WO2021102825A1 - 一种石墨烯分散设备 - Google Patents

一种石墨烯分散设备 Download PDF

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Publication number
WO2021102825A1
WO2021102825A1 PCT/CN2019/121668 CN2019121668W WO2021102825A1 WO 2021102825 A1 WO2021102825 A1 WO 2021102825A1 CN 2019121668 W CN2019121668 W CN 2019121668W WO 2021102825 A1 WO2021102825 A1 WO 2021102825A1
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Prior art keywords
graphene
dispersant
dispersion
stirring
stirring rod
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PCT/CN2019/121668
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English (en)
French (fr)
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谢建光
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谢建光
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Priority to PCT/CN2019/121668 priority Critical patent/WO2021102825A1/zh
Publication of WO2021102825A1 publication Critical patent/WO2021102825A1/zh

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations

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  • the application relates to a graphene dispersion equipment, which belongs to the field of graphene production equipment.
  • Graphene has excellent optical, electrical, and mechanical properties, and has important application prospects in materials science, micro-nano processing, energy, biomedicine, and drug delivery. It is considered a revolutionary material in the future.
  • the prior art discloses a graphene dispersion equipment with application number 201721521192.6, which is characterized in that it includes a dispersion barrel and a stirring mechanism.
  • the dispersion barrel is provided with a dispersion chamber.
  • the stirring mechanism includes a motor and a stirring rod.
  • the dispersion barrel is provided with a vacuum spray tube and a dispersant feed pipe connected to the dispersion chamber, a graphene feed port is provided on one side of the vacuum spray tube, and an inclined plate is provided at the bottom of the dispersion chamber to disperse A discharge door is hinged on one side of the chamber, but the prior art graphene dispersing equipment requires stirring and repeated stirring to disperse graphene with higher adhesion, which leads to a decrease in the efficiency of graphene dispersion.
  • this application provides a graphene dispersion device.
  • This application aims to solve the above technical problems at least to a certain extent.
  • the primary purpose of this application is to solve the technical problem: the existing graphene dispersion equipment needs to be stirred and repeated for dispersion of graphene with high adhesion, which leads to the problem of reduced graphene dispersion efficiency.
  • a graphene dispersion equipment which structure includes a buffer seat, a dispersant storage tank, a dispersant introduction column, a connecting plate, a lifter, a dispersing device, a connecting wire, a graphene storage cup, a stirring tube, a support seat, a control box, and a control Button, display screen
  • the buffer seat is vertically installed on the upper end of the dispersant storage tank and is on the same center line as the dispersant introduction column.
  • the dispersant introduction column has a cylindrical structure and is arranged at the upper end of the connecting plate.
  • the connecting plate is installed on the upper end of the dispersing device, the rear side of the dispersing device is provided with a lifter and is installed on the upper end of the stirring tube, the graphene storage cup is provided on the upper end of the support seat, and the support seat is provided on the right side of the control box
  • the display screen is embedded and installed on the front surface of the control box with control buttons at the lower end.
  • the dispersion equipment includes an ultrasonic disperser, a stirring rod, a housing, an ultrasonic transmitter, a dispersion chamber, a push-pull cylinder, a controller, and a fixed bearing.
  • Discharging head, discharging tube, graphene storage cylinder, connecting rod, vibrating motor, connecting guide post, the ultrasonic disperser is installed at both ends of the stirring rod and inside the shell, and the ultrasonic transmitter is installed vertically on The lower end of the ultrasonic disperser and the stirring rod are on the same centerline, the lower end of the stirring rod is connected with the connecting rod through, the dispersion chamber is installed at the lower end of the ultrasonic transmitter and connected with the push-pull cylinder through, the right side of the vibration motor It is connected to the fixed bearing through a connecting rod and the upper end is connected to the controller through a connecting guide post.
  • the discharging pipe is installed on the upper end of the discharging head and is on the same center line as the stirring rod.
  • the graphene storage cylinder is installed on the The lower end of the inner side of the shell.
  • control button is embedded and installed on the front surface of the control box, and the rear side of the buffer seat is connected to the control box through a connecting wire.
