WO2021190643A1 - 槟榔风味的制品 - Google Patents

槟榔风味的制品 Download PDF

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Publication number
WO2021190643A1
WO2021190643A1 PCT/CN2021/083378 CN2021083378W WO2021190643A1 WO 2021190643 A1 WO2021190643 A1 WO 2021190643A1 CN 2021083378 W CN2021083378 W CN 2021083378W WO 2021190643 A1 WO2021190643 A1 WO 2021190643A1
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WO
WIPO (PCT)
Prior art keywords
acid
arecoline
extract
oil
salt
Prior art date
Application number
PCT/CN2021/083378
Other languages
English (en)
French (fr)
Inventor
傅国锋
卢禁
楚明
周星
黄雯雯
徐中立
李永海
Original Assignee
深圳市水槟榔生物科技有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from CN202010587899.7A external-priority patent/CN113951545A/zh
Application filed by 深圳市水槟榔生物科技有限公司 filed Critical 深圳市水槟榔生物科技有限公司
Priority to US17/914,774 priority Critical patent/US20230133076A1/en
Priority to EP21777018.9A priority patent/EP4129982A4/en
Priority to JP2022558558A priority patent/JP2023519006A/ja
Publication of WO2021190643A1 publication Critical patent/WO2021190643A1/zh

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D211/68—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D211/72—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D211/78—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/18—Selection of materials, other than tobacco, suitable for smoking
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00—Chewing gum
    • A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00—Chewing gum
    • A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
    • A23G4/068—Chewing gum characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38—Other non-alcoholic beverages
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A23L2/56—Flavouring or bittering agents
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
    • A23L25/30—Mashed or comminuted products, e.g. pulp, pastes, meal, powders; Products made therefrom, e.g. blocks, flakes, snacks; Liquid or semi-liquid products
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303—Plant extracts other than tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06—Use of materials for tobacco smoke filters
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06—Use of materials for tobacco smoke filters
    • A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06—Use of materials for tobacco smoke filters
    • A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Definitions

  • the application belongs to the technical field of chemical synthesis, and relates to a betel nut flavored product.
  • Arecoline (Arecoline), chemical name "1,2,5,6-tetrahydro-1-methyl-3-picolinic acid methyl ester", an oily liquid, has a choline-like effect.
  • Arecoline is a compound with great application value, and its preparation method and application have always attracted people's attention.
  • the application provides a betel nut flavored product, the product containing arecoline salt.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the article is an aerosol-forming substrate for being atomized to generate an aerosol for smoking.
  • the mass percentage of the arecoline salt is 0.2%-15%, preferably 1%-15%, further preferably 2%-15%, It is more preferably 2% to 10%, still more preferably 2% to 5%, still more preferably 2% to 4%, and more preferably 3% to 4%.
  • the arecoline salt is arecoline hydrobromide and/or arecoline benzoate.
  • the preparation method of the arecoline salt is: using ethyl acetate as the extractant to extract arecoline from the areco nuts, adjust the PH value of the extract to 7.5-8.5, take the ethyl acetate layer, and then add Hydrobromic acid or benzoic acid generates arecoline salt crystals, and the arecoline salt crystals are recrystallized to obtain arecoline hydrobromide or arecoline benzoate.
  • the aerosol-forming substrate further includes a solvent and a fragrance.
  • the solvent includes at least one of the following:
  • the solvent includes glycerin, and the mass percentage of glycerin in the aerosol-forming matrix is 0-90%.
  • the solvent includes propylene glycol, and the mass percentage of propylene glycol in the aerosol-forming matrix is 9%-99.8%.
  • the fragrance is selected from at least one of the following:
  • the aerosol-forming substrate is a liquid phase, which is used for atomization using any one of a heating atomization device, an ultrasonic atomization device, an air compression atomization device, and a pressing atomization device to generate Aerosol.
  • the aerosol generating substrate is a solid phase, and is configured to generate an aerosol for inhalation when heated below the ignition point.
  • the article is a bead used in an aerosol generating article.
  • the product is chewing gum.
  • the article is a beverage.
  • the arecoline salt is used in the product, and the user can ingest arecoline when inhaling, and produce a similar effect of chewing betel nut, with low irritation.
  • the first embodiment of the present application provides a use of arecoline salt in preparing an aerosol-forming substrate.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.2%-15%, preferably 1%-15% It is more preferably 2% to 15%, still more preferably 2% to 10%, still more preferably 2% to 5%, still more preferably 2% to 4%.
  • the object added to the arecoline salt includes a solvent.
  • the solvent is selected from at least one of the following:
  • the solvent includes glycerin, and the mass percentage of the glycerin is 0-90%.
  • the solvent includes propylene glycol, and the mass percentage of the propylene glycol is 9%-99.8%.
  • the object added to the arecoline salt further includes a fragrance.
  • the fragrance is selected from at least one of the following:
  • fragrance is not limited to the substances listed above, and all fragrances complying with FEMA codes and CAS codes can be applied.
  • the subject added to the arecoline salt does not contain nicotine and/or nicotine salt.
  • the second embodiment of the present application provides an aerosol-forming substrate, and the aerosol-forming substrate includes:
  • the mass percentage of the arecoline salt is 0.2%-15%, preferably 1%-15%, more preferably 2%-15%, still more preferably 2% to 12%, more preferably 2% to 10%, still more preferably 2% to 8%, still more preferably 2% to 5%, still more preferably 2% to 4%, still more preferably 2% to 3% , More preferably 3% to 4%.
  • the complex acid of the arecoline salt includes at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, benzoic acid, salicylic acid, oxalic acid, citric acid, sorbic acid , Tartaric acid, adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, color Acid, serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine
  • the arecoline salt is arecoline hydrobromide and/or arecoline benzoate.
  • the arecoline salt is obtained by neutralizing the arecoline extracted from the areco nuts with the complex acid.
  • the arecoline salt is arecoline hydrobromide or arecoline benzoate
  • the preparation method is: using ethyl acetate as the extractant to extract arecoline from the areco nuts, and adjust the pH value of the extract to 7.5-8.5, Take the ethyl acetate layer, and then add hydrobromic acid or benzoic acid to generate arecoline salt crystals, and the arecoline salt crystals are recrystallized to obtain arecoline hydrobromide or arecoline benzoate.
  • the solvent includes at least one of the following:
  • the solvent includes glycerin
  • the mass percentage of glycerin in the aerosol-forming matrix is 0% to 90%, preferably 0% to 80%, more preferably 0% to 70%, and even more preferably 0% ⁇ 60%, more preferably 10% to 60%, still more preferably 20% to 60%, still more preferably 30% to 60%, still more preferably 40% to 60%, more preferably 50% to 60%.
  • the solvent includes propylene glycol
  • the mass percentage of propylene glycol in the aerosol-forming substrate is 9%-99.8%, preferably 9%-90%, more preferably 9%-80%, and still more preferably 9. % To 70%, more preferably 9% to 60%, still more preferably 9% to 50%, still more preferably 20% to 50%, still more preferably 30% to 50%, more preferably 35% to 45% .
  • the aerosol-forming substrate includes a fragrance
  • the fragrance is selected from at least one of the following:
  • fragrance is not limited to the substances listed above, and all fragrances complying with FEMA codes and CAS codes can be applied.
  • the arecoline salt is arecoline hydrobromide.
  • the solvent is a mixture of glycerin and propylene glycol with a mass ratio of 1:1.
  • the suction experience of the aerosol-forming substrate can be evaluated from two aspects: the first aspect is the satisfaction of the smoker after the absorption of arecoline salt; the second aspect, Smokers may feel uncomfortable after taking too much arecoline salt.
  • the first aspect is the satisfaction of the smoker after the absorption of arecoline salt
  • the second aspect Smokers may feel uncomfortable after taking too much arecoline salt.
  • the content of arecoline salt in the aerosol-forming substrate is lower than At 0.2%, the smoker does not feel the satisfaction brought by the intake of arecoline; as the content increases, the sense of satisfaction increases; after more than 5%, the discomfort caused by the intake of arecoline salt begins to appear, and Under the experimental conditions, it gradually appears as the content increases; after the content exceeds 15%, the discomfort is unacceptable.
