WO2021119900A1 - Pneumatic tray for gan material growth - Google Patents

Pneumatic tray for gan material growth Download PDF

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Publication number
WO2021119900A1
WO2021119900A1 PCT/CN2019/125531 CN2019125531W WO2021119900A1 WO 2021119900 A1 WO2021119900 A1 WO 2021119900A1 CN 2019125531 W CN2019125531 W CN 2019125531W WO 2021119900 A1 WO2021119900 A1 WO 2021119900A1
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WO
WIPO (PCT)
Prior art keywords
disk
tray
center
master
gan material
Prior art date
Application number
PCT/CN2019/125531
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French (fr)
Chinese (zh)
Inventor
黄业
刘鹏
王健辉
卢敬权
Original Assignee
东莞市中镓半导体科技有限公司
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Application filed by 东莞市中镓半导体科技有限公司 filed Critical 东莞市中镓半导体科技有限公司
Priority to PCT/CN2019/125531 priority Critical patent/WO2021119900A1/en
Publication of WO2021119900A1 publication Critical patent/WO2021119900A1/en

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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/458Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for supporting substrates in the reaction chamber
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/12Substrate holders or susceptors
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere

Definitions

  • This application relates to the technical field of GaN material growth devices, for example, to a pneumatic tray for GaN material growth.
  • GaN Gallium nitride
  • HVPE Hydride vapor phase epitaxy
  • the key factors include the need to obtain a stable laminar flow field in the HVPE reaction chamber and the provision of trays that can rotate at a high temperature of not less than 800°C.
  • the rotation of the tray is realized by a traditional motor, and it is difficult to obtain a stable rotation speed due to the limitation of high temperature in the process environment.
  • the existing connection gap between the composite structure of the daughter disk and the master disk is easy to grow GaN polycrystalline. With the process time, the GaN polycrystalline will become thicker and thicker, which will eventually lead to the integration of the daughter disk and the master disk. Rotation, which in turn leads to process failure.
  • the present application provides a pneumatic tray for GaN material growth, which can be used under high temperature conditions without disturbing the reaction conditions of the reaction gas above the tray.
  • a pneumatic tray for GaN material growth comprising a sub-disk and a master disk.
  • the upper surface of the master disk is provided with a disk position for placing the sub-disk, and the disk position is provided with a position close to the center of the disk position.
  • a spiral groove extending to the edge of the disk position, one end of the groove close to the center of the disk position communicates with the air source, and the other end of the groove communicates with the outside.
  • the sub-disk and the mother-disk are made of graphite, ceramic or quartz materials.
  • the upper surface of the sub-disk is provided with workpiece grooves for placing the substrate, and the number of the workpiece grooves is 1 or more and 10 or less.
  • the outer peripheral edge of the sub-disk extends downward to form a guide boss, the guide boss is located on the outer side of the side wall of the bay, and an opening is formed between the guide boss and the side wall of the bay and faces downward The exhaust port.
  • the center of the disk position is located at the center of the master disk, the guide boss is wrapped around the outer side of the side wall of the master disk, and the end of the groove away from the center of the disk position passes through the exhaust port Connect with the outside world.
  • the number of the bays is one.
  • the center of the disk position is deviated from the center of the master disk, an air storage cavity is provided on the master disk around the disk position, and the side of the air storage cavity away from the center of the master disk penetrates the master disk
  • An edge gap is formed on the side wall of the groove; the end of the groove away from the center of the disk position communicates with the air storage cavity through the exhaust port, and communicates with the outside through an edge gap provided on the air storage cavity.
  • the number of the bays is one, and the bays are eccentrically arranged with the mother disk; or,
  • the number of the disk positions is at least two, and the at least two disk positions are equally spaced along the circumferential direction of the master disk.
  • the number of bays may be five.
  • An exhaust passage is arranged between the air storage cavity and the side wall of the master disk.
  • the exhaust duct is located on both sides of the edge gap.
  • the number of exhaust passages for each disk position is four, and two exhaust passages are respectively provided on both sides of the edge gap.
  • a disk gap is provided between the outer peripheral side wall of the sub disk and the inner side wall of the master disk, and the width of the disk gap is smaller than the width of the air storage cavity.
  • the disc gap can be selected according to the thickness specifications of the GaN single crystal product, and the distance of the disc gap is equal to 1.2 to 2 times the thickness of the GaN single crystal product.
  • An air collection cavity is provided in the middle of the master disk, the air collection cavity is configured to communicate with an external air source, an end of the groove close to the center of the disk position is provided with an air distribution hole, and the air collection cavity Communicate with the vent hole.
  • the master disc includes a disc main body and a disc base fixedly connected, the disc position is arranged on the disc main body, and the air collection cavity is arranged on the middle of the disc base.
  • the disc main body and the disc base have an integral structure or a separate structure.
  • the center of the disk position is provided with a rotating shaft, one end of the rotating shaft is inserted into the center of the sub-disk, and the other end of the rotating shaft is inserted into the mother disk.
  • the rotating shaft is made of graphite, ceramic or quartz material.
  • the bottom of the master plate is connected to one end of a lifting rod, the lifting rod is configured to move up and down, a main air passage is opened in the middle of the lifting rod, and the main air passage is configured to communicate with an external air source, so The main air passage is communicated with the groove through an air collecting cavity and an air distribution hole in sequence.
  • the pneumatic tray also includes a lifting drive mechanism and a rotation drive mechanism.
  • One end of the rotation drive mechanism is connected to the other end of the lifting rod to drive the lifting rod to rotate.
  • the lifting drive mechanism is connected to the rotation drive mechanism.
  • the other end is connected to drive the rotation drive mechanism and the lifting rod to move up and down as a whole; or, one end of the lifting drive mechanism is connected to the other end of the lifting rod to drive the lifting rod to move up and down, and the rotation drive
  • the mechanism is connected with the other end of the lifting drive mechanism to drive the lifting drive mechanism and the lifting rod to rotate integrally.
  • the main air passage communicates with the groove through the air collection cavity.
  • the bottom of the master disk is connected with a lifting rod, the lifting rod is configured to move up and down and horizontally rotate, the middle of the lifting rod is provided with a main air passage communicating with an air source, and the main air passage is connected to the concave The slots are connected.
  • the present application provides a pneumatic tray for GaN material growth, which drives the sub-disk to rotate through airflow.
  • it can overcome the defect that the existing motor drive cannot be used at high temperatures, so that the pneumatic tray can meet high-temperature operating conditions.
  • the inert gas can be discharged in a horizontal direction or a downward sloping direction, thereby avoiding disturbing the upper part of the sub-disk
  • the overall atmosphere of the reaction gas ensures the effective mixing and reaction of the reaction gas.
  • Figure 1 is a full cross-sectional view of the pneumatic tray according to the first embodiment
  • FIG. 2 is a full cross-sectional view of the master disk according to the first embodiment from a top perspective;
  • Figure 3 is a top view of the sub-disk (four-workpiece slot) described in the first embodiment
  • FIG. 4 is a top view of the sub-disk (a workpiece slot) according to the first embodiment
  • Figure 5 is a top view of the pneumatic tray (six trays) described in the third embodiment
  • Figure 6 is a full cross-sectional view of the A-A direction shown in Figure 5;
  • Figure 7 is a front view of the pneumatic tray described in the third embodiment (the tray base is not shown);
  • Figure 8 is a full cross-sectional view of the B-B direction shown in Figure 7;
  • FIG. 9 is a schematic diagram of the structure of the master disk described in the third embodiment.
  • Figure 10 is a top view of the master disk described in the third embodiment.
  • 11 is a top view of the assembly of one of the bays of the master disc and the daughter disc in the third embodiment
  • Fig. 12 is a full cross-sectional view taken along the line C-C shown in Fig. 11;
  • Figure 13 is a top view of the pneumatic tray (five trays) described in the third embodiment
  • Figure 14 is a full cross-sectional view from the direction D-D shown in Figure 13;
  • Figure 15 is a full cross-sectional view of the fourth embodiment based on the A-A direction shown in Figure 5;
  • Fig. 16 is a full cross-sectional view of the fourth embodiment based on the direction D-D shown in Fig. 13.
  • a pneumatic tray for GaN material growth includes a sub-disk 1 and a master disk 2.
  • the sub-disk 1 and the master disk 2 can be made of graphite, ceramic or quartz materials, and the sub-disk 1 is configured
  • the master disk 2 is configured to support the daughter disk 1 and drive the daughter disk 1 to rotate through an inert gas.
