YU27001A - Postupak za prečišćavanje amonijumsulfata - Google Patents

Postupak za prečišćavanje amonijumsulfata

Info

Publication number
YU27001A
YU27001A YU27001A YU27001A YU27001A YU 27001 A YU27001 A YU 27001A YU 27001 A YU27001 A YU 27001A YU 27001 A YU27001 A YU 27001A YU 27001 A YU27001 A YU 27001A
Authority
YU
Yugoslavia
Prior art keywords
ammonium sulfate
sodium sulfate
energy
bicarbonate
art
Prior art date
Application number
YU27001A
Other languages
English (en)
Inventor
Robin Phinney
Mark Hantke
Original Assignee
Airborne Industrial Minerals Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Airborne Industrial Minerals Inc. filed Critical Airborne Industrial Minerals Inc.
Publication of YU27001A publication Critical patent/YU27001A/sh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/24—Sulfates of ammonium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/02—Preparation by double decomposition
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/18—Preparation by the ammonia-soda process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Fertilizers (AREA)
  • Treating Waste Gases (AREA)
  • Removal Of Specific Substances (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

Postupak za sintetizovanje amonijumsulfata i natrijum bikarbonata kvaliteta prema Farmakopeji SAD. Postupak omogućuje prevodjenje, uz efikasno korišćenje energije, prekursorskog natrijumsulfata i natrijum bikarbonata u amonijumsulfat, djubrivo visokog kvaliteta, i u natrijum bikarbonat farmaceutskog kvaliteta zasićenjem procesnog luga natrijumsulfatom. Ovaj stepen ranije nije uočen u poznatom stanju tehnike, što je dovelo do toga da su postupci prema poznatom stanju tehnike bili neefikasni sa stanovišta tehnike, energije i kvaliteta proizvoda. Ovaj postupak ponovo uvodi natrijumsulfat u procesni lug ili rastvor radi ponavljanja procesa prevodjenja bez problema razdvajanja i troškova za energiju koji su inherentni u poznatom stanju tehnike.[A process for synthesizing ammonium sulfate and United States Pharmacopoeia grade sodium bicarbonate. The process allows an energy efficient conversion of precursor sodium sulfate and bicarbonate to ammonium sulfate high grade fertilizer and the pharmaceutical grade sodium bicarbonate by saturation of process brine with sodium sulfate. This step was previously unrecognized in the art, which resulted in prior art methods being ineffectual from engineering, energy and product quality points of view. The present process reintroduces sodium sulfate into the process brine or solution to perpetuate the conversion process in the absence of separation problems and energy expenditures inherent in the prior art techniques.
YU27001A 1998-10-13 1999-09-30 Postupak za prečišćavanje amonijumsulfata YU27001A (sh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10396898P 1998-10-13 1998-10-13

Publications (1)

Publication Number Publication Date
YU27001A true YU27001A (sh) 2003-10-31

Family

ID=22297984

Family Applications (1)

Application Number Title Priority Date Filing Date
YU27001A YU27001A (sh) 1998-10-13 1999-09-30 Postupak za prečišćavanje amonijumsulfata

Country Status (23)