  • the third embodiment of the present application provides an aerosol generating system, including an atomizing device and the aerosol forming substrate described in the second embodiment;
  • the atomizing device is configured to atomize the aerosol-forming substrate to form an aerosol.
  • the atomization device is a heating atomization device.
  • the atomization device is an ultrasonic atomization device.
  • the aerosol-forming substrate includes arecoline salt, glycerin, and propylene glycol.
  • the oscillation frequency of the ultrasonic atomization device is greater than 1 MHz.
  • the atomization device is an air-compressed atomization device or a push-type spray device.
  • the aerosol-forming substrate includes arecoline salt, ethanol, and water.
  • the fourth embodiment of the present application provides a use of arecoline salt in the manufacture of aerosol-generating products.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.2%-15%, preferably 1%- 15%, more preferably 2% to 15%, still more preferably 2% to 10%, still more preferably 2% to 5%, still more preferably 2% to 4%, more preferably 3% to 4%.
  • the objects added to the arecoline salt include atomizers, adhesives, and plant fibers.
  • the mass percentage of the atomizing agent is 5%-30%, preferably 10%- 30%, more preferably 10% to 25%, still more preferably 15% to 25%.
  • the atomizing agent is selected from at least one of the following:
  • the mass percentage of the binder is 1%-20%, preferably 1%- 15%, more preferably 1% to 10%, still more preferably 3% to 10%, still more preferably 5% to 10%.
  • the adhesive is selected from at least one of the following:
  • the mass percentage of the plant fiber is 40% to 80%, preferably 40% to 70%. %, more preferably 50% to 70%, still more preferably 50% to 65%, still more preferably 50% to 60%.
  • the plant fiber is selected from at least one of the following:
  • Betel nut fiber wood pulp fiber, hemp pulp fiber, cotton pulp fiber, bagasse pulp fiber, bamboo pulp fiber, coconut pulp fiber.
  • the object added to the arecoline salt further includes a fragrance.
  • the fragrance is selected from at least one of the following:
  • fragrance is not limited to the substances listed above, and all fragrances complying with FEMA codes and CAS codes can be applied.
  • the subject added to the arecoline salt does not contain tobacco ingredients.
  • the method for manufacturing the aerosol-generating product includes one of a papermaking method, a dry papermaking method, a thick slurry method, and a rolling method.
  • the fifth embodiment of the present application provides an aerosol-generating product, the raw materials of which include arecoline salt, atomizing agent, adhesive and plant fiber.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.2% to 15%, preferably 1% to 15%, more preferably 2% to 15%, and even more preferably 2. % To 10%, more preferably 2% to 5%, still more preferably 2% to 4%, more preferably 3% to 4%.
  • the mass percentage of the atomizing agent is 5% to 30%, preferably 10% to 30%, more preferably 10% to 25%, and even more preferably 15%. % ⁇ 25%.
  • the atomizing agent is selected from at least one of the following:
  • the mass percentage of the binder is 1% to 20%, preferably 1% to 15%, more preferably 1% to 10%, and even more preferably 3. %-10%, more preferably 5%-10%.
  • the adhesive is selected from at least one of the following:
  • the mass percentage of the plant fiber is 40% to 80%, preferably 40% to 70%, more preferably 50% to 70%, and even more preferably 50% ⁇ 65%, more preferably 50% to 60%.
  • the plant fiber is selected from at least one of the following:
  • Betel nut fiber wood pulp fiber, hemp pulp fiber, cotton pulp fiber, bagasse pulp fiber, bamboo pulp fiber, coconut pulp fiber.
  • the raw material further includes a flavoring agent.
  • the fragrance is selected from at least one of the following:
  • fragrance is not limited to the substances listed above, and all fragrances complying with FEMA codes and CAS codes can be applied.
  • the raw material does not contain tobacco ingredients.
  • Step 1 Prepare a thin substrate. Select the solid residue of betel nut extract and soak it in water at a water temperature of 60-80°C and a soaking time of 0.5-2h. Filter, and then beat the filtered solid to obtain a slurry. Weigh 50-70 parts by weight of the slurry , 3-10 parts of solid binder, uniformly mix, send the mixed slurry to the paper machine for forming, and dry to a moisture content of about 10-15% to obtain a sheet base;
  • the solid binder can be carboxymethyl cellulose, hydroxypropyl methyl cellulose, polyvinyl alcohol, rosin, xanthan gum, acacia, guar gum, chitosan, pectin, locust bean gum, One or more of starch, sodium alginate and shellac.
  • Step 2 Prepare the coating liquid. Weigh 1-50 parts of arecoline salt, 2-20 parts of spices, and 40-80 parts of atomizing agent by weight, and mix them evenly to obtain a coating liquid;
  • the atomizing agent is a mixture of glycerin and propylene glycol, and the mixing ratio is 3 to 5:1.
  • Step 3 Coating the sheet substrate. Weigh 25%-40% of the weight of the flake substrate obtained in step 1 and weigh the coating liquid obtained in step 2 and spray the coating liquid on the flake substrate, and let it stand for 40-60 hours under constant temperature and humidity conditions to obtain arecoline-containing Salt plant flakes;
  • Step 4 Prepare heat-not-burn cigarettes.
  • the plant flakes obtained in step 3 are made into cigarette sticks according to the size, and the cigarette sticks are connected with the filter to obtain heat-not-burn cigarettes containing arecoline salt.
  • the heating non-burning cigarettes prepared by the above preparation method are heated by an aerosol generating device (heating method adopts resistance heating), and the temperature of the surface of the heating element in the working state is measured by an infrared thermal imager.
  • heating method adopts resistance heating
  • infrared thermal imager The test results are shown in the following table
  • Smoking and sensory quality evaluation are carried out with ordinary heat-not-burn cigarettes: the heat-not-burn cigarettes prepared by the above preparation method can ingest arecoline and produce similar effects of chewing betel nut, with low irritation.
  • the sixth embodiment of the present application provides a use of arecoline salt in a liquid composition for preparing fast-fried beads; wherein, the fast-fried beads include a fragile shell and the liquid composition, and the liquid composition is set in the Fragile inside the shell.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.2% to 15%, preferably 1% to 15%, more preferably 2% to 15%, and more preferably It is 2% to 10%, more preferably 2% to 5%, still more preferably 2% to 4%, more preferably 3% to 4%.
  • the object added to the arecoline salt includes an atomizer.
  • the mass percentage of the atomizing agent is 5% to 30%, preferably 10% to 30%, more preferably 10% to 25%, and more preferably It is 15% to 25%.
  • the atomizing agent is selected from at least one of the following:
  • the object added to the arecoline salt further includes a fragrance.
  • the fragrance is selected from at least one of the following:
  • fragrance is not limited to the substances listed above, and all fragrances complying with FEMA codes and CAS codes can be applied.
  • the subject added to the arecoline salt does not contain nicotine and/or nicotine salt.
  • the explosive beads are implanted in an aerosol-generating article.
  • the raw material of the aerosol-generating article does not contain tobacco ingredients.
  • the seventh embodiment of the present application provides a bead that includes a fragile shell and a liquid composition, and the liquid composition is arranged in the fragile shell;
  • the liquid composition includes arecoline salt and an atomizing agent.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.2% to 15%, preferably 1% to 15%, further preferably 2% to 15%, further It is preferably 2% to 10%, more preferably 2% to 5%, still more preferably 2% to 4%, and more preferably 3% to 4%.
  • the mass percentage of the atomizing agent is 5% to 30%, preferably 10% to 30%, more preferably 10% to 25%, and more preferably It is 15% to 25%.
  • the atomizing agent is selected from at least one of the following:
  • the liquid composition further includes a fragrance.
  • the fragrance is selected from at least one of the following:
  • fragrance is not limited to the substances listed above, and all fragrances complying with FEMA codes and CAS codes can be applied.
  • the liquid composition does not contain nicotine and/or nicotine salt.
  • the eighth embodiment of the present application provides an aerosol-generating product, including the explosive beads described in the seventh embodiment.
  • the raw material of the aerosol-generating article does not contain tobacco ingredients.
  • a papermaking method a dry papermaking method, a thick slurry method, and a rolling method can be used to prepare aerosol-generating products.