  • the upper surface of the master disk 2 is provided with a bay 211 for placing the sub-disk 1, and the bay 211 is provided with a spiral groove 212 extending from a position close to the center of the bay 211 to an edge position of the bay 211.
  • the groove One end of 212 close to the center of the tray 211 is connected to the air source, and the other end of the groove 212 is connected to the outside.
  • the sub-disk 1 is placed on the tray 211, and the inert gas is enclosed between the groove 212 and the sub-disk 1. Circulate in the rotating air channel.
  • a disk position 211 is provided on the master disk 2, and the center of the disk position 211 is located at the center of the master disk 2.
  • the outer peripheral edge of the sub disk 1 extends downward to form a guide boss 11, and the guide boss 11 is located on the disk.
  • On the outer side of the side wall of the position 211 there is a gap between the inner side wall of the guide boss 11 and the side wall of the disk position 211, and the gap forms the exhaust port 3 with the opening facing downward.
  • One end of the location is connected.
  • a rotating shaft 4 is arranged in the center of the disk position 211, and the rotating shaft 4 is made of graphite, ceramic or quartz material. One end of the rotating shaft 4 is inserted into the center of the sub disk 1, and the other end of the rotating shaft 4 is inserted into the center of the bay 211 of the mother disk 2. By providing the rotating shaft 4, the rotation center of the sub-disk 1 can be effectively fixed, and the reliability of the sub-disk 1 in the working process is improved.
  • the master disk 2 includes a disk main body 21 and a disk base 22 that are fixedly connected.
  • the disk main body 21 and the disk base 22 are integrally formed, and the disk position 211 is provided on the disk main body 21.
  • the disk base 22 is provided with an air collecting cavity 221 communicating with an air source, and an end of the groove 212 close to the center of the disk position 211 is provided with an air distribution hole 23, and the air collecting cavity 221 is in communication with the air distribution hole 23.
  • the upper surface of the sub-disk 1 is provided with four workpiece grooves 12 for placing substrates, as shown in FIG. 3.
  • the number of workpiece grooves 12 may be 1 or 2 or 3 or 5 or 6 or 7 or 8 or 9 or 10. The state where the number of workpiece grooves 12 is one is shown in FIG. 4.
  • an external gas source passes the inert gas into the groove 212 through the gas collecting cavity 221 and the gas distribution hole 23, and the inert gas flows in the channel formed by the groove 212 and the sub-disk 1 until the groove 212 is located At one end of the edge position, the inert gas is finally discharged downward along the exhaust port 3.
  • the sub-disk 1 and the mother disk 2 are air-floated and isolated, and the spiral directional airflow drives the sub-disk 1 to rotate. This design drives the sub-disk 1 to rotate through the airflow.
  • the pneumatic tray can meet the working conditions of high temperature greater than 800°C and meet the requirements of the HVPE process.
  • the groove 212 communicates with the outside, so that the inert gas can be discharged in a horizontal direction or a downward oblique direction, so as to avoid disturbing the overall atmosphere of the reaction gas above the sub-disk 1 and ensure the effective mixing and reaction of the reaction gas;
  • the pneumatic tray can also control the speed of the tray in real time by controlling the flow of inert gas, so as to adapt to different product process requirements and improve the quality of material growth.
  • the master disk 2 also includes a lifting rod.
  • the bottom of the master disk 2 is connected to the lifting rod.
  • the lifting rod is made of graphite, ceramic or quartz.
  • the middle of the lifting rod is provided with a main air passage communicating with the air source.
  • the channel communicates with the groove 212 through the gas collecting cavity 221 and the gas distribution hole 23 in sequence.
  • the pneumatic tray also includes a lifting drive mechanism, which is connected with the lifting rod to drive the lifting rod to move up and down.
  • a disk position is arranged on the master disk, and the center of the disk position is deviated from the center of the master disk, that is, the disk position and the master disk are arranged eccentrically.
  • the outer peripheral edge of the sub-disk extends downward to form a guide boss, the guide boss is located on the outer side of the side wall of the disk position, and an air storage cavity is provided on the master disk around the outer circumference of the disk position, so The side of the air storage cavity away from the center of the master disk penetrates through the side wall of the master disk to form an edge gap, and the end of the groove 212 away from the center of the disk position 21 communicates with the air storage cavity and passes through the air storage cavity.
  • the edge gap is connected to the outside world.
  • the inert gas discharged downward from the gap between the inner side wall of the guide boss and the outer side wall of the tray can quickly enter the gas storage cavity and further flow to the place.
  • the edge notch realizes horizontal or oblique downward discharge, away from the reaction gas above the sub-disk, so as to avoid affecting the reaction gas atmosphere and improve the reaction quality of the reaction gas.
  • a disk gap is provided between the outer peripheral side wall of the sub disk and the inner side wall of the master disk.
  • the width of the disk gap is smaller than the width of the air storage cavity.
  • the inert gas mainly tends to flow in the gas storage cavity, rather than a large amount of upward and outward discharge from the disc gap, to ensure the overall atmosphere of the reaction gas; on the other hand, a small amount of inert gas can be left in the disc gap to prevent The reaction gas reacts in the gap between the sub-disk and the mother disk to form a crystal, thereby preventing the sub-disk and the mother disk from being connected as a whole and becoming stuck.
  • the disc gap can be selected according to the thickness specifications of the GaN single crystal product, and the distance of the disc gap is preferably equal to 1.2 to 2 times the thickness of the GaN single crystal product.
  • an exhaust channel is provided between the air storage cavity and the side wall of the master disk, the number of exhaust channels is four, and two exhaust channels are respectively provided on both sides of the edge gap .
  • the pneumatic tray also includes a lifting drive mechanism and a rotation drive mechanism.
  • One end of the rotation drive mechanism is connected to the other end of the lifting rod to drive the lifting rod to rotate.
  • the lifting drive mechanism is connected to the other end of the rotation drive mechanism. Connected to drive the rotating drive mechanism and the lifting rod to move up and down as a whole.
  • the lifting and rotation of the master disk can be realized, so as to adjust the distance between the pneumatic tray and the reaction gas nozzle above, thereby controlling the growth process of GaN material, which can effectively solve the growth problem. Uniformity and growth rate issues.
  • one end of the lifting driving mechanism is connected to the other end of the lifting rod to drive the lifting rod to move up and down
  • the rotation driving mechanism is connected to the other end of the lifting driving mechanism to drive The lifting driving mechanism and the lifting rod rotate integrally.
  • Six bays 211 are provided on the master disk 2, and the six bays 211 are distributed at equal intervals along the circumferential direction of the master disk 2, as shown in FIG. 5. In other embodiments, the number of bays 211 may also be two or three or four or five or seven or eight or nine or ten or more. The state where five bays 211 are set on the master disk 2 is shown in FIG. 13 and FIG. 14.
  • the outer peripheral edge of the sub disk 1 extends downward to form a guide boss 11, which is located on the outside of the side wall of the disk position 211, and the master disk 2 surrounds the disk.
  • An air storage cavity 24 is provided on the outer periphery of the position 211, and the side of the air storage cavity 24 away from the center of the master disk 2 penetrates the side wall of the master disk 2 to form an edge gap 25.
  • the end of the groove 212 provided on the disk position 21 away from the center of the disk position 21 communicates with the air storage cavity 24, and communicates with the outside through the edge gap provided on the air storage cavity.
  • the above design enables the inert gas discharged downward from the gap between the inner side wall of the guide boss 11 and the outer side wall of the tray 211 to quickly enter the gas storage chamber 24 and further flow to the edge gap 25, realizing the horizontal or inclined inert gas
  • the outward discharge in the downward direction is far away from the reaction gas above the sub-disk 1, so as to avoid affecting the reaction gas atmosphere and improve the reaction quality of the reaction gas.
  • a disk gap 5 is provided between the outer peripheral side wall of the sub disk 1 and the inner side wall of the master disk 2.
  • the width of the disk gap 5 is smaller than the width of the air storage cavity 24.
  • it can make the inert gas mainly tend to flow in the gas storage cavity 24, instead of being discharged from the disc gap 5 upwards and outwards in a large amount, so as to ensure the overall atmosphere of the reaction gas; on the other hand, it can make a small amount of inert gas remain in the disc gap 5,
  • the reaction gas is prevented from reacting at the gap between the sub-disk 1 and the mother disk 2 to form crystals, thereby preventing the sub-disk 1 and the mother disk 2 from being integrated and jammed.