  • the stirring tube is arranged inside the graphene storage cup, and the graphene storage cup is arranged at the lower end of the dispersion device.
  • dispersant introduction column and the dispersing device are on the same center line, and the lifter is installed on the rear side of the connecting plate.
  • stirring tube and the discharging head are on the same center line, and the shell is vertically installed at the lower end of the connecting plate.
  • model of the vibration motor is YDEJ, which has the function of reducing the noise caused by the working process of the dispersing equipment.
  • model of the controller is ID120-P, which has the function of controlling the device to perform the dispersed stirring operation.
  • the present application is a graphene dispersing equipment.
  • the dispersing equipment is arranged in the structure, and the dispersing agent is introduced into the stirring rod through the dispersing agent storage tank and the dispersing agent introduction column in the device, and then the dispersing agent is introduced into the stirring rod through the stirring rod and the discharge pipe.
  • the dispersant is imported and exported through the discharging head, and during the dispersant introduction process, the device is pushed by the ultrasonic disperser to control the ultrasonic transmitter for sonic emission to reduce the graphene bonding speed in the graphene storage tank, and the stirring tube is used for exporting and stirring , So as to enhance the graphene dispersion speed.
  • FIG. 1 is a schematic diagram of the structure of a graphene dispersion device of this application.
  • FIG. 2 is a schematic diagram of a cross-sectional structure of a dispersion device of a graphene dispersion device according to the present application.
  • buffer seat-1 dispersant storage tank-2, dispersant introduction column-3, connecting plate-4, elevator-5, dispersing equipment-6, connecting wire-7, graphene storage cup-8, stirring Tube-9, Support Base-10, Control Box-11, Control Button-12, Display-13, Ultrasonic Disperser-601, Stirring Rod-602, Shell-603, Ultrasonic Transmitter-604, Dispersion Room-605 , Push-pull cylinder-606, controller-607, fixed bearing-608, discharge head-609, discharge tube-610, graphene storage cylinder-611, connecting rod-612, vibration motor-613, connecting guide column-614 .
  • This application provides a technical solution for graphene dispersion equipment: its structure includes a buffer seat 1, a dispersant storage tank 2, a dispersant introduction column 3, a connecting plate 4, a lifter 5, and a dispersing device 6 , Connecting wire 7, graphene storage cup 8, stirring tube 9, support seat 10, control box 11, control button 12, display screen 13, the buffer seat 1 is vertically installed on the upper end of the dispersant storage tank 2 and is connected with the dispersant
  • the introduction column 3 is on the same centerline
  • the dispersant introduction column 3 is a cylindrical structure and is arranged at the upper end of the connecting plate 4
  • the connecting plate 4 is installed at the upper end of the dispersing device 6, and the dispersing device 6 is arranged on the rear side.
  • the dispersion device 6 includes an ultrasonic disperser 601, a stirring rod 602, a housing 603, an ultrasonic transmitter 604, a dispersion chamber 605, a push-pull cylinder 606, a controller 607, and a fixed Bearing 608, discharge head 609, discharge pipe 610, graphene storage cylinder 611, connecting rod 612, vibration motor 613, connecting guide post 614, the ultrasonic disperser 601 is installed at both ends of the stirring rod 602 and installed in the housing Inside 603, the ultrasonic transmitter 604 is vertically installed at the lower end of the ultrasonic disperser 601 and on the same center line as the stirring rod 602. The lower end of the stirring rod 602 is connected to the connecting rod 612 through the dispersion chamber 605.
  • the lower end of the transmitter 604 is connected to the push-pull cylinder 606, the right side of the vibration motor 613 is connected to the fixed bearing 608 through the connecting rod 612, and the upper end is connected to the controller 607 through the connecting guide post 614.
  • the discharge pipe 610 Installed at the upper end of the discharge head 609 and on the same center line as the stirring rod 602, the graphene storage cylinder 611 is installed at the lower end of the inner side of the housing 603, and the control button 12 is embedded and installed on the front surface of the control box 11.
