WO2021088399A1 - 一种保湿补水面膜组合物、面膜及其制备方法 - Google Patents

一种保湿补水面膜组合物、面膜及其制备方法 Download PDF

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WO2021088399A1
WO2021088399A1 PCT/CN2020/101349 CN2020101349W WO2021088399A1 WO 2021088399 A1 WO2021088399 A1 WO 2021088399A1 CN 2020101349 W CN2020101349 W CN 2020101349W WO 2021088399 A1 WO2021088399 A1 WO 2021088399A1
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parts
extract
facial mask
moisturizing
mask composition
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PCT/CN2020/101349
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English (en)
French (fr)
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汪垠明
汪羿典
符春丽
田伟兰
汪翔
祝荣梅
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湖北创界生物科技有限公司
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Publication of WO2021088399A1 publication Critical patent/WO2021088399A1/zh
Priority to ZA2022/01242A priority Critical patent/ZA202201242B/en

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
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    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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    • A61K8/553—Phospholipids, e.g. lecithin
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    • A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
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    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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Definitions

  • the invention belongs to the technical field of cosmetics, and specifically relates to a moisturizing and hydrating facial mask composition, a facial mask and a preparation method thereof.
  • Facial mask is a category of skin care products and a carrier of beauty care products. It is applied to the face for beauty functions such as moisturizing, whitening, anti-aging, and balancing oils.
  • the principle of the mask is to use the short time of covering the face to temporarily isolate the outside air and pollution, increase the skin temperature, expand the skin pores, promote sweat gland secretion and metabolism, increase the oxygen content of the skin, and help the skin eliminate the epidermis
  • moisturizing is the eternal theme of skin care. It is an important condition to ensure skin health and delay aging.
  • skin moisturizing structure is lost, and the moisture content between skin tissue cells and cells decreases.
  • the content drops below 10%, the skin will appear dry, lose its elasticity, wrinkle, and accelerate skin aging; on the other hand, the skin will be damaged by heat, cold, wind, cleaning agents, ultraviolet radiation, etc., and the surface will become more severe. dry. Therefore, how to maintain skin moisture and reduce moisture loss is very important.
  • the present invention provides a moisturizing and hydrating facial mask composition, a facial mask and a preparation method thereof.
  • the composition of the present invention selects natural raw material extracts, is safe and effective, can be quickly absorbed by the skin, and moisturizes The effect is excellent, and at the same time it effectively locks in moisture.
  • the first objective of the present invention is to provide a moisturizing and hydrating facial mask composition, comprising water, auxiliary materials and plant extracts.
  • the plant extracts include rose water, Portulaca oleracea extract, Dendrobium officinale extract, and white truffle Bacteria extract, Snow lotus extract, Tremella fruit body extract, Centella asiatica extract, Soybean seed extract, Tea leaf extract, and Teflon extract.
  • Turkic rose flower water is preferably Damascus rose. After refined distillation, it has a natural moisturizing function, which can promote deep absorption of water, improve dry skin, reduce fine lines, and has a natural fragrance. Purslane extract has comprehensive properties such as preventing dryness and aging in winter, increasing skin comfort, scavenging free radicals, and improving skin comfort.
  • Dendrobium candidum is an orchidaceous herb, which was regarded as the "Holy Good for Health” in ancient times; in ancient folks, it has the reputation of "life-saving fairy grass”.
  • Dendrobium officinale contains mucus, which has nourishing and nourishing effects on human skin, and can make human skin smooth and youthful forever. Its core active ingredient is Dendrobium officinale polysaccharide, which has the functions of activating macrophages, anti-oxidation, strengthening immunity, anti-aging, anti-bacterial and anti-inflammatory.
  • White truffle extract can inhibit melanin production, promote skin's internal metabolism, revitalize cells, and provide healthy energy for the skin.
  • Snow lotus extract also has a certain regulating effect on smooth muscle. This is because Saussurea Total Alkaloids can act on histamine and relieve smooth muscle spasms. Third, it has anti-inflammatory effects and functions.
  • Tremella fruit body extract is a kind of material-derived hyaluronic acid.
  • the water-soluble polymer isopolysaccharide extracted from Tremella fungus has moisture retention performance surpassing that of hyaluronic acid, can retain 490 times the water, and has excellent film-forming properties. And extremely smooth feeling, excellent skin care effect. Enhance cellular immune function, eliminate free radicals, anti-oxidation, anti-aging, supplement nutrition, increase skin elasticity, and reduce skin texture.