  • the disc gap 5 can be selected according to the thickness specifications of the GaN single crystal product, and the distance of the disc gap 5 is preferably equal to 1.2 to 2 times the thickness of the GaN single crystal product.
  • An exhaust duct 26 is provided between the air storage chamber 24 and the side wall of the master disk 2 in this embodiment.
  • Each group of air storage chambers 24 is provided with four exhaust ducts 26, and two exhaust ducts are provided on both sides of the edge gap 25. Road 26.
  • the master disk 2 includes a disk main body 21 and a disk base 22 that are fixedly connected.
  • the disk main body 21 and the disk base 22 are formed as separate parts.
  • the bottom of the master disk 2 is connected to one end of the lifting rod, and the middle of the lifting rod is provided with a main air passage communicating with an air source, and the main air passage communicates with the groove 212 through the air collecting cavity 221 and the air distribution hole 23 .
  • the pneumatic tray includes a lifting drive mechanism and a rotation drive mechanism. One end of the rotation drive mechanism is connected with the other end of the lifting rod to drive the lifting rod to rotate. The lifting drive mechanism is connected with the other end of the rotation drive mechanism to drive the rotation drive mechanism. And the lifting rod moves up and down as a whole.
  • the lifting and rotation of the master disk 2 can be realized, so as to adjust the distance between the pneumatic tray and the upper reactive gas nozzle, and then control the growth process of GaN material, which can effectively solve the growth uniformity and The problem of growth rate.
  • one end of the lifting driving mechanism is connected to the other end of the lifting rod to drive the lifting rod to move up and down
  • the rotation driving mechanism is connected to the other end of the lifting driving mechanism to drive the lifting driving mechanism and the lifting rod to rotate integrally.
  • the master disc 2 includes a disc main body 21 and a disc base 22 that are fixedly connected, and the disc main body 21 and the disc base 22 are integrally formed.
  • five disk positions 211 are provided on the sub disk 1, and the master disk 2 includes a disk main body 21 and a disk base 22 that are fixedly connected.
  • the disk main body 21 and the disk base 22 are integrally formed.
  • the specific structure is shown in FIG. 13 And 16 are shown.

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Abstract

A pneumatic tray for GaN material growth, comprising a sub-tray (1) and a mother tray (2). The upper surface of the mother tray (2) is provided with a tray position (211) for placing the sub-tray (1). The tray position (211) is provided with a spiral groove (212) extending from the position close to the center of the tray position (211) to the edge position of the tray position (211). One end of the groove (212) close to the center of the tray position (211) is communicated with an air source, and the other end of the groove (212) is communicated with the outside by means of the side wall of the mother tray (2).

Description

用于GaN材料生长的气动托盘Pneumatic tray for GaN material growth 技术领域Technical field
本申请涉及GaN材料生长装置技术领域,例如涉及一种用于GaN材料生长的气动托盘。This application relates to the technical field of GaN material growth devices, for example, to a pneumatic tray for GaN material growth.
背景技术Background technique
氮化镓(以下简称GaN)作为最重要的第三代宽禁带半导体材料,被广泛应用于蓝光LED和高温高频大功率电子器件的制备。氢化物气相外延(Hydride vapor phase epitaxy,HVPE)技术作为生长氮化镓(GaN)厚膜材料方法之一,以其生长速率高(最高可达800μm/h),生产成本低,生长工艺简单的特点,非常适合氮化镓(GaN)厚膜生长技术的推广和应用。要推进GaN厚膜的产业化,大批量生产高质量GaN厚膜,其中的关键因素包括HVPE反应室内需要获得稳定的层流流场和提供可以在不低于800℃高温环境下旋转的托盘。现有的以传统电机的方式实现托盘的旋转,在该工艺环境下由于高温的限制,很难获取稳定的转速。另外,现有的子盘与母盘组合结构的连接间隙部分容易生长GaN多晶,随着工艺时长,GaN多晶将越来越厚,最终导致子盘与母盘成一个整体,子盘无法转动,进而导致工艺失败。Gallium nitride (hereinafter referred to as GaN), as the most important third-generation wide-bandgap semiconductor material, is widely used in the preparation of blue LEDs and high-temperature, high-frequency and high-power electronic devices. Hydride vapor phase epitaxy (HVPE) technology is one of the methods for growing gallium nitride (GaN) thick film materials. It has a high growth rate (up to 800μm/h), low production cost, and simple growth process. Features, very suitable for the promotion and application of gallium nitride (GaN) thick film growth technology. To promote the industrialization of GaN thick films and mass-produce high-quality GaN thick films, the key factors include the need to obtain a stable laminar flow field in the HVPE reaction chamber and the provision of trays that can rotate at a high temperature of not less than 800°C. In the prior art, the rotation of the tray is realized by a traditional motor, and it is difficult to obtain a stable rotation speed due to the limitation of high temperature in the process environment. In addition, the existing connection gap between the composite structure of the daughter disk and the master disk is easy to grow GaN polycrystalline. With the process time, the GaN polycrystalline will become thicker and thicker, which will eventually lead to the integration of the daughter disk and the master disk. Rotation, which in turn leads to process failure.
发明内容Summary of the invention
本申请提供一种用于GaN材料生长的气动托盘,能够在高温条件下使用,且不会干扰托盘上方反应气体的反应条件。The present application provides a pneumatic tray for GaN material growth, which can be used under high temperature conditions without disturbing the reaction conditions of the reaction gas above the tray.
一种用于GaN材料生长的气动托盘,包括子盘和母盘,所述母盘的上表面设置有用于放置所述子盘的盘位,所述盘位上设置有由靠近盘位中心位置延伸至盘位边缘位置的螺旋状的凹槽,所述凹槽靠近所述盘位的中心的一端与气源连通,所述凹槽的另一端与外界连通。A pneumatic tray for GaN material growth, comprising a sub-disk and a master disk. The upper surface of the master disk is provided with a disk position for placing the sub-disk, and the disk position is provided with a position close to the center of the disk position. A spiral groove extending to the edge of the disk position, one end of the groove close to the center of the disk position communicates with the air source, and the other end of the groove communicates with the outside.
所述子盘和母盘是石墨、陶瓷或石英材料。The sub-disk and the mother-disk are made of graphite, ceramic or quartz materials.
所述子盘的上表面设置有用于放置衬底的工件槽,所述工件槽的数量是1个以上10个以下。The upper surface of the sub-disk is provided with workpiece grooves for placing the substrate, and the number of the workpiece grooves is 1 or more and 10 or less.
所述子盘的外周边缘向下延伸形成导向凸台,所述导向凸台位于所述盘位的侧壁的外侧,所述导向凸台与所述盘位的侧壁之间形成开口朝下的排气口。The outer peripheral edge of the sub-disk extends downward to form a guide boss, the guide boss is located on the outer side of the side wall of the bay, and an opening is formed between the guide boss and the side wall of the bay and faces downward The exhaust port.
所述盘位的中心位于所述母盘的中心,所述导向凸台包绕在所述母盘的侧壁的外侧,所述凹槽远离所述盘位中心的一端通过所述排气口与外界连通。The center of the disk position is located at the center of the master disk, the guide boss is wrapped around the outer side of the side wall of the master disk, and the end of the groove away from the center of the disk position passes through the exhaust port Connect with the outside world.
所述盘位的数量是一个。The number of the bays is one.
所述盘位的中心偏离所述母盘的中心,所述母盘上围绕所述盘位设置有储气腔,所述储气腔远离所述母盘的中心的一侧贯穿所述母盘的侧壁形成边缘缺口;所述凹槽远离所述盘位中心的一端通过所述排气口与所述储气腔连通,并通过储气腔上设置的边缘缺口与外界连通。The center of the disk position is deviated from the center of the master disk, an air storage cavity is provided on the master disk around the disk position, and the side of the air storage cavity away from the center of the master disk penetrates the master disk An edge gap is formed on the side wall of the groove; the end of the groove away from the center of the disk position communicates with the air storage cavity through the exhaust port, and communicates with the outside through an edge gap provided on the air storage cavity.
所述盘位的数量是一个,所述盘位与所述母盘偏心布局;或者,The number of the bays is one, and the bays are eccentrically arranged with the mother disk; or,
所述盘位的数量是至少两个,所述至少两个盘位沿所述母盘的圆周方向等间隔分布。所述盘位的数量可以是五个。The number of the disk positions is at least two, and the at least two disk positions are equally spaced along the circumferential direction of the master disk. The number of bays may be five.