  • the rear side of the buffer seat 1 is connected to the control box 11 through a connecting wire 7, the stirring tube 9 is arranged inside the graphene storage cup 8, and the graphene storage cup 8 is arranged at the lower end of the dispersing device 6.
  • the agent introduction column 3 and the dispersion device 6 are on the same centerline, the lifter 5 is installed on the back side of the connecting plate 4, the stirring tube 9 and the discharge head 609 are on the same centerline, and the housing 603 is vertical Installed at the lower end of the connecting plate 4, the vibration motor 613 model is YDEJ, which has the function of reducing the noise caused by the working process of the dispersing equipment, and the controller 607 model is ID120-P, which has a control device for dispersing stirring The role of the operation.
  • the vibration motor 613 mentioned in this patent is to install a set of adjustable eccentric blocks at both ends of the rotor shaft.
  • the centrifugal force generated by the high-speed rotation of the shaft and the eccentric block is used to obtain the exciting force.
  • the display screen 13 is a kind of The electronic file is displayed on the screen through a specific transmission device and then reflected to the display tool of the human eye.
  • the introduction column 3 introduces the dispersant into the stirring rod 602 in the dispersing device 6, and then the dispersant is introduced and exported through the discharge head 609 through the stirring rod 602 and the discharge pipe 610, and during the dispersant introduction process, the device is dispersed by ultrasonic
  • the device 601 pushes and controls the ultrasonic transmitter 604 to emit sound waves to reduce the graphene bonding speed in the graphene storage cylinder 611, and is led out and stirred through the stirring tube 9 to enhance the graphene dispersion speed, and can be performed by the elevator 5. Adjust the height of the dispersing device 6 to perform a uniform dispersing operation.