  • a papermaking method a dry papermaking method, a thick slurry method, and a rolling method can be used to prepare aerosol-generating products.
  • the raw materials of the aerosol-generating product and the preparation steps thereof reference may be made to the content described in the foregoing embodiment.
  • Explosive beads can be implanted into the filter tip section (not limited to this position) of heating non-combustion cigarettes through the filter rod embedding technology (not limited to this technology).
  • the smoker can squeeze the blasted beads to ingest betel nuts Alkali and other substances.
  • Preparation method Weigh the arecoline salt of the above formula weight, add glyceryl caprylate and menthol under stirring, and mix well to prepare.
  • the fire-fighting beads containing Example 1 were implanted into heat-not-burn cigarettes, and the heat-not-burn cigarettes that did not contain fire-fighting beads were used for smoking and sensory quality evaluation: the heat-not-burn cigarettes containing the fire-fighting beads of Example 1 could Ingested arecoline, and produces similar effects of chewing betel nut, with less irritation.
  • the ninth embodiment of the application provides a use of arecoline salt in the manufacture of chewing gum.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.02% to 2%, preferably 0.02% to 1.6%, and more preferably 0.02% to 1.2%, more preferably 0.02% to 1%, still more preferably 0.1% to 1%, still more preferably 0.2% to 1%, still more preferably 0.4% to 1%.
  • the object added to the arecoline salt includes a gum base.
  • the mass percentage of the gum base is 20% to 75%, preferably 20% to 70%, and more preferably 20%. % To 60%, more preferably 20% to 50%, still more preferably 25% to 50%, still more preferably 30% to 50%, still more preferably 35% to 50%, still more preferably 35% to 45%.
  • the object added to the arecoline salt further includes a sweetener.
  • the sweetener is selected from at least one of the following:
  • the mass percentage of the sweetener is 20% to 75%, preferably 20% to 70%, and more preferably 20% to 60%, more preferably 20% to 50%, still more preferably 25% to 50%, still more preferably 25% to 40%, still more preferably 25% to 35%, still more preferably 30% to 35% .
  • the object added to the arecoline salt further includes a filler material.
  • the filler material is selected from at least one of the following:
  • the mass percentage of the filler material when manufacturing the chewing gum, based on the total mass of the raw materials of the chewing gum, is 0.03% to 23%, preferably 0.03% to 20%, and more preferably 0.03%. % To 15%, more preferably 0.03% to 10%, still more preferably 0.5% to 10%, still more preferably 1% to 10%, still more preferably 1.5% to 10%, still more preferably 2% to 8%, More preferably, it is 2% to 6%.
  • the objects added to the arecoline salt further include flavoring agents.
  • the flavoring agent is selected from at least one of the following:
  • Mint spearmint, cinnamon, borneol, flavor.
  • the tenth embodiment of the present application provides a chewing gum whose raw materials include arecoline salt and gum base.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.02% to 2%, preferably 0.02% to 1.6%, more preferably 0.02% to 1.2%, further preferably 0.02 % To 1%, more preferably 0.1% to 1%, still more preferably 0.2% to 1%, still more preferably 0.4% to 1%.
  • the mass percentage of the gum base is 20% to 75%, preferably 20% to 70%, more preferably 20% to 60%, and even more preferably 20% ⁇ 50%, more preferably 25% to 50%, still more preferably 30% to 50%, still more preferably 35% to 50%, still more preferably 35% to 45%.
  • the raw material further includes a sweetener.
  • the sweetener is selected from at least one of the following:
  • the mass percentage of the sweetener is 20% to 75%, preferably 20% to 70%, more preferably 20% to 60%, and even more preferably 20%. % To 50%, more preferably 25% to 50%, still more preferably 25% to 40%, still more preferably 25% to 35%, still more preferably 30% to 35%.
  • the raw material further includes filler materials.
  • the filler material is selected from at least one of the following:
  • the mass percentage of the filler material is 0.03% to 23%, preferably 0.03% to 20%, more preferably 0.03% to 15%, further preferably 0.03% ⁇ 10%, more preferably 0.5% to 10%, still more preferably 1% to 10%, still more preferably 1.5% to 10%, still more preferably 2% to 8%, still more preferably 2% to 6%.
  • the raw materials also include flavoring agents.
  • the flavoring agent is selected from at least one of the following:
  • Mint spearmint, cinnamon, borneol, flavor.
  • Preparation method heat the gum base to 70 ⁇ 105°C, stir in a mixer, add powdered sugar, and let the temperature drop to 60 ⁇ 80°C, then add buffer pair, additives, glucose syrup, arecoline salt, and finally roll into pieces , Forming into finished products.
  • Preparation method heat the gum base to 70 ⁇ 105°C, stir in a mixer, add xylitol and non-sucrose, and let the temperature drop to 60 ⁇ 80°C, then add buffer pair, additives, arecoline salt, and finally roll into pieces , Forming into finished products.
  • the chewing gum prepared by the above preparation method is edible and the sensory quality evaluation is carried out with ordinary chewing gum: the chewing gum prepared by the above preparation method can produce the similar effect of chewing betel nut, has low irritation and good taste. Since the chewing gum does not contain lime powder and cellulose, it avoids the problems of abrasion and irritation of the oral mucosa when chewing betel nuts, and oral diseases.
  • the eleventh embodiment of the present application provides a use of arecoline salt in the preparation of beverages.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.01% to 0.5%, preferably 0.01% to 0.4%, and more preferably 0.01% ⁇ 0.3%, more preferably 0.01% to 0.2%, still more preferably 0.05% to 0.2%.
  • the object added to the arecoline salt includes water.
  • the mass percentage of the water is 75% to 90%.
  • the object added to the arecoline salt further includes functional ingredients.
  • the functional ingredient is selected from at least one of the following:
  • Luo Han Guo juice concentrate natural menthol, licorice juice concentrate, honeysuckle juice concentrate, chrysanthemum extract, kudzu root extract, loquat puree.
  • the mass percentage of the functional ingredient is 0.5% to 2%.
  • the object added to the arecoline salt further includes an acidity regulator.
  • the acidity regulator is selected from at least one of the following:
  • the mass percentage of the acidity regulator is 0.1% to 5%.
  • the object added to the arecoline salt further includes a sweetener.
  • the sweetener is selected from at least one of the following:
  • the mass percentage of the sweetener is 0.5% to 5%.
  • the object added to the arecoline salt further includes an antioxidant.
  • the antioxidant is selected from at least one of the following:
  • Ascorbic acid sodium erythorbate, vitamin C, vitamin E.
  • the mass percentage of the antioxidant when preparing the beverage, based on the total mass of the beverage, is 0.05% to 0.15%.
  • the object added to the arecoline salt when preparing the beverage, further includes a preservative.
  • the preservative is selected from at least one of the following:
  • the mass percentage of the preservative when preparing the beverage, based on the total mass of the beverage, is 0.01% to 0.05%.
  • the objects added to the arecoline salt further include edible flavors.
  • the mass percentage of the edible flavor is 0.5% to 5%.
  • the twelfth embodiment of the present application provides a beverage whose raw materials include arecoline salt and water.
  • the arecoline salt is obtained by neutralizing arecoline and a complex acid.
  • the complex acid of the arecoline salt is selected from at least one of the following:
  • Formic acid acetic acid, propionic acid, butyric acid, isovaleric acid, 2-methylbutanoic acid, valeric acid, 3-methylpentanoic acid, 2-methyl-2-pentenoic acid, trans-2-hexenoic acid, Caproic acid, heptanoic acid, caprylic acid, 2-nonenoic acid, capric acid, dodecanoic acid, myristic acid, palmitic acid, octadecanoic acid, arachidic acid, salicylic acid, oxalic acid, citric acid, sorbic acid, tartaric acid, Adipic acid, hydrochloric acid, hydrobromic acid, glycine, alanine, valine, leucine, isoleucine, methionine (methionine), phenylalanine, proline, tryptophan, Serine, tyrosine, cysteine, methionine, asparagine, glutamine, threonine, aspartic acid
  • the molar ratio of the arecoline to the complexing acid is n; wherein the value range of n is 0 ⁇ n ⁇ 10, preferably 0 ⁇ n ⁇ 8, and more preferably 0 ⁇ n ⁇ 6, more preferably 0 ⁇ n ⁇ 5, still more preferably 0 ⁇ n ⁇ 3, and still more preferably 0 ⁇ n ⁇ 2.