所述储气腔与所述母盘的侧壁之间设置有排气道。An exhaust passage is arranged between the air storage cavity and the side wall of the master disk.
所述排气道位于所述边缘缺口的两侧。The exhaust duct is located on both sides of the edge gap.
每个所述盘位的排气道的数量是四个,所述边缘缺口的两侧分别设置两个所述排气道。The number of exhaust passages for each disk position is four, and two exhaust passages are respectively provided on both sides of the edge gap.
所述子盘的外周侧壁与母盘的内侧壁之间设置有盘间隙,所述盘间隙的宽度小于所述储气腔的宽度。A disk gap is provided between the outer peripheral side wall of the sub disk and the inner side wall of the master disk, and the width of the disk gap is smaller than the width of the air storage cavity.
所述盘间隙可根据GaN单晶产品厚度规格进行选择,所述盘间隙的距离等于GaN单晶产品厚度的1.2倍至2倍。The disc gap can be selected according to the thickness specifications of the GaN single crystal product, and the distance of the disc gap is equal to 1.2 to 2 times the thickness of the GaN single crystal product.
所述母盘的中部设设置有有集气腔,所述集气腔配置为与外部气源连通,所述凹槽靠近所述盘位的中心的一端设置有分气孔,所述集气腔与所述分气孔连通。An air collection cavity is provided in the middle of the master disk, the air collection cavity is configured to communicate with an external air source, an end of the groove close to the center of the disk position is provided with an air distribution hole, and the air collection cavity Communicate with the vent hole.
所述母盘包括固定连接的盘主体和盘底座,所述盘位设置在所述盘主体上,所述集气腔设置在所述盘底座的中部上。The master disc includes a disc main body and a disc base fixedly connected, the disc position is arranged on the disc main body, and the air collection cavity is arranged on the middle of the disc base.
所述盘主体与盘底座为一体成型结构或者分体结构。The disc main body and the disc base have an integral structure or a separate structure.
所述盘位的中心设置有旋转轴,所述旋转轴的一端插入所述子盘的中心,所述旋转轴的另一端插入所述母盘。The center of the disk position is provided with a rotating shaft, one end of the rotating shaft is inserted into the center of the sub-disk, and the other end of the rotating shaft is inserted into the mother disk.
所述旋转轴是石墨、陶瓷或石英材料。The rotating shaft is made of graphite, ceramic or quartz material.
所述母盘的底部与升降杆的一端连接,所述升降杆被配置为上下移动,所述升降杆的中部开设有主气道,所述主气道被配置为与外部气源连通,所述主气道依次通过集气腔、分气孔与所述凹槽连通。The bottom of the master plate is connected to one end of a lifting rod, the lifting rod is configured to move up and down, a main air passage is opened in the middle of the lifting rod, and the main air passage is configured to communicate with an external air source, so The main air passage is communicated with the groove through an air collecting cavity and an air distribution hole in sequence.
该气动托盘还包括升降驱动机构和旋转驱动机构,所述旋转驱动机构的一端与所述升降杆的另一端连接,以驱动所述升降杆转动,所述升降驱动机构与所述旋转驱动机构的另一端连接,以驱动所述旋转驱动机构和升降杆整体上下移动;或者,所述升降驱动机构的一端与所述升降杆的另一端连接,以驱动所述升降杆上下移动,所述旋转驱动机构与所述升降驱动机构的另一端连接,以驱动所述升降驱动机构和升降杆整体旋转。The pneumatic tray also includes a lifting drive mechanism and a rotation drive mechanism. One end of the rotation drive mechanism is connected to the other end of the lifting rod to drive the lifting rod to rotate. The lifting drive mechanism is connected to the rotation drive mechanism. The other end is connected to drive the rotation drive mechanism and the lifting rod to move up and down as a whole; or, one end of the lifting drive mechanism is connected to the other end of the lifting rod to drive the lifting rod to move up and down, and the rotation drive The mechanism is connected with the other end of the lifting drive mechanism to drive the lifting drive mechanism and the lifting rod to rotate integrally.
所述主气道通过所述集气腔与所述凹槽连通。The main air passage communicates with the groove through the air collection cavity.
所述母盘的底部与升降杆连接,所述升降杆被配置为上下移动和水平旋转,所述升降杆的中部开设有与气源连通的主气道,所述主气道与所述凹槽连通。The bottom of the master disk is connected with a lifting rod, the lifting rod is configured to move up and down and horizontally rotate, the middle of the lifting rod is provided with a main air passage communicating with an air source, and the main air passage is connected to the concave The slots are connected.
本申请提供一种用于GaN材料生长的气动托盘,通过气流驱动子盘旋转,一方面,能够克服现有的电机驱动在高温无法使用的缺陷,从而使该气动托盘能够满足高温的使用工况,满足HVPE工艺的要求,另一方面,通过将凹槽经所述母盘的侧壁与外界连通,能够使惰性气体沿水平方向或向下倾斜方向排出,从而避免扰乱所述子盘上方的反应气体的整体气氛,保证反应气体的有效混合与反应。The present application provides a pneumatic tray for GaN material growth, which drives the sub-disk to rotate through airflow. On the one hand, it can overcome the defect that the existing motor drive cannot be used at high temperatures, so that the pneumatic tray can meet high-temperature operating conditions. , To meet the requirements of the HVPE process. On the other hand, by connecting the groove to the outside through the side wall of the master disk, the inert gas can be discharged in a horizontal direction or a downward sloping direction, thereby avoiding disturbing the upper part of the sub-disk The overall atmosphere of the reaction gas ensures the effective mixing and reaction of the reaction gas.
附图说明Description of the drawings
图1为实施例一所述的气动托盘的全剖视图;Figure 1 is a full cross-sectional view of the pneumatic tray according to the first embodiment;
图2为实施例一所述的母盘的俯视视角的全剖视图;2 is a full cross-sectional view of the master disk according to the first embodiment from a top perspective;
图3为实施例一所述的子盘(四工件槽)的俯视图;Figure 3 is a top view of the sub-disk (four-workpiece slot) described in the first embodiment;
图4为实施例一所述的子盘(一工件槽)的俯视图;4 is a top view of the sub-disk (a workpiece slot) according to the first embodiment;
图5为实施例三所述的气动托盘(六个盘位)的俯视图;Figure 5 is a top view of the pneumatic tray (six trays) described in the third embodiment;
图6为图5所示A-A向的全剖视图;Figure 6 is a full cross-sectional view of the A-A direction shown in Figure 5;
图7为实施例三所述的气动托盘的正视图(盘底座未示出);Figure 7 is a front view of the pneumatic tray described in the third embodiment (the tray base is not shown);
图8为图7所示B-B向的全剖视图;Figure 8 is a full cross-sectional view of the B-B direction shown in Figure 7;
图9为实施例三所述的母盘的结构示意图;9 is a schematic diagram of the structure of the master disk described in the third embodiment;
图10为实施例三所述的母盘的俯视图;Figure 10 is a top view of the master disk described in the third embodiment;
图11为实施例三所述的母盘其中一个盘位与子盘组装的俯视图;11 is a top view of the assembly of one of the bays of the master disc and the daughter disc in the third embodiment;
图12图11所示C-C向的全剖视图;Fig. 12 is a full cross-sectional view taken along the line C-C shown in Fig. 11;
图13为实施例三所述的气动托盘(五个盘位)的俯视图;Figure 13 is a top view of the pneumatic tray (five trays) described in the third embodiment;
图14为图13所示D-D向的全剖视图;Figure 14 is a full cross-sectional view from the direction D-D shown in Figure 13;
图15为实施例四的基于图5所示A-A向的全剖视图;Figure 15 is a full cross-sectional view of the fourth embodiment based on the A-A direction shown in Figure 5;
图16为实施例四的基于图13所示D-D向的全剖视图。Fig. 16 is a full cross-sectional view of the fourth embodiment based on the direction D-D shown in Fig. 13.