  • This application solves the problem that the graphene dispersion equipment needs to stir and repeat the stirring for the graphene with high adhesion to disperse, which leads to the reduction of the graphene dispersion efficiency.
  • This application uses the combination of the above components to set the dispersion in the structure. Equipment, and the dispersant is introduced into the stirring rod through the dispersant storage tank and the dispersant introduction column in the device, and then the dispersant is introduced and discharged through the discharge head through the stirring rod and the discharge pipe, and the dispersant is introduced during the dispersant introduction process.
  • the device controls the ultrasonic transmitter to emit sound waves through the push of the ultrasonic disperser to reduce the graphene bonding speed in the graphene storage cylinder, and conducts agitation through the stirring tube to enhance the graphene dispersion speed.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

一种石墨烯分散设备，其结构包括缓冲座（1）、分散剂储存罐（2）、分散剂导入柱（13）、连接盘（4）、升降器（15）、分散设备（16）、连接导线（7）、石墨烯存放杯（8）、搅拌管（9）、支撑座（10）、控制箱（11）、控制按钮（12）、显示屏（13），分散剂导入柱（13）为圆柱体结构并且设于连接盘（4）的上端，连接盘（4）安装于分散设备（6）的上端，在结构上设置了分散设备（6），并且通过该装置中的分散剂储存罐（2）与分散剂导入柱（3）将分散剂导入到搅拌杆（602）内，接着通过搅拌杆（602）与出料管（610）将分散剂通过出料头（609）进导出，并在分散剂导入过程，装置通过超声波分散器（601）推压进行控制超声波发射器（604）进行声波发射降低石墨烯存放缸（611）内的石墨烯黏合速度，并通过搅拌管（9）进行导出搅拌，从而进行加强石墨烯分散速度。

Description

一种石墨烯分散设备 技术领域
本申请涉及一种石墨烯分散设备，属于石墨烯生产设备领域。
背景技术
石墨烯具有优异的光学、电学、力学特性，在材料学、微纳加工、能源、生物医学和药物传递等方面具有重要的应用前景，被认为是一种未来革命性的材料。
现有技术公开了申请号为：201721521192.6的一种石墨烯分散设备，其特征在于，包括分散桶和搅拌机构，分散桶内设有分散室，搅拌机构包括电机和搅拌杆，搅拌杆底端伸入分散室内，所述分散桶上设有连通分散室的真空喷射管和分散剂入料管，真空喷射管一侧设有石墨烯进料口，所述分散室内腔底部设有斜板，分散室一侧铰接有出料门，但是该现有技术石墨烯分散设备对黏合性较高的石墨烯，需要进行搅拌重复搅拌进行分散，导致对石墨烯分散效率降低。
发明内容
本申请为克服上述现有技术所述的至少一种缺陷，提供一种石墨烯分散设备。
本申请旨在至少在一定程度上解决上述技术问题。
本申请的首要目的是解决技术问题：现有石墨烯分散设备对黏合性较高的石墨烯，需要进行搅拌重复搅拌进行分散，导致对石墨烯分散效率降低的问题。
为解决上述技术问题，本申请的技术方案如下：