  • the mass percentage of the arecoline salt is 0.01% to 0.5%, preferably 0.01% to 0.4%, more preferably 0.01% to 0.3%, and more preferably It is 0.01% to 0.2%, more preferably 0.05% to 0.2%.
  • the mass percentage of the water is 75% to 90%.
  • the raw material further includes functional ingredients.
  • the functional ingredient is selected from at least one of the following:
  • Luo Han Guo juice concentrate natural menthol, licorice juice concentrate, honeysuckle juice concentrate, chrysanthemum extract, kudzu root extract, loquat puree.
  • the mass percentage of the functional ingredient is 0.5% to 2%.
  • the raw material further includes an acidity regulator.
  • the acidity regulator is selected from at least one of the following:
  • the mass percentage of the acidity regulator is 0.1% to 5%.
  • the raw material further includes a sweetener.
  • the sweetener is selected from at least one of the following:
  • the mass percentage of the sweetener is 0.5% to 5%.
  • the raw material further includes an antioxidant.
  • the antioxidant is selected from at least one of the following:
  • Ascorbic acid sodium erythorbate, vitamin C, vitamin E.
  • the mass percentage of the antioxidant is 0.05% to 0.15%.
  • the raw material also includes a preservative.
  • the preservative is selected from at least one of the following:
  • the mass percentage of the preservative is 0.01% to 0.05%.
  • the raw materials also include food flavors.
  • the mass percentage of the edible flavor is 0.5% to 5%.
  • Preparation method fully mixing arecoline salt with water, honeysuckle concentrated juice, licorice concentrated juice, citric acid, sodium citrate, stevioside, vitamin C, sodium sorbate, and edible essence to prepare a beverage.
  • the beverage prepared by the above preparation method retains various nutrients beneficial to the human body in honeysuckle and licorice.
  • the beverage is rich in arecoline, betel nut polyphenols and other ingredients. Phlegm to relieve cough, relieve emergency and relieve pain and other functions.

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Abstract

一种槟榔风味的制品，包含槟榔碱盐。在制品中应用槟榔碱盐，用户吸食时能够摄取到槟榔碱，并且产生咀嚼槟榔的类似效果，刺激性较低。

Description

槟榔风味的制品
相关申请的交叉参考
本申请权利要求于2020年06月24日提交中国专利局，申请号为202010587899.7，名称为“槟榔风味的制品”的中国专利申请的优先权，其全部内容通过引用结合在本申请中，以及，要求于2020年03月27日提交中国专利局，申请号为202010227895.8，名称为“气溶胶形成基质”的中国专利申请的优先权，其全部内容通过引用结合在本申请中。
技术领域
本申请属于化学合成技术领域，涉及一种槟榔风味的制品。
背景技术
槟榔碱(Arecoline)，化学名“1,2,5,6-四氢-1-甲基-3-吡啶甲酸甲酯”，油状液体，具有拟胆碱作用。槟榔碱是一种有着很大应用价值的化合物，其制备方法及其应用历来为人们所关注。
然而槟榔碱的性质不稳定，而且目前没有商用产品存在，无法确定槟榔碱的转化率，更无法确定是否可让抽吸者达到咀嚼槟榔的效果；另外，尚未发现槟榔碱盐在制品当中的应用。
发明内容
本申请提供一种槟榔风味的制品，所述制品包含槟榔碱盐。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠 檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，所述制品为气溶胶形成基质，用于被雾化以生成供吸食的气溶胶。
在一些实施例中，以气溶胶形成基质的总质量计，其中所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％，更优选的为3％～4％。
在一些实施例中，所述槟榔碱盐为氢溴酸槟榔碱和/或苯甲酸槟榔碱。
在一些实施例中，所述槟榔碱盐的制备方法为：采用乙酸乙酯作为提取剂从槟榔果中提取槟榔碱，调节提取物PH值至7.5～8.5，取乙酸乙酯层，再通过加入氢溴酸或苯甲酸生成槟榔碱盐结晶，所述槟榔碱盐结晶经过重结晶后得到氢溴酸槟榔碱或苯甲酸槟榔碱。
在一些实施例中，所述气溶胶形成基质还包括溶剂和香味剂。
在一些实施例中，所述溶剂包括以下至少之一：
丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，棕榈油，花生油，玉米油，色拉油。
在一些实施例中，所述溶剂包括甘油，且所述气溶胶形成基质中甘油的质量百分比为0～90％。
在一些实施例中，所述所述溶剂包括丙二醇，且所述气溶胶形成基质中丙二醇的质量百分比为9％～99.8％。
在一些实施例中，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
在一些实施方案中，所述气溶胶形成基质为液相，用于采用加热雾化装置、超声波雾化装置、空气压缩式雾化装置、按压式喷雾装置中的任意一种进行雾化以生成气溶胶。
在一些实施方案中，所述气溶胶生成基质为固相，设置为加热到燃点以下时，生成供吸食的气溶胶。
在一些实施方案中，所述制品为用于气溶胶生成制品中的爆珠。
在一些实施方案中，所述制品为口香糖。
在一些实施方案中，所述制品为饮料。
本申请在制品中应用槟榔碱盐，用户吸食时能够摄取到槟榔碱，并且产生咀嚼槟榔的类似效果，刺激性较低。
具体实施方式
本申请将结合以下实施例作进一步描述。
实施方式一：
本申请实施方式一提供一种槟榔碱盐在制备气溶胶形成基质中的用途。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，制备所述气溶胶形成基质时，以所述气溶胶形成基质的总质量计，所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％。