图1至图16中:In Figure 1 to Figure 16:
1、子盘;11、导向凸台;12、工件槽;1. Sub-disk; 11. Guiding boss; 12. Workpiece groove;
2、母盘;21、盘主体;211、盘位;212、凹槽;22、盘底座;221、集气腔;23、分气孔;24、储气腔;25、边缘缺口;26、排气道;2. Master disk; 21. Disk body; 211. Disk position; 212. Groove; 22. Disk base; 221. Air collecting cavity; 23. Air distribution hole; 24. Air storage cavity; 25. Edge gap; 26. Row airway;
3、排气口;3. Exhaust port;
4、旋转轴;4. Rotation axis;
5、盘间隙。5. Disc gap.
具体实施方式Detailed ways
下面结合附图并通过具体实施方式来进一步说明本申请的技术方案。The technical solutions of the present application will be further described below in conjunction with the drawings and specific implementations.
实施例一:Example one:
一种用于GaN材料生长的气动托盘,如图1和图2所示,包括子盘1和母盘2,子盘1和母盘2可采用石墨、陶瓷或石英材料,子盘1被配置为承载用于GaN外延生长的衬底,母盘2被配置为通过惰性气体承托子盘1和带动子盘1旋转。母盘2的上表面设置有用于放置子盘1的盘位211,盘位211上设置有由靠近盘位211的中心位置延伸至盘位211的边缘位置的螺旋状的凹槽212,凹槽212靠近盘位211的中心的一端与气源连通,凹槽212的另一端与外界连通,子盘1放置在盘位211上,惰性气体在凹槽212与子盘1之间围闭形成的旋转气流通道内流通。A pneumatic tray for GaN material growth, as shown in Figure 1 and Figure 2, includes a sub-disk 1 and a master disk 2. The sub-disk 1 and the master disk 2 can be made of graphite, ceramic or quartz materials, and the sub-disk 1 is configured In order to support the substrate for GaN epitaxial growth, the master disk 2 is configured to support the daughter disk 1 and drive the daughter disk 1 to rotate through an inert gas. The upper surface of the master disk 2 is provided with a bay 211 for placing the sub-disk 1, and the bay 211 is provided with a spiral groove 212 extending from a position close to the center of the bay 211 to an edge position of the bay 211. The groove One end of 212 close to the center of the tray 211 is connected to the air source, and the other end of the groove 212 is connected to the outside. The sub-disk 1 is placed on the tray 211, and the inert gas is enclosed between the groove 212 and the sub-disk 1. Circulate in the rotating air channel.
在本实施例中,母盘2上设置一个盘位211,且盘位211的中心位于母盘2的中心,子盘1的外周边缘向下延伸形成导向凸台11,导向凸台11位于盘位211的侧壁外侧,导向凸台11的内侧壁与盘位211的侧壁之间具有空隙,所述空隙形成开口朝下的排气口3,排气口3与凹槽212的位于边缘位置的一端连通。通过设置包绕在盘位211的侧壁外侧的导向凸台11和开口向下的排气口3,能够使由凹槽212内排出的惰性气体向下移动或被压在靠底部的区域,并最终向下排出,降低了惰性气体向上排出影响上方反应气体整体气氛的风险,保证反应气体的反应效率和质量。In this embodiment, a disk position 211 is provided on the master disk 2, and the center of the disk position 211 is located at the center of the master disk 2. The outer peripheral edge of the sub disk 1 extends downward to form a guide boss 11, and the guide boss 11 is located on the disk. On the outer side of the side wall of the position 211, there is a gap between the inner side wall of the guide boss 11 and the side wall of the disk position 211, and the gap forms the exhaust port 3 with the opening facing downward. One end of the location is connected. By arranging the guide boss 11 and the exhaust port 3 with downward opening around the side wall of the bay 211, the inert gas discharged from the groove 212 can be moved downward or pressed in the area near the bottom. Finally, it is discharged downwards, which reduces the risk that the inert gas is discharged upwards and affects the overall atmosphere of the reaction gas above, and ensures the reaction efficiency and quality of the reaction gas.
盘位211的中心设置有旋转轴4,旋转轴4是石墨、陶瓷或石英材料制成。旋转轴4的一端插入子盘1的中心,旋转轴4的另一端插入母盘2的盘位211 的中心。通过设置旋转轴4,能够对子盘1的转动中心进行有效固定,提高子盘1在工作过程中的可靠性。A rotating shaft 4 is arranged in the center of the disk position 211, and the rotating shaft 4 is made of graphite, ceramic or quartz material. One end of the rotating shaft 4 is inserted into the center of the sub disk 1, and the other end of the rotating shaft 4 is inserted into the center of the bay 211 of the mother disk 2. By providing the rotating shaft 4, the rotation center of the sub-disk 1 can be effectively fixed, and the reliability of the sub-disk 1 in the working process is improved.
母盘2包括固定连接的盘主体21和盘底座22,本实施例中,盘主体21与盘底座22为一体成型结构,盘位211设置在盘主体21上。盘底座22设置有与气源连通的集气腔221,凹槽212靠近盘位211的中心的一端设置有分气孔23,集气腔221与分气孔23连通。The master disk 2 includes a disk main body 21 and a disk base 22 that are fixedly connected. In this embodiment, the disk main body 21 and the disk base 22 are integrally formed, and the disk position 211 is provided on the disk main body 21. The disk base 22 is provided with an air collecting cavity 221 communicating with an air source, and an end of the groove 212 close to the center of the disk position 211 is provided with an air distribution hole 23, and the air collecting cavity 221 is in communication with the air distribution hole 23.
于本实施例中,子盘1的上表面设置有四个用于放置衬底的工件槽12,如图3所示。于其它实施例中,工件槽12的数量可以是1个或2个或3个或5个或6个或7个或8个或9个或10个。工件槽12数量为一个的状态如图4所示。In this embodiment, the upper surface of the sub-disk 1 is provided with four workpiece grooves 12 for placing substrates, as shown in FIG. 3. In other embodiments, the number of workpiece grooves 12 may be 1 or 2 or 3 or 5 or 6 or 7 or 8 or 9 or 10. The state where the number of workpiece grooves 12 is one is shown in FIG. 4.
于本实施例中,外部的气源将惰性气体通过集气腔221和分气孔23通入凹槽212,惰性气体在凹槽212与子盘1围闭形成的通道内流动至凹槽212位于边缘位置的一端,最终惰性气体沿排气口3向下排出。惰性气体在流动过程中使子盘1与母盘2气浮隔离,且螺旋状的定向气流驱动子盘1旋转。这种设计通过气流驱动子盘1旋转,一方面,能够克服现有的电机驱动在高温无法使用的缺陷,从而使该气动托盘能够满足大于800℃高温的使用工况,满足HVPE工艺的要求,另一方面,通过凹槽212与外界连通,能够使惰性气体沿水平方向或向下倾斜方向排出,从而避免扰乱子盘1上方的反应气体的整体气氛,保证反应气体的有效混合与反应;该气动托盘还可以通过控制惰性气体的流量,实时控制托盘的转速,从而适用不同的产品工艺需求和提高材料生长的质量。In this embodiment, an external gas source passes the inert gas into the groove 212 through the gas collecting cavity 221 and the gas distribution hole 23, and the inert gas flows in the channel formed by the groove 212 and the sub-disk 1 until the groove 212 is located At one end of the edge position, the inert gas is finally discharged downward along the exhaust port 3. During the flow of the inert gas, the sub-disk 1 and the mother disk 2 are air-floated and isolated, and the spiral directional airflow drives the sub-disk 1 to rotate. This design drives the sub-disk 1 to rotate through the airflow. On the one hand, it can overcome the disadvantage of the existing motor drive that cannot be used at high temperatures, so that the pneumatic tray can meet the working conditions of high temperature greater than 800°C and meet the requirements of the HVPE process. On the other hand, the groove 212 communicates with the outside, so that the inert gas can be discharged in a horizontal direction or a downward oblique direction, so as to avoid disturbing the overall atmosphere of the reaction gas above the sub-disk 1 and ensure the effective mixing and reaction of the reaction gas; The pneumatic tray can also control the speed of the tray in real time by controlling the flow of inert gas, so as to adapt to different product process requirements and improve the quality of material growth.