一种石墨烯分散设备，其结构包括缓冲座、分散剂储存罐、分散剂导入柱、连接盘、升降器、分散设备、连接导线、石墨烯存放杯、搅拌管、支撑座、控制箱、控制按钮、显示屏，所述缓冲座垂直安装于分散剂储存罐的上端并且与分散剂导入柱在同一中心线上，所述分散剂导入柱为圆柱体结构并且设于连接盘的上端，所述连接盘安装于分散设备的上端，所述分散设备后侧设有升降器并且安装于搅拌管的上端，所述石墨烯存放杯设于支撑座的上端，所述支撑座设于控制箱右侧，所述显示屏嵌入安装于控制箱的前端表面并且下端设有控制按钮，所述分散设备包括超声波分散器、搅拌杆、壳体、超声波发射器、分散室、推拉缸、控制器、固定轴承、出料头、出料管、石墨烯存放缸、连接杆、振动电机、连接导柱，所述超声波分散器安装于搅拌杆两端并且安装于壳体内侧，所述超声波发射器垂直安装于超声波分散器的下端并且与搅拌杆在同一中心线上，所述搅拌杆下端与连接杆贯穿连接，所述分散室安装于超声波发射器的下端并且与推拉缸贯穿连接，所述振动电机右侧通过连接杆与固定轴承相连 接并且上端通过连接导柱与控制器相连接，所述出料管安装于出料头的上端并且与搅拌杆在同一中心线上，所述石墨烯存放缸安装于壳体内侧下端。
进一步地，所述控制按钮嵌入安装于控制箱的前端表面，所述缓冲座后侧通过连接导线与控制箱相连接。
进一步地，所述搅拌管设于石墨烯存放杯的内侧，所述石墨烯存放杯设于分散设备的下端。
进一步地，所述分散剂导入柱与分散设备在同一中心线上，所述升降器安装于连接盘的后侧。
进一步地，所述搅拌管与出料头在同一中心线上，所述壳体垂直安装于连接盘的下端。
进一步地，所述振动电机型号为YDEJ，其具有进行降低分散设备设备工作过程造成噪音的作用。
进一步地，所述控制器型号为ID120-P，其具有进行控制装置进行分散搅拌操作的作用。
与现有技术相比，本申请技术方案的有益效果是：
本申请一种石墨烯分散设备，在结构上设置了分散设备，并且通过该装置中的分散剂储存罐与分散剂导入柱将分散剂导入到搅拌杆内，接着通过搅拌杆与出料管将分散剂通过出料头进导出，并在分散剂导入过程，装置通过超声波分散器推压进行控制超声波发射器进行声波发射降低石墨烯存放缸内的石墨烯黏合速度，并通过搅拌管进行导出搅拌，从而进行加强石墨烯分散速度。
附图说明
图1为本申请一种石墨烯分散设备的结构示意图；
图2为本申请一种石墨烯分散设备的分散设备剖面结构示意图。
图中：缓冲座-1、分散剂储存罐-2、分散剂导入柱-3、连接盘-4、升降器-5、分散设备-6、连接导线-7、石墨烯存放杯-8、搅拌管-9、支撑座-10、控制箱-11、控制按钮-12、显示屏-13、超声波分散器-601、搅拌杆-602、壳体-603、超声波发射器-604、分散室-605、推拉缸-606、控制器-607、固定轴承-608、出料头-609、出料管-610、石墨烯存放缸-611、连接杆-612、振动电机-613、连接导柱-614。
附图仅用于示例性说明，不能理解为对本专利的限制；为了更好说明本实施例，附图某些部件会有省略、放大或缩小，并不代表实际产品的尺寸；对于本领域技术人员来说， 附图中某些公知结构及其说明可能省略是可以理解的；相同或相似的标号对应相同或相似的部件；附图中描述位置关系的用语仅用于示例性说明，不能理解为对本专利的限制。
具体实施方式
下面结合附图和实施例对本申请的技术方案做进一步的说明。
实施例1
请参阅图1、图2，本申请提供一种石墨烯分散设备技术方案：其结构包括缓冲座1、分散剂储存罐2、分散剂导入柱3、连接盘4、升降器5、分散设备6、连接导线7、石墨烯存放杯8、搅拌管9、支撑座10、控制箱11、控制按钮12、显示屏13，所述缓冲座1垂直安装于分散剂储存罐2的上端并且与分散剂导入柱3在同一中心线上，所述分散剂导入柱3为圆柱体结构并且设于连接盘4的上端，所述连接盘4安装于分散设备6的上端，所述分散设备6后侧设有升降器5并且安装于搅拌管9的上端，所述石墨烯存放杯8设于支撑座10的上端，所述支撑座10设于控制箱11右侧，所述显示屏13嵌入安装于控制箱11的前端表面并且下端设有控制按钮12，所述分散设备6包括超声波分散器601、搅拌杆602、壳体603、超声波发射器604、分散室605、推拉缸606、控制器607、固定轴承608、出料头609、出料管610、石墨烯存放缸611、连接杆612、振动电机613、连接导柱614，所述超声波分散器601安装于搅拌杆602两端并且安装于壳体603内侧，所述超声波发射器604垂直安装于超声波分散器601的下端并且与搅拌杆602在同一中心线上，所述搅拌杆602下端与连接杆612贯穿连接，所述分散室605安装于超声波发射器604的下端并且与推拉缸606贯穿连接，所述振动电机613右侧通过连接杆612与固定轴承608相连接并且上端通过连接导柱614与控制器607相连接，所述出料管610安装于出料头609的上端并且与搅拌杆602在同一中心线上，所述石墨烯存放缸611安装于壳体603内侧下端，所述控制按钮12嵌入安装于控制箱11的前端表面，所述缓冲座1后侧通过连接导线7与控制箱11相连接，所述搅拌管9设于石墨烯存放杯8的内侧，所述石墨烯存放杯8设于分散设备6的下端，所述分散剂导入柱3与分散设备6在同一中心线上，所述升降器5安装于连接盘4的后侧，所述搅拌管9与出料头609在同一中心线上，所述壳体603垂直安装于连接盘4的下端，所述振动电机613型号为YDEJ，其具有进行降低分散设备设备工作过程造成噪音的作用，所述控制器607型号为ID120-P，其具有进行控制装置进行分散搅拌操作的作用。