在一些实施方案中，制备所述气溶胶形成基质时，添加到所述槟榔 碱盐中的对象包括溶剂。
在一些实施方案中，所述溶剂选自以下至少之一：
1,2-丙二醇，1,3-丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，甜橙油，柠檬油，薄荷油，棕榈油，花生油，玉米油，色拉油。
在一些实施方案中，所述溶剂包括甘油，且所述甘油的质量百分比为0～90％。
在一些实施方案中，所述溶剂包括丙二醇，且所述丙二醇的质量百分比为9％～99.8％。
在一些实施方案中，添加到所述槟榔碱盐中的对象还包括香味剂。
在一些实施方案中，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、 独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
需要说明的是，香味剂并不限于以上所列出的物质，符合FEMA编码、CAS编码的香味剂都可以适用。
在一些实施方案中，添加到所述槟榔碱盐中的对象不含有尼古丁和/或尼古丁盐。
实施方式二：
本申请实施方式二提供一种气溶胶形成基质，所述气溶胶形成基质包括：
槟榔碱盐；
溶剂；
任选地香味剂。
优选的，以气溶胶形成基质的总质量计，其中所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～12％，进一步优选为2％～10％，进一步优选为2％～8％，进一步优选为2％～5％，进一步优选为2％～4％，进一步优选为2％～3％，更优选的为3％～4％。
优选的，所述槟榔碱盐的配合酸包括以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，苯甲酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
优选的，所述槟榔碱盐为氢溴酸槟榔碱和/或苯甲酸槟榔碱。
优选的，所述槟榔碱盐由从槟榔果中提取出来的槟榔碱与所述配合酸中和得到。
优选的，所述槟榔碱盐为氢溴酸槟榔碱或苯甲酸槟榔碱盐，制备方法为：采用乙酸乙酯作为提取剂从槟榔果中提取槟榔碱，调节提取物PH值至7.5～8.5，取乙酸乙酯层，再通过加入氢溴酸或苯甲酸生成槟榔碱盐结晶，所述槟榔碱盐结晶经过重结晶后得到氢溴酸槟榔碱或苯甲酸槟榔碱。
优选的，所述溶剂包括以下至少之一：
丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，棕榈油，花生油，玉米油，色拉油。
优选的，所述溶剂包括甘油，且所述气溶胶形成基质中甘油的质量百分比为0～90％，优选的为0％～80％，进一步优选为0％～70％，进一步优选为0％～60％，进一步优选为10％～60％，进一步优选为20％～60％，进一步优选为30％～60％，进一步优选为40％～60％，更优选的为50％～60％。
优选的，所述溶剂包括丙二醇，且所述气溶胶形成基质中丙二醇的质量百分比为9％～99.8％，优选的为9％～90％，进一步优选为9％～80％，进一步优选为9％～70％，进一步优选为9％～60％，进一步优选为9％～50％，进一步优选为20％～50％，进一步优选为30％～50％，更优选的为35％～45％。
优选的，所述气溶胶形成基质包括香味剂，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3 (5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
需要说明的是，香味剂并不限于以上所列出的物质，符合FEMA编码、CAS编码的香味剂都可以适用。
实验测试方法：
槟榔碱盐选用氢溴酸槟榔碱。溶剂选择质量比1：1的甘油和丙二醇的混合物。
用抽烟机按照国际标准进行抽吸，并用剑桥滤片收集气溶胶形成基质雾化出来的气溶胶，测试气溶胶中的氢溴酸槟榔碱的质量为m1。再测试剩余气溶胶形成基质中的氢溴酸槟榔碱的质量为m2，气溶胶形成基质中的总氢溴酸槟榔碱的质量为m0，计算转化率k＝m1/(m0-m2)。
其中，涉及到的国际标准可参考：
CORESTA RECOMMENDED METHOD N°81，Afnor standardization XP D90-300-3，International Standard ISO 20768:2018 and PD CEN/TR 17236:2018。
抽吸电子烟的参数如下所示：
Figure PCTCN2021083378-appb-000001
Figure PCTCN2021083378-appb-000002
抽吸体验测试：
气溶胶形成基质经过雾化后，可以从两个方面评测该气溶胶形成基质的抽吸体验：第一方面是抽吸后，抽吸者对吸收槟榔碱盐后的满足感；第二方面，抽吸者摄入过高的槟榔碱盐后会产生不适感。通过多人抽吸评价，并综合两个方面的体验，给不同的气溶胶形成基质按0-5分进行评分，得到抽吸体验较好的实施例。
实验测试结果：
Figure PCTCN2021083378-appb-000003
Figure PCTCN2021083378-appb-000004
从上述实验测试结果可以看出，随着气溶胶形成基质中氢溴酸槟榔碱的含量的提高，转化率成下降趋势，气溶胶形成基质中氢溴酸槟榔碱的含量达到15％时，转化率仍然高于50％。此外，不同氢溴酸槟榔碱含量的气溶胶形成基质在雾化成气溶胶之后，气溶胶中槟榔碱盐含量不同，抽吸者的体验感觉不同，在气溶胶形成基质中槟榔碱盐含量低于0.2％时，抽吸者感觉不到槟榔碱摄入带来的满足感；随着含量升高，满足感提高；超过5％以后，开始出现槟榔碱盐摄入带来的不适感，并且在实验条件下，随含量增加逐渐显现；超过15％含量后，不适感不可接受。
实施方式三：
本申请实施方式三提供一种气溶胶生成系统，包括雾化装置以及实施方式二所述的气溶胶形成基质；
所述雾化装置被配置为对所述气溶胶形成基质进行雾化以形成气溶胶。
在一些实施方案中，所述雾化装置为加热雾化装置。
在一些实施方案中，所述雾化装置为超声波雾化装置。
在一些实施方案中，所述气溶胶形成基质包括槟榔碱盐、甘油以及丙二醇。
在一些实施方案中，所述超声波雾化装置的振荡频率大于1MHz。
在一些实施方案中，所述雾化装置为空气压缩式雾化装置或者按压式喷雾装置。
在一些实施方案中，所述气溶胶形成基质包括槟榔碱盐、乙醇以及水。
实施方式四：
本申请实施方式四提供一种槟榔碱盐在制造气溶胶生成制品中的 用途。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，制造所述气溶胶生成制品时，以所述气溶胶生成制品的原料的总质量计，所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％，更优选的为3％～4％。
在一些实施方案中，制造所述气溶胶生成制品时，添加到所述槟榔碱盐中的对象包括：雾化剂、粘合剂以及植物纤维。
在一些实施方案中，制造所述气溶胶生成制品时，以所述气溶胶生成制品的原料的总质量计，所述雾化剂的质量百分比为5％～30％，优选的为10％～30％，进一步优选为10％～25％，进一步优选为15％～25％。
在一些实施方案中，所述雾化剂选自以下至少之一：
1,2-丙二醇，1,3-丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，甜橙油，柠檬油，薄荷油，棕榈油，花生油，玉米油，色拉油。
在一些实施方案中，制造所述气溶胶生成制品时，以所述气溶胶生成制品的原料的总质量计，所述粘合剂的质量百分比为1％～20％，优选的 为1％～15％，进一步优选为1％～10％，进一步优选为3％～10％，进一步优选为5％～10％。
在一些实施方案中，所述粘合剂选自以下至少之一：
羧甲基纤维素、羟丙基甲基纤维素、聚乙烯醇、松香、黄原胶、阿拉伯胶、瓜尔胶、壳聚糖、果胶、刺槐豆胶、淀粉、海藻酸钠、虫胶。
在一些实施方案中，制造所述气溶胶生成制品时，以所述气溶胶生成制品的原料的总质量计，所述植物纤维的质量百分比为40％～80％，优选的为40％～70％，进一步优选为50％～70％，进一步优选为50％～65％，进一步优选为50％～60％。
在一些实施方案中，所述植物纤维选自以下至少之一：
槟榔纤维、木浆纤维、麻浆纤维、棉浆纤维、蔗渣浆纤维、竹浆纤维、椰子浆纤维。
在一些实施方案中，添加到所述槟榔碱盐中的对象还包括香味剂。
在一些实施方案中，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香 花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