于本实施例中,还包括升降杆,母盘2的底部与升降杆连接,升降杆是石墨、陶瓷或石英材料制成,升降杆的中部开设有与气源连通的主气道,主气道依次通过集气腔221、分气孔23与凹槽212连通。该气动托盘还包括升降驱动机构,升降驱动机构与升降杆连接,以驱动升降杆上下移动。通过设置可上下移动的升降杆,能够实现母盘2的升降,从而调节该气动托盘与上方反应气体喷头的距离,进而控制GaN材料的生长过程,能够有效解决生长均匀性和生长速率的问题。In this embodiment, it also includes a lifting rod. The bottom of the master disk 2 is connected to the lifting rod. The lifting rod is made of graphite, ceramic or quartz. The middle of the lifting rod is provided with a main air passage communicating with the air source. The channel communicates with the groove 212 through the gas collecting cavity 221 and the gas distribution hole 23 in sequence. The pneumatic tray also includes a lifting drive mechanism, which is connected with the lifting rod to drive the lifting rod to move up and down. By providing a lifting rod that can move up and down, the master disk 2 can be raised and lowered, thereby adjusting the distance between the pneumatic tray and the upper reactive gas nozzle, and controlling the growth process of the GaN material, which can effectively solve the problems of growth uniformity and growth rate.
随着半导体器件需求大幅提升以及各类半导体器件的开发,对化合物半导体设备性能和相关设备生长出来的材料的生长效率和生长质量提出了新的要求。如何提升均匀性和生长速率这两项重要指标,是当前面临的主要难题。在制备化合物半导体材料的设备中,随时调整托盘旋转方式、托盘旋转速度和调节托盘与喷头距离是获取较好的均匀性和高生长速率的主要方法,因此本实施例通过控制惰性气体的流量,能够实时控制托盘的转速,从而适用不同的产品工艺需求和提高材料生长的质量。With the substantial increase in demand for semiconductor devices and the development of various types of semiconductor devices, new requirements have been put forward for the performance of compound semiconductor devices and the growth efficiency and growth quality of materials grown from related devices. How to improve the two important indicators of uniformity and growth rate is the main problem currently facing. In the equipment for preparing compound semiconductor materials, adjusting the tray rotation mode, the tray rotation speed and the distance between the tray and the nozzle at any time are the main methods to obtain better uniformity and high growth rate. Therefore, this embodiment controls the flow of inert gas. It can control the rotation speed of the tray in real time, so as to adapt to different product process requirements and improve the quality of material growth.
实施例二:Embodiment two:
本实施例与实施例一的区别在于:The difference between this embodiment and the first embodiment is:
所述母盘上设置一个盘位,所述盘位的中心偏离所述母盘的中心,即所述盘位与所述母盘偏心布局。所述子盘的外周边缘向下延伸形成导向凸台,所述导向凸台位于所述盘位的侧壁的外侧,所述母盘上围绕所述盘位的外周设置有储气腔,所述储气腔远离所述母盘的中心的一侧贯穿所述母盘的侧壁形成边缘缺口,凹槽212远离盘位21中心的一端与储气腔连通,并通过储气腔上设置的边缘缺口与外界连通。通过设置所述储气腔和边缘缺口,能够使从所述导向凸台内侧壁与盘位的外侧壁之间的间隙向下排出的惰性气体快速进入所述储气腔,并进一步流动至所述边缘缺口,实现水平方向或倾斜向下方向的外排,远离所述子盘上方的反应气体,从而避免对反应气体气氛造成影响,提高反应气体的反应质量。A disk position is arranged on the master disk, and the center of the disk position is deviated from the center of the master disk, that is, the disk position and the master disk are arranged eccentrically. The outer peripheral edge of the sub-disk extends downward to form a guide boss, the guide boss is located on the outer side of the side wall of the disk position, and an air storage cavity is provided on the master disk around the outer circumference of the disk position, so The side of the air storage cavity away from the center of the master disk penetrates through the side wall of the master disk to form an edge gap, and the end of the groove 212 away from the center of the disk position 21 communicates with the air storage cavity and passes through the air storage cavity. The edge gap is connected to the outside world. By providing the gas storage cavity and the edge gap, the inert gas discharged downward from the gap between the inner side wall of the guide boss and the outer side wall of the tray can quickly enter the gas storage cavity and further flow to the place. The edge notch realizes horizontal or oblique downward discharge, away from the reaction gas above the sub-disk, so as to avoid affecting the reaction gas atmosphere and improve the reaction quality of the reaction gas.
所述子盘的外周侧壁与母盘内侧壁之间设置有盘间隙,所述盘间隙的宽度小于所述储气腔的宽度,通过设置宽度较小的所述盘间隙,一方面能够使惰性气体主要趋向于在所述储气腔内流动,而非大量从所述盘间隙向上外排,保证反应气体的整体气氛;另一方面能够使少量的惰性气体残存于所述盘间隙,防止反应气体在子盘与母盘之间的间隙位置进行反应形成结晶体,进而避免子盘与母盘连成一体而卡死。所述盘间隙可根据GaN单晶产品厚度规格进行选择,所述盘间隙的距离优选等于GaN单晶产品厚度的1.2倍至2倍。A disk gap is provided between the outer peripheral side wall of the sub disk and the inner side wall of the master disk. The width of the disk gap is smaller than the width of the air storage cavity. By setting the disk gap with a smaller width, it can make The inert gas mainly tends to flow in the gas storage cavity, rather than a large amount of upward and outward discharge from the disc gap, to ensure the overall atmosphere of the reaction gas; on the other hand, a small amount of inert gas can be left in the disc gap to prevent The reaction gas reacts in the gap between the sub-disk and the mother disk to form a crystal, thereby preventing the sub-disk and the mother disk from being connected as a whole and becoming stuck. The disc gap can be selected according to the thickness specifications of the GaN single crystal product, and the distance of the disc gap is preferably equal to 1.2 to 2 times the thickness of the GaN single crystal product.
本实施例的所述储气腔与所述母盘的侧壁之间设置有排气道,排气道的数量是四个,所述边缘缺口的两侧分别设置两个所述排气道。通过设置所述排气道,能够增加所述储气腔向外排气的通道,使所述储气腔内的惰性气体及时外排,避免所述储气腔内的气体因压力过大而从所述子盘的盘间隙向上外排,从而降低惰性气体扰乱上方反应气体气氛的风险。In this embodiment, an exhaust channel is provided between the air storage cavity and the side wall of the master disk, the number of exhaust channels is four, and two exhaust channels are respectively provided on both sides of the edge gap . By arranging the exhaust passage, it is possible to increase the passage for the gas storage chamber to exhaust outwards, so that the inert gas in the gas storage chamber can be discharged in time, and the gas in the gas storage chamber can be prevented from being caused by excessive pressure Discharge upward and outward from the disc gap of the sub-disc, thereby reducing the risk of inert gas disturbing the atmosphere of the reaction gas above.
于本实施例中,还包括升降杆,所述母盘的底部与升降杆的一端连接,所述升降杆的中部开设有与气源连通的主气道,所述主气道依次通过集气腔、分气孔23与所述凹槽连通。该气动托盘还包括升降驱动机构和旋转驱动机构,所述旋转驱动机构一端与所述升降杆的另一端连接,以驱动所述升降杆转动,所述升降驱动机构与所述旋转驱动机构另一端连接,以驱动旋转驱动机构和升降杆整体上下移动。通过设置可上下移动和水平旋转的所述升降杆,能够实现所述母盘的升降和旋转,从而调节该气动托盘与上方反应气体喷头的距离,进而控制GaN材料的生长过程,能够有效解决生长均匀性和生长速率的问题。于其它实施例中,所述升降驱动机构的一端与所述升降杆的另一端连接,以驱动所述升降杆上下移动,所述旋转驱动机构与所述升降驱动机构的另一端连接,以 驱动所述升降驱动机构和升降杆整体旋转。In this embodiment, it further includes a lifting rod, the bottom of the master plate is connected to one end of the lifting rod, the middle of the lifting rod is provided with a main air passage communicating with an air source, and the main air passage sequentially passes through the air collection The cavity and the air distribution hole 23 are in communication with the groove. The pneumatic tray also includes a lifting drive mechanism and a rotation drive mechanism. One end of the rotation drive mechanism is connected to the other end of the lifting rod to drive the lifting rod to rotate. The lifting drive mechanism is connected to the other end of the rotation drive mechanism. Connected to drive the rotating drive mechanism and the lifting rod to move up and down as a whole. By setting the lifting rod that can move up and down and rotate horizontally, the lifting and rotation of the master disk can be realized, so as to adjust the distance between the pneumatic tray and the reaction gas nozzle above, thereby controlling the growth process of GaN material, which can effectively solve the growth problem. Uniformity and growth rate issues. In other embodiments, one end of the lifting driving mechanism is connected to the other end of the lifting rod to drive the lifting rod to move up and down, and the rotation driving mechanism is connected to the other end of the lifting driving mechanism to drive The lifting driving mechanism and the lifting rod rotate integrally.