本专利所说的振动电机613是在转子轴两端各安装一组可调偏心块，利用轴及偏心块高速旋转产生的离心力得到激振力，所述显示屏13它是一种将一定的电子文件通过特定的传输设备显示到屏幕上再反射到人眼的显示工具。
例如，王师傅在进行使用时，先将分散剂存放于分散剂储存罐2内侧，然后通过控制控制箱11中的控制按钮12进行控制分散剂的导出，并且通过分散剂储存罐2与分散剂导入柱3将分散剂导入到分散设备6中的搅拌杆602内，接着通过搅拌杆602与出料管610将分散剂通过出料头609进导出，并在分散剂导入过程，装置通过超声波分散器601推压进行控制超声波发射器604进行声波发射降低石墨烯存放缸611内的石墨烯黏合速度，并通过搅拌管9进行导出搅拌，从而进行加强石墨烯分散速度，并且可通过升降器5进行调节分散设备6高度，从而进行均匀分散的操作。
本申请解决了石墨烯分散设备对黏合性较高的石墨烯，需要进行搅拌重复搅拌进行分散，导致对石墨烯分散效率降低的问题，本申请通过上述部件的互相组合，在结构上设置了分散设备，并且通过该装置中的分散剂储存罐与分散剂导入柱将分散剂导入到搅拌杆内，接着通过搅拌杆与出料管将分散剂通过出料头进导出，并在分散剂导入过程，装置通过超声波分散器推压进行控制超声波发射器进行声波发射降低石墨烯存放缸内的石墨烯黏合速度，并通过搅拌管进行导出搅拌，从而进行加强石墨烯分散速度。
显然，本申请的上述实施例仅仅是为清楚地说明本申请所作的举例，而并非是对本申请的实施方式的限定。对于所属领域的普通技术人员来说，在上述说明的基础上还可以做出其它不同形式的变化或变动。这里无需也无法对所有的实施方式予以穷举。凡在本申请的精神和原则之内所作的任何修改、等同替换和改进等，均应包含在本申请权利要求的保护范围之内。

Claims (5)

  1. 一种石墨烯分散设备，其特征在于：其结构包括缓冲座(1)、分散剂储存罐(2)、分散剂导入柱(3)、连接盘(4)、升降器(5)、分散设备(6)、连接导线(7)、石墨烯存放杯(8)、搅拌管(9)、支撑座(10)、控制箱(11)、控制按钮(12)、显示屏(13)，所述缓冲座(1)垂直安装于分散剂储存罐(2)的上端并且与分散剂导入柱(3)在同一中心线上，所述分散剂导入柱(3)为圆柱体结构并且设于连接盘(4)的上端，所述连接盘(4)安装于分散设备(6)的上端，所述分散设备(6)后侧设有升降器(5)并且安装于搅拌管(9)的上端，所述石墨烯存放杯(8)设于支撑座(10)的上端，所述支撑座(10)设于控制箱(11)右侧，所述显示屏(13)嵌入安装于控制箱(11)的前端表面并且下端设有控制按钮(12)，所述分散设备(6)包括超声波分散器(601)、搅拌杆(602)、壳体(603)、超声波发射器(604)、分散室(605)、推拉缸(606)、控制器(607)、固定轴承(608)、出料头(609)、出料管(610)、石墨烯存放缸(611)、连接杆(612)、振动电机(613)、连接导柱(614)，所述超声波分散器(601)安装于搅拌杆(602)两端并且安装于壳体(603)内侧，所述超声波发射器(604)垂直安装于超声波分散器(601)的下端并且与搅拌杆(602)在同一中心线上，所述搅拌杆(602)下端与连接杆(612)贯穿连接，所述分散室(605)安装于超声波发射器(604)的下端并且与推拉缸(606)贯穿连接，所述振动电机(613)右侧通过连接杆(612)与固定轴承(608)相连接并且上端通过连接导柱(614)与控制器(607)相连接，所述出料管(610)安装于出料头(609)的上端并且与搅拌杆(602)在同一中心线上，所述石墨烯存放缸(611)安装于壳体(603)内侧下端。
  2. 根据权利要求1所述的一种石墨烯分散设备，其特征在于：所述控制按钮(12)嵌入安装于控制箱(11)的前端表面，所述缓冲座(1)后侧通过连接导线(7)与控制箱(11)相连接。
  3. 根据权利要求1所述的一种石墨烯分散设备，其特征在于：所述搅拌管(9)设于石墨烯存放杯(8)的内侧，所述石墨烯存放杯(8)设于分散设备(6)的下端。
  4. 根据权利要求1所述的一种石墨烯分散设备，其特征在于：所述分散剂导入柱(3)与分散设备(6)在同一中心线上，所述升降器(5)安装于连接盘(4)的后侧。
  5. 根据权利要求1所述的一种石墨烯分散设备，其特征在于：所述搅拌管(9)与出料头(609)在同一中心线上，所述壳体(603)垂直安装于连接盘(4)的下端。
PCT/CN2019/121668 2019-11-28 2019-11-28 一种石墨烯分散设备 WO2021102825A1 (zh)

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