需要说明的是，香味剂并不限于以上所列出的物质，符合FEMA编码、CAS编码的香味剂都可以适用。
在一些实施方案中，添加到所述槟榔碱盐中的对象不含有烟草成分。
在一些实施方案中，制造所述气溶胶生成制品的方法包括造纸法、干法造纸法、稠浆法、辊压法中的一种。
实施方式五：
本申请实施方式五提供一种气溶胶生成制品，其原料包括槟榔碱盐、雾化剂、粘合剂以及植物纤维。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，以原料的总质量计，所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％，更优选的为3％～4％。
在一些实施方案中，以原料的总质量计，所述雾化剂的质量百分比为5％～30％，优选的为10％～30％，进一步优选为10％～25％，进一步优选为15％～25％。
在一些实施方案中，所述雾化剂选自以下至少之一：
1,2-丙二醇，1,3-丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，甜橙油，柠檬油，薄荷油，棕榈油，花生油，玉米油，色拉油。
在一些实施方案中，以原料的总质量计，所述粘合剂的质量百分比为1％～20％，优选的为1％～15％，进一步优选为1％～10％，进一步优选为3％～10％，进一步优选为5％～10％。
在一些实施方案中，所述的粘合剂选自以下至少之一：
羧甲基纤维素、羟丙基甲基纤维素、聚乙烯醇、松香、黄原胶、阿拉伯胶、瓜尔胶、壳聚糖、果胶、刺槐豆胶、淀粉、海藻酸钠、虫胶。
在一些实施方案中，以原料的总质量计，所述植物纤维的质量百分比为40％～80％，优选的为40％～70％，进一步优选为50％～70％，进一步优选为50％～65％，进一步优选为50％～60％。
在一些实施方案中，所述植物纤维选自以下至少之一：
槟榔纤维、木浆纤维、麻浆纤维、棉浆纤维、蔗渣浆纤维、竹浆纤维、椰子浆纤维。
在一些实施方案中，所述原料还包括香味剂。
在一些实施方案中，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲 酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
需要说明的是，香味剂并不限于以上所列出的物质，符合FEMA编码、CAS编码的香味剂都可以适用。
在一些实施方案中，所述原料不含有烟草成分。
实施例1：
按照如下步骤制备加热不燃烧烟支：
步骤1：制备薄片基底。选取槟榔提取物固体残渣，将其浸泡在水中，水温为60～80℃，浸泡时间为0.5～2h，过滤，然后将滤后的固体打浆得到浆液，以重量份计称取浆液50～70份，固体粘合剂3～10份，均匀混合，将混合后的浆料送至抄纸机抄造成型，干燥至含水率约为10～15％，得到薄片基底；
其中，固体粘合剂可以为羧甲基纤维素、羟丙基甲基纤维素、聚乙烯醇、松香、黄原胶、阿拉伯胶、瓜尔胶、壳聚糖、果胶、刺槐豆胶、淀粉、海藻酸钠、虫胶中的一种或者多种。
步骤2：制备涂布液。以重量计称取槟榔碱盐1～50份，香料2～20份，雾化剂40～80份，混合均匀，得到涂布液；
其中，雾化剂为甘油和丙二醇混合物，混合比例为3～5:1。
步骤3：涂布薄片基底。按照步骤1得到的薄片基底重量的25％～40％称取步骤2得到的涂布液，将涂布液喷涂到薄片基底上，在恒温恒湿条件下静置40～60h，得到含槟榔碱盐的植物薄片；
步骤4：制备加热不燃烧烟支。将步骤3得到的植物薄片按尺寸制成烟支棒，将烟支棒与滤嘴连接得到含槟榔碱盐的加热不燃烧烟支。
将上述制备方法制备得到的加热不燃烧烟支，采用气溶胶生成装置(加热方式采用电阻加热)进行加热，采用红外热成像仪测试处于工作状态的发热体表面的温度，测试结果如下表格所示
Figure PCTCN2021083378-appb-000005
从该测试结果可以看出，烟支中的槟榔碱盐在150℃～250℃之间能够雾化并生成可吸食的气溶胶。
与普通的加热不燃烧烟支进行抽吸和感官质量评价：上述制备方法制备得到的加热不燃烧烟支，能够摄取到槟榔碱，并且产生咀嚼槟榔的类似效果，刺激性较低。
实施方式六：
本申请实施方式六提供一种槟榔碱盐在制备爆珠的液体组合物中的用途；其中，所述爆珠包括易碎壳体和所述液体组合物，所述液体组合物设置在所述易碎壳体内。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬 氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，以液体组合物的总质量计，所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％，更优选的为3％～4％。
在一些实施方案中，制备所述液体组合物时，添加到所述槟榔碱盐中的对象包括雾化剂。
在一些实施方案中，以液体组合物的总质量计，所述雾化剂的质量百分比为5％～30％，优选的为10％～30％，进一步优选为10％～25％，进一步优选为15％～25％。
在一些实施方案中，所述雾化剂选自以下至少之一：
1,2-丙二醇，1,3-丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，甜橙油，柠檬油，薄荷油，棕榈油，花生油，玉米油，色拉油。
在一些实施方案中，添加到所述槟榔碱盐中的对象还包括香味剂。
在一些实施方案中，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、 苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
需要说明的是，香味剂并不限于以上所列出的物质，符合FEMA编码、CAS编码的香味剂都可以适用。
在一些实施方案中，添加到所述槟榔碱盐中的对象不含有尼古丁和/或尼古丁盐。
在一些实施方案中，所述爆珠植入在气溶胶生成制品中。
在一些实施方案中，所述气溶胶生成制品的原料不含有烟草成分。
实施方式七：
本申请实施方式七提供一种爆珠，包括易碎壳体和液体组合物，所述液体组合物设置在所述易碎壳体内；
其中，所述液体组合物包括槟榔碱盐以及雾化剂。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸， 癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，以液体组合物的总质量计，其中所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％，更优选的为3％～4％。
在一些实施方案中，以液体组合物的总质量计，所述雾化剂的质量百分比为5％～30％，优选的为10％～30％，进一步优选为10％～25％，进一步优选为15％～25％。
在一些实施方案中，所述雾化剂选自以下至少之一：
1,2-丙二醇，1,3-丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，甜橙油，柠檬油，薄荷油，棕榈油，花生油，玉米油，色拉油。
在一些实施方案中，所述液体组合物还包括香味剂。
在一些实施方案中，所述香味剂选自以下至少之一：
橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、 苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
需要说明的是，香味剂并不限于以上所列出的物质，符合FEMA编码、CAS编码的香味剂都可以适用。
在一些实施方案中，所述液体组合物不含有尼古丁和/或尼古丁盐。
实施方式八：
本申请实施方式八提供一种气溶胶生成制品，包括实施方式七所述的爆珠。
在一些实施方案中，所述气溶胶生成制品的原料不含有烟草成分。
在该实施方式中，可以采用造纸法、干法造纸法、稠浆法、辊压法制备气溶胶生成制品。具体地，所述气溶胶生成制品的原料及其制备步骤，可参考前述实施方式所述内容。
爆珠可通过滤棒嵌珠技术(并不限于此技术)植入加热不燃烧烟支的滤嘴段(并不限于此位置)，在使用时，抽吸者可挤破爆珠来摄取槟榔碱等物质。
需要说明的是，在该实施方式中，对易碎壳体的成分及其制备工艺、 以及爆珠的制备工艺没有特殊的限制，可采用本领域技术人员熟知的技术即可。
实施例1：
按照如下配方制备爆珠中的液体组合物：
槟榔碱盐10wt％、辛癸酸甘油酯80wt％、薄荷脑10wt％。
制备方法：称取如上配方重量的槟榔碱盐，在搅拌下加入辛癸酸甘油酯、薄荷脑，混匀后制成。
将含有实施例1的爆珠植入加热不燃烧烟支，与未含有爆珠的加热不燃烧烟支进行抽吸和感官质量评价：含有实施例1的爆珠的加热不燃烧烟支，能够摄取到槟榔碱，并且产生咀嚼槟榔的类似效果，刺激性较低。