实施例三:Example three:
本实施例与实施例一的区别在于:The difference between this embodiment and the first embodiment is:
母盘2上设置六个盘位211,六个盘位211沿母盘2的圆周方向等间隔分布,如图5所示。于其它实施例中,盘位211的数量还可以是两个或三个或四个或五个或七个或八个或九个或十个或更多。母盘2上设置五个盘位211的状态如图13和图14所示。Six bays 211 are provided on the master disk 2, and the six bays 211 are distributed at equal intervals along the circumferential direction of the master disk 2, as shown in FIG. 5. In other embodiments, the number of bays 211 may also be two or three or four or five or seven or eight or nine or ten or more. The state where five bays 211 are set on the master disk 2 is shown in FIG. 13 and FIG. 14.
如图6至图12所示,于本实施例中,子盘1的外周边缘向下延伸形成导向凸台11,导向凸台11位于盘位211的侧壁的外侧,母盘2上围绕盘位211的外周设置有储气腔24,储气腔24远离母盘2的中心的一侧贯穿母盘2的侧壁形成边缘缺口25。通过设置储气腔24和边缘缺口25,盘位21上设置的凹槽212远离盘位21中心的一端与储气腔24连通,并通过储气腔上设置的边缘缺口与外界连通。上述设计能够使从导向凸台11内侧壁与盘位211的外侧壁之间的间隙向下排出的惰性气体快速进入储气腔24,并进一步流动至边缘缺口25,实现惰性气体水平方向或倾斜向下方向的外排,远离子盘1上方的反应气体,从而避免对反应气体气氛造成影响,提高反应气体的反应质量。As shown in Figures 6 to 12, in this embodiment, the outer peripheral edge of the sub disk 1 extends downward to form a guide boss 11, which is located on the outside of the side wall of the disk position 211, and the master disk 2 surrounds the disk. An air storage cavity 24 is provided on the outer periphery of the position 211, and the side of the air storage cavity 24 away from the center of the master disk 2 penetrates the side wall of the master disk 2 to form an edge gap 25. By providing the air storage cavity 24 and the edge gap 25, the end of the groove 212 provided on the disk position 21 away from the center of the disk position 21 communicates with the air storage cavity 24, and communicates with the outside through the edge gap provided on the air storage cavity. The above design enables the inert gas discharged downward from the gap between the inner side wall of the guide boss 11 and the outer side wall of the tray 211 to quickly enter the gas storage chamber 24 and further flow to the edge gap 25, realizing the horizontal or inclined inert gas The outward discharge in the downward direction is far away from the reaction gas above the sub-disk 1, so as to avoid affecting the reaction gas atmosphere and improve the reaction quality of the reaction gas.
如图12所示,子盘1的外周侧壁与母盘2内侧壁之间设置有盘间隙5,盘间隙5的宽度小于储气腔24的宽度,通过设置宽度较小的盘间隙5,一方面能够使惰性气体主要趋向于在储气腔24内流动,而非大量从盘间隙5向上外排,保证反应气体的整体气氛;另一方面能够使少量的惰性气体残存于盘间隙5,防止反应气体在子盘1与母盘2连接的间隙位置进行反应形成结晶体,进而避免子盘1与母盘2连成一体而卡死。盘间隙5可根据GaN单晶产品厚度规格进行选择,盘间隙5的距离优选等于GaN单晶产品厚度的1.2倍至2倍。As shown in Figure 12, a disk gap 5 is provided between the outer peripheral side wall of the sub disk 1 and the inner side wall of the master disk 2. The width of the disk gap 5 is smaller than the width of the air storage cavity 24. By setting the disk gap 5 with a smaller width, On the one hand, it can make the inert gas mainly tend to flow in the gas storage cavity 24, instead of being discharged from the disc gap 5 upwards and outwards in a large amount, so as to ensure the overall atmosphere of the reaction gas; on the other hand, it can make a small amount of inert gas remain in the disc gap 5, The reaction gas is prevented from reacting at the gap between the sub-disk 1 and the mother disk 2 to form crystals, thereby preventing the sub-disk 1 and the mother disk 2 from being integrated and jammed. The disc gap 5 can be selected according to the thickness specifications of the GaN single crystal product, and the distance of the disc gap 5 is preferably equal to 1.2 to 2 times the thickness of the GaN single crystal product.
本实施例的储气腔24与母盘2的侧壁之间设置有排气道26,每组储气腔24设置四个排气道26,边缘缺口25的两侧分别设置两个排气道26。通过设置排气道26,能够增加储气腔24向外排气的通道,使储气腔24内的惰性气体及时外排,避免储气腔24内的气体压力过大而从盘间隙5向上外排,从而降低惰性气体扰乱上方反应气体气氛的风险。An exhaust duct 26 is provided between the air storage chamber 24 and the side wall of the master disk 2 in this embodiment. Each group of air storage chambers 24 is provided with four exhaust ducts 26, and two exhaust ducts are provided on both sides of the edge gap 25. Road 26. By providing the exhaust duct 26, it is possible to increase the passage for the gas storage chamber 24 to exhaust outward, so that the inert gas in the gas storage chamber 24 is discharged out in time, and the gas pressure in the gas storage chamber 24 is prevented from going upward from the disc gap 5 due to excessive pressure. It is discharged outside, thereby reducing the risk of inert gas disturbing the reaction gas atmosphere above.
母盘2包括固定连接的盘主体21和盘底座22,本实施例中,如图6所示,盘主体21与盘底座22为分体成型结构。通过设置分体式的盘主体21和盘底座22,能够降低母盘2的制造难度。The master disk 2 includes a disk main body 21 and a disk base 22 that are fixedly connected. In this embodiment, as shown in FIG. 6, the disk main body 21 and the disk base 22 are formed as separate parts. By providing a separate disc main body 21 and a disc base 22, the manufacturing difficulty of the master disc 2 can be reduced.
于本实施例中,母盘2的底部与升降杆的一端连接,升降杆的中部开设有与气源连通的主气道,主气道通过集气腔221、分气孔23与凹槽212连通。该 气动托盘包括升降驱动机构和旋转驱动机构,旋转驱动机构的一端与升降杆的另一端连接,以驱动升降杆转动,升降驱动机构与旋转驱动机构的另一端连接,以驱动所这旋转驱动机构和升降杆整体上下移动。通过设置可上下移动和水平旋转的升降杆,能够实现母盘2的升降和旋转,从而调节该气动托盘与上方反应气体喷头的距离,进而控制GaN材料的生长过程,能够有效解决生长均匀性和生长速率的问题。于其它实施例中,升降驱动机构的一端与升降杆的另一端连接,以驱动升降杆上下移动,旋转驱动机构与升降驱动机构的另一端连接,以驱动升降驱动机构和升降杆整体旋转。In this embodiment, the bottom of the master disk 2 is connected to one end of the lifting rod, and the middle of the lifting rod is provided with a main air passage communicating with an air source, and the main air passage communicates with the groove 212 through the air collecting cavity 221 and the air distribution hole 23 . The pneumatic tray includes a lifting drive mechanism and a rotation drive mechanism. One end of the rotation drive mechanism is connected with the other end of the lifting rod to drive the lifting rod to rotate. The lifting drive mechanism is connected with the other end of the rotation drive mechanism to drive the rotation drive mechanism. And the lifting rod moves up and down as a whole. By setting a lifting rod that can move up and down and rotate horizontally, the lifting and rotation of the master disk 2 can be realized, so as to adjust the distance between the pneumatic tray and the upper reactive gas nozzle, and then control the growth process of GaN material, which can effectively solve the growth uniformity and The problem of growth rate. In other embodiments, one end of the lifting driving mechanism is connected to the other end of the lifting rod to drive the lifting rod to move up and down, and the rotation driving mechanism is connected to the other end of the lifting driving mechanism to drive the lifting driving mechanism and the lifting rod to rotate integrally.