Country Link
US (1) US6106796A (sh)
EP (1) EP1124756A1 (sh)
JP (1) JP2002527329A (sh)
KR (1) KR20010088871A (sh)
CN (2) CN1177759C (sh)
AU (1) AU765320B2 (sh)
BG (1) BG105426A (sh)
BR (1) BR9914548A (sh)
CA (1) CA2284969A1 (sh)
CZ (1) CZ20011177A3 (sh)
EA (1) EA200100341A1 (sh)
HR (1) HRP20000126A2 (sh)
HU (1) HUP0104345A3 (sh)
ID (1) ID28731A (sh)
NO (1) NO20011850L (sh)
NZ (1) NZ510785A (sh)
PL (1) PL347034A1 (sh)
SI (1) SI20635A (sh)
SK (1) SK5012001A3 (sh)
TR (1) TR200100966T2 (sh)
WO (1) WO2000021886A1 (sh)
YU (1) YU27001A (sh)
ZA (1) ZA200001143B (sh)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7393378B2 (en) * 2003-02-11 2008-07-01 Airborne Industrial Minerals Inc. Method for recovering purified sodium bicarbonate and ammonium sulfate
CN101746779B (zh) * 2009-12-16 2011-05-18 上海高桥大同净水材料有限公司 用于水处理的液态硫酸铵的精制方法
CN102210966A (zh) * 2010-04-02 2011-10-12 航空工业矿石公司 烟道气净化方法
CN102198953A (zh) * 2011-04-07 2011-09-28 四川金圣赛瑞化工有限责任公司 以蜜胺尾气和芒硝联合生产纯碱和硫酸铵的方法
EP2882879A4 (en) * 2012-08-10 2016-11-23 Sparstane Technologies LLC PROCESS FOR THE CONVERSION OF DEGREASING GYPSUM FROM A GASEOUS EFFLUENT (FGD) TO AMMONIUM SULPHATE AND CALCIUM CARBONATE
CN108046295B (zh) * 2018-01-10 2020-02-28 四川大学 用硫酸钠溶液生产碳酸氢钠和硫酸铵的方法
CN111039305B (zh) * 2018-10-12 2021-11-12 中国科学院过程工程研究所 一种硫酸钠短流程制备碳酸氢钠与硫酸铵的方法
CN111039304B (zh) * 2018-10-12 2021-11-12 中国科学院过程工程研究所 一种硫酸钠制备硫酸铵与碳酸氢钠的方法
CN114349028B (zh) * 2021-11-29 2023-06-23 攀钢集团研究院有限公司 沉钒废水资源化利用的方法
CN114291827B (zh) * 2021-12-09 2022-06-28 中国科学院过程工程研究所 一种大颗粒碳酸氢钠的制备方法
CN114751429B (zh) * 2022-04-01 2023-06-23 北京赛科康仑环保科技有限公司 一种脱硫灰制小苏打的处理工艺

Family Cites Families (45)

