- 2000-02-10 AT AT00916827T patent/ATE316536T1/de not_active IP Right Cessation
- 2000-02-11 US US09/890,968 patent/US6498219B1/en not_active Expired - Lifetime
-
2001
- 2001-09-10 ZA ZA200107439A patent/ZA200107439B/en unknown
Also Published As
Publication number | Publication date |
---|---|
CA2362511A1 (en) | 2000-08-17 |
CN1340062A (zh) | 2002-03-13 |
JP2002536509A (ja) | 2002-10-29 |
TR200102319T2 (tr) | 2001-11-21 |
DE50012127D1 (de) | 2006-04-13 |
ES2257290T3 (es) | 2006-08-01 |
BR0008115B1 (pt) | 2010-01-26 |
US6498219B1 (en) | 2002-12-24 |
BR0008115A (pt) | 2001-11-06 |
ID30021A (id) | 2001-11-01 |
JP4705245B2 (ja) | 2011-06-22 |
CA2362511C (en) | 2008-05-06 |
CN1142942C (zh) | 2004-03-24 |
ZA200107439B (en) | 2002-09-10 |
KR100651091B1 (ko) | 2006-11-29 |
KR20010102026A (ko) | 2001-11-15 |
AU3803700A (en) | 2000-08-29 |
AU772839B2 (en) | 2004-05-06 |
EP1153042A1 (de) | 2001-11-14 |
EP1153042B1 (de) | 2006-01-25 |
DE19905712A1 (de) | 2000-08-17 |
WO2000047632A1 (de) | 2000-08-17 |
ATE316536T1 (de) | 2006-02-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FA | Abandonment or withdrawal |