实施方式九：
本申请实施方式九提供一种槟榔碱盐在制造口香糖中的用途。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，制造所述口香糖时，以所述口香糖的原料的总质量计，所述槟榔碱盐的质量百分比为0.02％～2％，优选的为0.02％～1.6％， 进一步优选为0.02％～1.2％，进一步优选为0.02％～1％，进一步优选为0.1％～1％，进一步优选为0.2％～1％，进一步优选为0.4％～1％。
在一些实施方案中，制造所述口香糖时，添加到所述槟榔碱盐中的对象包括胶基。
在一些实施方案中，制造所述口香糖时，以所述口香糖的原料的总质量计，所述胶基的质量百分比为20％～75％，优选的为20％～70％，进一步优选为20％～60％，进一步优选为20％～50％，进一步优选为25％～50％，进一步优选为30％～50％，进一步优选为35％～50％，进一步优选为35％～45％。
在一些实施方案中，添加到所述槟榔碱盐中的对象还包括甜味剂。
在一些实施方案中，所述甜味剂选自以下至少之一：
白砂糖、冰糖、蔗糖、麦芽糖、玉米糖浆、葡糖糖浆、果糖、麦芽糊精、聚葡萄糖、木糖醇、山梨醇、麦芽糖醇、赤藻糖醇、阿斯巴甜、安赛蜜、三氯蔗糖、甜菊苷、纽甜。
在一些实施方案中，制造所述口香糖时，以所述口香糖的原料的总质量计，所述甜味剂的质量百分比为20％～75％，优选的为20％～70％，进一步优选为20％～60％，进一步优选为20％～50％，进一步优选为25％～50％，进一步优选为25％～40％，进一步优选为25％～35％，进一步优选为30％～35％。
在一些实施方案中，添加到所述槟榔碱盐中的对象还包括填料材料。
在一些实施方案中，所述填料材料选自以下至少之一：
碳酸钠，碳酸氢钠，碳酸钾，碳酸钙、磷酸二钙、磷酸二氢钠。
在一些实施方案中，制造所述口香糖时，以所述口香糖的原料的总质量计，所述填料材料的质量百分比为0.03％～23％，优选的为0.03％～20％，进一步优选为0.03％～15％，进一步优选为0.03％～10％，进一步优选为0.5％～10％，进一步优选为1％～10％，进一步优选为1.5％～10％，进一步优选为2％～8％，进一步优选为2％～6％。
在一些实施方案中，添加到所述槟榔碱盐中的对象还包括调味剂。
在一些实施方案中，所述调味剂选自以下至少之一：
薄荷、留兰香、肉桂、冰片、香精。
实施方式十：
本申请实施方式十提供一种口香糖，其原料包括槟榔碱盐以及胶基。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，以原料的总质量计，所述槟榔碱盐的质量百分比为0.02％～2％，优选的为0.02％～1.6％，进一步优选为0.02％～1.2％，进一步优选为0.02％～1％，进一步优选为0.1％～1％，进一步优选为0.2％～1％，进一步优选为0.4％～1％。
在一些实施方案中，以原料的总质量计，所述胶基的质量百分比为20％～75％，优选的为20％～70％，进一步优选为20％～60％，进一步优选为20％～50％，进一步优选为25％～50％，进一步优选为30％～50％，进一步优选为35％～50％，进一步优选为35％～45％。
在一些实施方案中，所述原料还包括甜味剂。
在一些实施方案中，所述甜味剂选自以下至少之一：
白砂糖、冰糖、蔗糖、麦芽糖、玉米糖浆、葡糖糖浆、果糖、麦芽糊精、聚葡萄糖、木糖醇、山梨醇、麦芽糖醇、赤藻糖醇、阿斯巴甜、 安赛蜜、三氯蔗糖、甜菊苷、纽甜。
在一些实施方案中，以原料的总质量计，所述甜味剂的质量百分比为20％～75％，优选的为20％～70％，进一步优选为20％～60％，进一步优选为20％～50％，进一步优选为25％～50％，进一步优选为25％～40％，进一步优选为25％～35％，进一步优选为30％～35％。
在一些实施方案中，所述原料还包括填料材料。
在一些实施方案中，所述填料材料选自以下至少之一：
碳酸钠，碳酸氢钠，碳酸钾，碳酸钙、磷酸二钙、磷酸二氢钠。
在一些实施方案中，以原料的总质量计，所述填料材料的质量百分比为0.03％～23％，优选的为0.03％～20％，进一步优选为0.03％～15％，进一步优选为0.03％～10％，进一步优选为0.5％～10％，进一步优选为1％～10％，进一步优选为1.5％～10％，进一步优选为2％～8％，进一步优选为2％～6％。
在一些实施方案中，所述原料还包括调味剂。
在一些实施方案中，所述调味剂选自以下至少之一：
薄荷、留兰香、肉桂、冰片、香精。
实施例1：
按照如下配方制备口香糖：
胶基54wt％，糖粉23wt％，葡萄糖浆14wt％，碳酸钾4wt％，薄荷调味剂3wt％，薄荷醇1wt％，槟榔碱盐1wt％。
制备方法：将胶基加热至70～105℃，放入搅拌机中搅拌，加入糖粉，并让温度降至60～80℃，再加入缓冲对，添加剂，葡萄糖浆，槟榔碱盐，最后轧片，成型制成成品。
实施例2：
按照如下配方制备木糖醇口香糖：
胶基54wt％，木糖醇23wt％，非蔗糖14wt％，碳酸钾4wt％，薄荷调味剂3wt％，薄荷醇1wt％，槟榔碱盐1wt％。
制备方法：将胶基加热至70～105℃，放入搅拌机中搅拌，加入木糖醇和非蔗糖，并让温度降至60～80℃，再加入缓冲对，添加剂，槟榔碱盐，最后轧片，成型制成成品。
将上述制备方法制备得到的口香糖，与普通的口香糖进行食用和感官质量评价：上述制备方法制备得到的口香糖，能够产生咀嚼槟榔的类似效果，刺激性低，口感较好。由于该口香糖不含有石灰粉和纤维素，避免了咀嚼槟榔时存在的口腔黏膜的磨损和刺激、诱发口腔疾病的问题。
实施方式十一：
本申请实施方式十一提供一种槟榔碱盐在制备饮料中的用途。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述槟榔碱盐的质量百分比为0.01％～0.5％，优选的为0.01％～0.4％，进一步优选为0.01％～0.3％，进一步优选为0.01％～0.2％，进一步优选为0.05％～0.2％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象包括水。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述水的质量百分比为75％～90％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象还包括功能性成分。
在一些实施方案中，所述功能性成分选自以下至少之一：
罗汉果浓缩汁、天然薄荷脑、甘草浓缩汁、金银花浓缩汁、菊花提取液、葛根提取液、枇杷原浆。
在一些实施方案中，以所述饮料的总质量计，所述功能性成分的质量百分比为0.5％～2％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象还包括酸度调节剂。
在一些实施方案中，所述酸度调节剂选自以下至少之一：
酒石酸、苹果酸、柠檬酸、柠檬酸钠。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述酸度调节剂的质量百分比为0.1％～5％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象还包括甜味剂。
在一些实施方案中，所述甜味剂选自以下至少之一：
白砂糖、冰糖、蔗糖、麦芽糖、玉米糖浆、葡糖糖浆、果糖、麦芽糊精、聚葡萄糖、木糖醇、山梨醇、麦芽糖醇、赤藻糖醇、阿斯巴甜、安赛蜜、三氯蔗糖、甜菊苷、纽甜。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述甜味剂的质量百分比为0.5％～5％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象还包括抗氧化剂。
在一些实施方案中，所述抗氧化剂选自以下至少之一：
抗坏血酸、异抗坏血酸钠、维生素C、维生素E。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述抗氧化剂的质量百分比为0.05％～0.15％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象还包括防腐剂。
在一些实施方案中，所述防腐剂选自以下至少之一：
苯甲酸钠、山梨酸钠、山梨酸钾。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述防腐剂的质量百分比为0.01％～0.05％。
在一些实施方案中，制备所述饮料时，添加到所述槟榔碱盐中的对象还包括食用香精。
在一些实施方案中，制备所述饮料时，以所述饮料的总质量计，所述食用香精的质量百分比为0.5％～5％。