实施例四:Embodiment four:
本实施例与实施例三的区别在于:The difference between this embodiment and the third embodiment is:
如图15所示,母盘2包括固定连接的盘主体21和盘底座22,盘主体21与盘底座22为一体成型结构。于其它实施例中,子盘1上设置五个盘位211,母盘2包括固定连接的盘主体21和盘底座22,盘主体21与盘底座22为一体成型结构,则具体结构如图13和16所示。As shown in FIG. 15, the master disc 2 includes a disc main body 21 and a disc base 22 that are fixedly connected, and the disc main body 21 and the disc base 22 are integrally formed. In other embodiments, five disk positions 211 are provided on the sub disk 1, and the master disk 2 includes a disk main body 21 and a disk base 22 that are fixedly connected. The disk main body 21 and the disk base 22 are integrally formed. The specific structure is shown in FIG. 13 And 16 are shown.

Claims (14)

  1. 一种用于GaN材料生长的气动托盘,包括子盘和母盘,所述母盘的上表面设置有用于放置所述子盘的盘位,所述盘位上设置有由靠近盘位中心位置延伸至盘位边缘位置的螺旋状的凹槽,所述凹槽靠近所述盘位的中心的一端与气源连通,所述凹槽的另一端与外界连通。A pneumatic tray for GaN material growth, comprising a sub-disk and a master disk. The upper surface of the master disk is provided with a disk position for placing the sub-disk, and the disk position is provided with a position close to the center of the disk position. A spiral groove extending to the edge of the disk position, one end of the groove close to the center of the disk position communicates with the air source, and the other end of the groove communicates with the outside.
  2. 根据权利要求1所述的用于GaN材料生长的气动托盘,其中,所述子盘的外周边缘向下延伸形成导向凸台,所述导向凸台位于所述盘位的侧壁的外侧,所述导向凸台与所述盘位的侧壁之间形成开口朝下的排气口。The pneumatic tray for GaN material growth according to claim 1, wherein the outer peripheral edge of the sub-disk extends downward to form a guide boss, and the guide boss is located on the outer side of the side wall of the tray, so An exhaust port with a downward opening is formed between the guide boss and the side wall of the disk position.
  3. 根据权利要求2所述的用于GaN材料生长的气动托盘,其中,所述盘位的中心位于所述母盘的中心,所述导向凸台包绕在所述母盘的侧壁的外侧,所述凹槽远离所述盘位中心的一端通过所述排气口与外界连通。The pneumatic tray for GaN material growth according to claim 2, wherein the center of the disk position is located at the center of the master disk, and the guide boss is wrapped around the outer side of the side wall of the master disk, The end of the groove away from the center of the disk position communicates with the outside through the exhaust port.
  4. 根据权利要求3所述的用于GaN材料生长的气动托盘,其中,所述盘位的数量是1个;所述子盘的上表面设置有工件槽,所述工件槽的数量是如下之一:1、2、3、4、5、6、7、8、9或10。The pneumatic tray for GaN material growth according to claim 3, wherein the number of the tray positions is one; the upper surface of the sub-tray is provided with workpiece grooves, and the number of the workpiece grooves is one of the following : 1, 2, 3, 4, 5, 6, 7, 8, 9 or 10.
  5. 根据权利要求2所述的用于GaN材料生长的气动托盘,其中,所述盘位的中心偏离所述母盘的中心,所述母盘上围绕所述盘位的外周设置有储气腔,所述储气腔远离所述母盘的中心的一侧贯穿所述母盘的侧壁形成边缘缺口;所述凹槽远离所述盘位中心的一端通过所述排气口与所述储气腔连通,并通过储气腔上设置的边缘缺口与外界连通。The pneumatic tray for GaN material growth according to claim 2, wherein the center of the disk position is offset from the center of the master disk, and an air storage cavity is provided on the master disk around the outer periphery of the disk position, The side of the air storage cavity away from the center of the master disk penetrates through the side wall of the master disk to form an edge gap; the end of the groove away from the center of the disk position passes through the exhaust port and the gas storage The cavity is in communication, and communicates with the outside through an edge gap provided on the air storage cavity.
  6. 根据权利要求5所述的用于GaN材料生长的气动托盘,其中,所述盘位的数量是一个,所述盘位与所述母盘偏心布局;或者,所述盘位的数量是至少两个,所述至少两个盘位沿所述母盘的圆周方向等间隔分布。The pneumatic tray for GaN material growth according to claim 5, wherein the number of the bay is one, and the bay and the master are arranged eccentrically; or, the number of the bay is at least two One, the at least two disk positions are equally spaced along the circumferential direction of the master disk.
  7. 根据权利要求5或6所述的用于GaN材料生长的气动托盘,其中,所述储气腔与所述母盘的侧壁之间设置有排气道。The pneumatic tray for GaN material growth according to claim 5 or 6, wherein an exhaust passage is provided between the gas storage cavity and the side wall of the master disk.
  8. 根据权利要求5、6或7所述的用于GaN材料生长的气动托盘,其中,所述子盘的外周侧壁与母盘的内侧壁之间设置有盘间隙,所述盘间隙的宽度小于所述储气腔的宽度。The pneumatic tray for GaN material growth according to claim 5, 6 or 7, wherein a disk gap is provided between the outer peripheral side wall of the sub disk and the inner side wall of the master disk, and the width of the disk gap is smaller than The width of the air storage cavity.
  9. 根据权利要求8所述的用于GaN材料生长的气动托盘,其中,所述盘间隙的距离等于GaN单晶产品厚度的1.2倍至2倍。8. The pneumatic tray for GaN material growth according to claim 8, wherein the distance of the tray gap is equal to 1.2 to 2 times the thickness of the GaN single crystal product.
  10. 根据权利要求1至9任一项所述的用于GaN材料生长的气动托盘,其中,所述母盘的中部设置有集气腔,所述集气腔被配置为与外部气源连通,所述凹槽靠近所述盘位的中心的一端设置有分气孔,所述集气腔与所述分气孔连通。The pneumatic tray for GaN material growth according to any one of claims 1 to 9, wherein a gas collecting cavity is provided in the middle of the master disk, and the gas collecting cavity is configured to communicate with an external gas source, so An air distribution hole is provided at one end of the groove close to the center of the disk position, and the air collection cavity is in communication with the air distribution hole.
  11. 根据权利要求10所述的用于GaN材料生长的气动托盘,其中,所述母盘包括固定连接的盘主体和盘底座,所述盘位设置在所述盘主体上,所述集气腔设置在所述盘底座的中部。The pneumatic tray for GaN material growth according to claim 10, wherein the master disk comprises a disk body and a disk base that are fixedly connected, the disk position is provided on the disk body, and the gas collecting cavity is provided In the middle of the tray base.
  12. 根据权利要求10所述的用于GaN材料生长的气动托盘,其中,所述盘位的中心设置有旋转轴,所述旋转轴的一端插入所述子盘的中心,所述旋转轴的另一端插入所述母盘。The pneumatic tray for GaN material growth according to claim 10, wherein the center of the tray is provided with a rotating shaft, one end of the rotating shaft is inserted into the center of the sub-disk, and the other end of the rotating shaft Insert the master disk.
  13. 根据权利要求1至12任一项所述的用于GaN材料生长的气动托盘,其中,所述母盘的底部与升降杆的一端连接,所述升降杆被配置为上下移动,所述升降杆的中部开设有主气道,所述主气道被配置为与外部气源连通,所述主气道依次通过集气腔、分气孔与所述凹槽连通。The pneumatic tray for GaN material growth according to any one of claims 1 to 12, wherein the bottom of the master disk is connected to one end of a lifting rod, the lifting rod is configured to move up and down, and the lifting rod A main air passage is opened in the middle of the, the main air passage is configured to communicate with an external air source, and the main air passage is in turn communicated with the groove through an air collection cavity and a gas distribution hole.
  14. 根据权利要求13所述的用于GaN材料生长的气动托盘,还包括:升降驱动机构和旋转驱动机构;所述旋转驱动机构一端与所述升降杆的另一端连接,所述升降驱动机构与所述旋转驱动机构另一端连接;或者所述升降驱动机构的一端与所述升降杆的另一端连接,所述旋转驱动机构与所述升降驱动机构的另一端连接。The pneumatic tray for GaN material growth according to claim 13, further comprising: a lifting drive mechanism and a rotation drive mechanism; one end of the rotation drive mechanism is connected to the other end of the lifting rod, and the lifting drive mechanism is connected to the lifting rod. The other end of the rotation drive mechanism is connected; or one end of the lift drive mechanism is connected with the other end of the lift rod, and the rotation drive mechanism is connected with the other end of the lift drive mechanism.
PCT/CN2019/125531 2019-12-16 2019-12-16 Pneumatic tray for gan material growth WO2021119900A1 (en)

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