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Publication number Priority date Publication date Assignee Title
CA821457A (en) * 1969-08-26 Montagna Antonio Separation of sodium sulphate and ammonium sulphate from aqueous solutions of a mixture of them
US1979151A (en) * 1931-07-15 1934-10-30 Alterum Kredit Aktien Ges Manufacture of alkali carbonate or alkali hydroxide
BE534078A (sh) * 1953-12-14
NL148013B (nl) * 1964-10-06 1975-12-15 Edison Soc Werkwijze om natriumsulfaat en ammoniumsulfaat afzonderlijk te winnen uit een waterige oplossing, die een mengsel daarvan bevat.
US3528767A (en) * 1966-03-16 1970-09-15 Donald E Garrett Production of potassium chloride,potassium sulfate and sodium sulfate from brines and the like containing potassium,chloride and sulfate
US3493329A (en) * 1966-03-30 1970-02-03 Edouard Louis Stiers Method of making sodium carbonate
US3423171A (en) * 1966-06-14 1969-01-21 Kali Forschungs Inst Method for making alkali metal sulfate
US3429657A (en) * 1966-09-02 1969-02-25 Us Interior Method for recovering and producing potassium salts
US3578399A (en) * 1968-10-23 1971-05-11 Int Minerals & Chem Corp Production of crystalline potassium sulfate
CA916665A (en) * 1970-02-17 1972-12-12 Cominco Ltd. Potash granulation
US3687639A (en) * 1970-05-25 1972-08-29 Int Minerals & Chem Corp Production of finely divided potassium sulfate crystals
US3656891A (en) * 1970-08-05 1972-04-18 Occidental Petroleum Corp Process for the production of potassium sulfate and borax
US3728438A (en) * 1970-09-03 1973-04-17 G Nasyrov Method of producing potassium sulphate from alkali metal sulphates or their mixtures with carbonates
US3843772A (en) * 1972-09-14 1974-10-22 Int Minerals & Chem Corp Production of white potassium sulfate crystals
US3983211A (en) * 1972-12-08 1976-09-28 Gakif Zakirovich Nasyrov Method of producing alumina and potassium sulphate form alunite
US3853490A (en) * 1973-01-22 1974-12-10 Int Minerals & Chem Corp Granulation of potassium sulfate
US3984521A (en) * 1973-12-03 1976-10-05 Gakif Zakirovich Nasyrov Method of producing alumina and potassium sulphate from alunite
US3967930A (en) * 1974-11-18 1976-07-06 N L Industries, Inc. Separation of complex potassium salts from brine evaporites
US3998935A (en) * 1975-01-30 1976-12-21 Pennzoil Company Manufacture of potassium sulfate
US4045543A (en) * 1975-11-12 1977-08-30 Pennzoil Company Production of potassium sulfate and hydrogen chloride
DE2627871C2 (de) * 1976-06-22 1978-08-24 Kali Und Salz Ag, 3500 Kassel Verfahren zur Gewinnung von grobem K2 SO4 in Kristallisatoren mit innerer Umwälzung und klassierendem Salzabzug
DE2643001C3 (de) * 1976-09-24 1979-06-07 Kali Und Salz Ag, 3500 Kassel Verfahren zur Herstellung von Kaliumsulfat
US4215100A (en) * 1978-05-18 1980-07-29 Antonova Nina V Method of producing potassium sulfate
DE2950404C2 (de) * 1978-12-25 1984-05-30 Asahi Kasei Kogyo K.K., Osaka Verfahren zur Herstellung von Kaliumsulfat
JPS5617922A (en) * 1979-07-19 1981-02-20 Chisso Corp Continuously manufacturing apparatus for potassium sulfate
US4268492A (en) * 1979-08-06 1981-05-19 Pennzoil Company Process for production of potassium sulfate and hydrochloric acid
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JPS57205315A (en) * 1981-06-15 1982-12-16 Chisso Corp Reducting method for amount of chlorine contained in modified potassium sulfate by very small amount
FR2523114A1 (fr) * 1982-03-11 1983-09-16 Alsace Mines Potasse Procede de fabrication de sulfate de potassium a partir de solutions contenant du chlorure de magnesium et de chlorure de potassium
JPS58161917A (ja) * 1982-03-19 1983-09-26 Onoda Kagaku Kogyo Kk 硫酸カリウムの製造方法
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US4554151A (en) * 1983-09-27 1985-11-19 Prodeco, Inc. Process for producing K3 H(SO4)2 crystals and potassium sulfate crystals
IT1174208B (it) * 1984-06-19 1987-07-01 Italkali Procentimento per la produzione di solfato potassico e di solfati potassico magnesiaci granulati, e granulati cosi'prodotti
US4707347A (en) * 1985-04-17 1987-11-17 Kali Und Salz Process for the production of potassium sulfate from potassium chloride by means of ion exchangers
US4844874A (en) * 1987-11-12 1989-07-04 Quad Environmental Technologies Corp. Method and means for controlling mist scrubber operation
FR2638108B1 (fr) * 1988-10-26 1991-02-08 Solvay Procede pour eliminer un residu comprenant du sulfate de sodium
US5654351A (en) * 1990-12-18 1997-08-05 Ormiston Mining And Smelting Co. Ltd. Method for sodium carbonate compound recovery and formation of ammonium sulfate
CA2032627C (en) * 1990-12-18 1997-01-14 Jack S. Thompson Process for producing sodium carbonate and ammonium sulphate from sodium sulphate
US5298050A (en) * 1992-10-09 1994-03-29 Great Salt Lake Minerals Corporation High water solubility potassium sulfate and method of producing same
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US5549876A (en) * 1994-11-28 1996-08-27 Dead Sea Works Production of potassium sulfate using differential contacting
US5552126A (en) * 1994-11-28 1996-09-03 Dead Sea Works Ltd. Co-production of potassium sulfate, sodium sulfate and sodium chloride
US5529764A (en) * 1994-11-28 1996-06-25 Dead Sea Works Ltd. Co-production of potassium sulfate and sodium sulfate
US5830422A (en) * 1995-06-23 1998-11-03 Ormiston Mining And Smelting Co. Ltd. Method for production of sodium bicarbonate, sodium carbonate and ammonium sulfate from sodium sulfate

Also Published As

Publication number Publication date
TR200100966T2 (tr) 2001-09-21
WO2000021886A1 (en) 2000-04-20
BG105426A (bg) 2001-12-29
CA2284969A1 (en) 2000-04-13
NZ510785A (en) 2003-11-28
PL347034A1 (en) 2002-03-11
HRP20000126A2 (en) 2001-02-28
BR9914548A (pt) 2001-06-26
EP1124756A1 (en) 2001-08-22
JP2002527329A (ja) 2002-08-27
ZA200001143B (en) 2000-11-21
CN1177759C (zh) 2004-12-01
CN1330611A (zh) 2002-01-09
AU5845599A (en) 2000-05-01
NO20011850L (no) 2001-06-13
HUP0104345A2 (hu) 2002-03-28
AU765320B2 (en) 2003-09-18
ID28731A (id) 2001-06-28
SK5012001A3 (en) 2001-10-08
KR20010088871A (ko) 2001-09-28
CZ20011177A3 (cs) 2001-09-12
SI20635A (sl) 2002-02-28
HUP0104345A3 (en) 2003-01-28
EA200100341A1 (ru) 2002-04-25
CN1491890A (zh) 2004-04-28
US6106796A (en) 2000-08-22
NO20011850D0 (no) 2001-04-10

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