实施方式十二：
本申请实施方式十二提供一种饮料，其原料包括槟榔碱盐以及水。
在一些实施方案中，所述槟榔碱盐由槟榔碱与配合酸中和得到。
在一些实施方案中，所述槟榔碱盐的配合酸选自以下至少之一：
甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
在一些实施方案中，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
在一些实施方案中，以所述饮料的总质量计，所述槟榔碱盐的质量百分比为0.01％～0.5％，优选的为0.01％～0.4％，进一步优选为0.01％～0.3％，进一步优选为0.01％～0.2％，进一步优选为0.05％～0.2％。
在一些实施方案中，以所述饮料的总质量计，所述水的质量百分比为75％～90％。
在一些实施方案中，所述原料还包括功能性成分。
在一些实施方案中，所述功能性成分选自以下至少之一：
罗汉果浓缩汁、天然薄荷脑、甘草浓缩汁、金银花浓缩汁、菊花提取液、葛根提取液、枇杷原浆。
在一些实施方案中，所述功能性成分的质量百分比为0.5％～2％。
在一些实施方案中，所述原料还包括酸度调节剂。
在一些实施方案中，所述酸度调节剂选自以下至少之一：
酒石酸、苹果酸、柠檬酸、柠檬酸钠。
在一些实施方案中，所述酸度调节剂的质量百分比为0.1％～5％。
在一些实施方案中，所述原料还包括甜味剂。
在一些实施方案中，所述甜味剂选自以下至少之一：
白砂糖、冰糖、蔗糖、麦芽糖、玉米糖浆、葡糖糖浆、果糖、麦芽糊精、聚葡萄糖、木糖醇、山梨醇、麦芽糖醇、赤藻糖醇、阿斯巴甜、安赛蜜、三氯蔗糖、甜菊苷、纽甜。
在一些实施方案中，所述甜味剂的质量百分比为0.5％～5％。
在一些实施方案中，所述原料还包括抗氧化剂。
在一些实施方案中，所述抗氧化剂选自以下至少之一：
抗坏血酸、异抗坏血酸钠、维生素C、维生素E。
在一些实施方案中，所述抗氧化剂的质量百分比为0.05％～0.15％。
在一些实施方案中，所述原料还包括防腐剂。
在一些实施方案中，所述防腐剂选自以下至少之一：
苯甲酸钠、山梨酸钠、山梨酸钾。
在一些实施方案中，所述防腐剂的质量百分比为0.01％～0.05％。
在一些实施方案中，所述原料还包括食用香精。
在一些实施方案中，所述食用香精的质量百分比为0.5％～5％。
实施例1：
按照如下配方制备饮料：
槟榔碱盐0.1wt％，水88wt％，金银花浓缩汁1wt％，甘草浓缩汁1wt％，柠檬酸2wt％，柠檬酸钠2wt％，甜菊糖苷3wt％，维生素C0.05wt％，山梨酸 钠0.05wt％，食用香精2.8wt％。
制备方法：将槟榔碱盐与水、金银花浓缩汁、甘草浓缩汁、柠檬酸、柠檬酸钠、甜菊糖苷、维生素C、山梨酸钠、食用香精充分混合，调制成饮料。
上述制备方法制备得到的饮料，保留了金银花、甘草中有利于人体的多种营养物质，饮料中富含槟榔碱、槟榔多酚等成分，饮料口感好，具有补脾益气、清热解毒、祛痰止咳、缓急止痛等多种功效。
本书面描述使用实例来公开本申请，包括最佳模式，且还使本领域技术人员能够制造和使用本申请。本申请的可授予专利的范围由权利要求书限定，且可以包括本领域技术人员想到的其它实例。如果这种其它实例具有不异于权利要求书的字面语言的结构元素，或者如果这种其它实例包括与权利要求书的字面语言无实质性差异的等效结构元素，则这种其它实例旨在处于权利要求书的范围之内。在不会造成不一致的程度下，通过参考将本文中参考的所有引用之处并入本文中。

Claims (18)

  1. 一种槟榔风味的制品，其特征在于，所述制品包含槟榔碱盐。
  2. 根据权利要求1所述的制品，其特征在于，所述槟榔碱盐由槟榔碱与配合酸中和得到。
  3. 根据权利要求2所述的制品，其特征在于，所述槟榔碱盐的配合酸选自以下至少之一：
    甲酸，乙酸，丙酸，丁酸，异戊酸，2-甲基丁酸，戊酸，3-甲基戊酸，2-甲基-2-戊烯酸，反-2-己烯酸，己酸，庚酸，辛酸，2-壬烯酸，癸酸，十二酸，十四酸，十六酸，十八酸，花生酸，水杨酸，草酸，柠檬酸，山梨酸，酒石酸，己二酸，盐酸，氢溴酸，甘氨酸，丙氨酸，缬氨酸，亮氨酸，异亮氨酸，甲硫氨酸(蛋氨酸)，苯丙氨酸，脯氨酸，色氨酸，丝氨酸，酪氨酸，半胱氨酸，蛋氨酸，天冬酰胺，谷氨酰胺，苏氨酸，天冬氨酸，谷氨酸，赖氨酸，精氨酸，组氨酸。
  4. 根据权利要求1-3任一所述的制品，其特征在于，所述槟榔碱与所述配合酸的摩尔比为n；其中，所述n的取值范围为0＜n≤10，优选的为0＜n≤8，进一步优选的为0＜n≤6，进一步优选的为0＜n≤5，进一步优选的为0＜n≤3，进一步优选的为0＜n≤2。
  5. 根据权利要求1-4任一所述的制品，其特征在于，所述制品为气溶胶形成基质，用于被雾化以生成供吸食的气溶胶。
  6. 根据权利要求5所述的制品，其特征在于，以气溶胶形成基质的总质量计，其中所述槟榔碱盐的质量百分比为0.2％～15％，优选的为1％～15％，进一步优选为2％～15％，进一步优选为2％～10％，进一步优选为2％～5％，进一步优选为2％～4％，更优选的为3％～4％。
  7. 根据权利要求6所述的制品，其特征在于，所述槟榔碱盐为氢溴 酸槟榔碱和/或苯甲酸槟榔碱。
  8. 根据权利要求7所述的制品，其特征在于，所述槟榔碱盐的制备方法为：采用乙酸乙酯作为提取剂从槟榔果中提取槟榔碱，调节提取物PH值至7.5～8.5，取乙酸乙酯层，再通过加入氢溴酸或苯甲酸生成槟榔碱盐结晶，所述槟榔碱盐结晶经过重结晶后得到氢溴酸槟榔碱或苯甲酸槟榔碱。
  9. 根据权利要求5所述的制品，其特征在于，所述气溶胶形成基质还包括溶剂和香味剂。
  10. 根据权利要求9所述的制品，其特征在于，所述溶剂包括以下至少之一：
    丙二醇，甘油，聚乙二醇200，聚乙二醇400，二丙二醇缩醚，乙醇，水，柠檬酸三乙酯，三醋酸甘油酯，辛癸酸甘油酯，异丙醇，棕榈油，花生油，玉米油，色拉油。
  11. 根据权利要求10所述的制品，其特征在于，所述溶剂包括甘油，且所述气溶胶形成基质中甘油的质量百分比为0～90％。
  12. 根据权利要求10所述的制品，其特征在于，所述所述溶剂包括丙二醇，且所述气溶胶形成基质中丙二醇的质量百分比为9％～99.8％。
  13. 根据权利要求9所述的制品，其特征在于，所述香味剂选自以下至少之一：
    橙花醇、反2-己烯醇、芳樟醇、苯甲醇、1-己醇、叶醇、alpha-松油醇、香茅醇、beta-苯乙醇、氧化芳樟醇、香叶醇、异戊醇、辛醇、己醇、癸醇、肉桂醇、庚醇、丁香酚、麦芽酚、乙基麦芽酚、百里香酚、异丁香酚、2-甲基丁酸、苹果酸、正戊酸、正己酸、食用乙酸、正辛酸、草莓酸、丁酸、柠檬酸、丙酸、3-甲基戊酸、异戊酸、乙酸异戊酯、甲酸戊酯、甲酸香叶酯、甲酸丁酯、甲酸苄酯、甲酸叶醇酯、丙位癸内酯、 丁位壬内酯、丙位辛内酯、丙位庚内酯、丙位十一内酯、丁位十二内酯、苯甲醛、草莓醛、肉桂醛、糠醛、柠檬醛、乙醛、3-甲硫基丙醛、天然3-巯基-2-甲基戊醛、异丁醛、反-2-辛烯醛、反-2-壬烯醛、反-2-癸烯醛、反,反-2,4-庚二烯醛、2,5-二甲基吡嗪、2-乙酰基呋喃、2-乙基-3(5或6)-二甲基吡嗪、2,3,5,6-四甲基吡嗪、2,3,5-三甲基吡嗪、2-乙酰基吡嗪、苯乙酮、beta-紫罗兰酮、突厥烯酮2号(芬美意)、丁二酮、甲位紫罗兰酮、乙偶姻(乙酰基甲基原醇)、乙偶姻(乙酰基甲基原醇)、甲基庚烯酮、香兰素、乙基香兰素、二氢香豆素、覆盆子酮、大茴香醚、甲基柏木醚、甲基-2-甲基-3-呋喃基二硫醚、冬青油、丁香花蕾油、十倍甜橙油、玫瑰木油、香叶油、苦杏仁油、丁香罗勒油、乙基香兰素、二氢香豆素、覆盆子酮、浓馥香兰素、吐鲁浸膏、秘鲁浸膏、橡木提取物、浓咖啡超临界萃取提取物(水溶)、可可提取物、咖啡酊、独活酊、香兰提取物、香草提取物、赖百当浸膏、鸢尾油或浸膏、茉莉浸膏、树苔浸膏(琥珀香)、罗望子提取物、津巴布韦烟提取物、烟草精油、白肋烟提取物、烤烟净油A、烤烟头香提取物、晒烟头香提取物。
  14. 根据权利要求5-13任一项所述的制品，其特征在于，所述气溶胶形成基质为液相，用于采用加热雾化装置、超声波雾化装置、空气压缩式雾化装置、按压式喷雾装置中的任意一种进行雾化以生成气溶胶。
  15. 根据权利要求5-13任一项所述的制品，其特征在于，所述气溶胶生成基质为固相，设置为加热到燃点以下时，生成供吸食的气溶胶。
  16. 根据权利要求1-4任一所述的制品，其特征在于，所述制品为用于气溶胶生成制品中的爆珠。
  17. 根据权利要求1-4任一所述的制品，其特征在于，所述制品为口香糖。
  18. 根据权利要求1-4任一所述的制品，其特征在于，所述制品为饮 料。
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