  • Centella asiatica extract can significantly increase the degree of hydration of the stratum corneum, which is mainly related to the triterpene saponins in the Centella asiatica extract. Centella asiatica triterpene saponins are hydrophilic sugar chains. Mainly glucose and rhamnose, which can combine with water in the occlusion layer to improve the barrier ability of the epidermis and enhance skin moisture.
  • Soybean seed extract is rich in flavonoids and other ingredients, which can promote the growth of fibroblasts, have skin-activating and anti-aging effects; at the same time, it can maintain skin moisture and have a moisturizing effect.
  • Tea extract is also a new type of natural antioxidant. It has a strong antioxidant effect at normal temperature and low concentration, inhibits collagenase and elastase, prevents the decrease or denaturation of elastin protein, and maintains skin elasticity. Achieve anti-wrinkle effect.
  • the extract of tetrandrine has strong skin lightening, anti-allergic and anti-inflammatory effects, and the skin is healthy and shiny after use.
  • the plant extracts also include Altai Bupleurum root extract, apple fruit cell culture extract, ylang-ylang flower extract, spring elm root extract, pseudoleaf tree root extract, purple pine cone Chrysanthemum extract, tree peony root bark extract.
  • Altai Bupleurum root extract contains volatile oil, Bupleurum alcohol, oleic acid, linolenic acid, palmitic acid, stearic acid, niacin, glucose and saponins, etc., has anti-inflammatory effects, anti-pathogen effects, plant-based natural extracts, Containing vitamin C and a variety of nutrients, it has a variety of effects and a variety of ingredients. After being extracted from plants, it is a characteristic ingredient for skin conditioning.
  • the main active ingredient saikosaponin can enhance the immune system of human cells, improve skin metabolism, increase capillary permeability, and proliferate cortical cells.
  • saikosaponin can absorb ultraviolet rays, and in vitro tests have shown that it also has the effect of inhibiting the formation of melanin.
  • Saikosaponin has good transdermal permeability and can accelerate the transdermal penetration of other ingredients. It has strong anti-oxidation, anti-inflammatory and anti-viral effects.
  • the uridine contained in it can accelerate the metabolism of skin cells and the regeneration of the skin stratum corneum.
  • Apple fruit cell culture extract has the effect of eliminating a variety of free radicals and can be used as an antioxidant. This is related to several contained proanthocyanidins; low luciferase activity is a sign of skin prone to atopic dermatitis, so It has anti-inflammatory properties; it can also be used as a skin-activating anti-wrinkle agent, moisturizer and slimming agent.
  • Ylang-Ylang extract can maintain skin moisture, maintain skin elasticity, and has moisturizing effect.
  • the spring elm root extract has excellent antioxidant, antibacterial, anti-inflammatory and dispersing abilities.
  • the active ingredients of false leaf tree root extract are mainly spirostanes and flavonoids, which promote smooth blood circulation, enhance skin cell metabolism, and have a moisturizing effect.
  • Purple Echinacea extract has excellent antioxidant, antibacterial, anti-inflammatory, and dispersing abilities, and is used as a conditioning agent, moisturizer, tonic, etc. in the field of personal care products.
  • Paeonia suffruticosa root bark extract has inhibitory effect on metalloproteinases and elastase, and has activating effect on cathepsin, which shows that it has skin activating and anti-aging functions, combined with excellent antioxidant properties, and can be used in anti-aging cosmetics; for collagen fiber
  • the gel has a good contraction effect, which means it has astringent effect on the dermis layer of the skin. It can be used in cosmetics for firming and removing bags under the eyes. It has good antibacterial and anti-inflammatory properties and can be used for the prevention and treatment of acne.
  • the excipients include butanediol, trehalose, 1,2-hexanediol, p-hydroxyacetophenone, glycerin, squalane, caprylic/capric triglyceride, isonon Isononyl acid, hydrogenated lecithin, PEG-10 soy sterol, disodium EDTA, tocopherol acetate, phenoxyethanol, xanthan gum, ethylhexyl glycerol, hydroxylated lecithin, allantoin, ⁇ -glucose Glycan, xylitol glucoside, anhydroxylitol, xylitol, glucose, panthenol, hydroxyethyl cellulose, dipotassium glycyrrhizinate, sodium hyaluronate, sodium polyglutamate, propylene glycol, taurine Acid, aminobutyric acid, threonine,
  • the auxiliary materials also include avocado oil, hydrolyzed collagen, calcium gluconate, honey, cetearyl glucoside, sesame seed oil and Yunnan camellia seed oil.
  • the composition includes the following ingredients: 30-80 parts of Rosa Turfica flower water, 0.03-0.07 parts of Portulaca oleracea extract, 1.2-1.6 parts of Dendrobium officinale extract, White Truffle fungus extract 1.1-1.5 parts, snow lotus extract 1.2-1.6 parts, Tremella fruit body extract 1.3-1.9 parts, Centella asiatica extract 1.1-1.5 parts, soybean seed extract 1.1-1.5 parts, tea extract 1.2-1.6 parts, Fenfangji extract 0.08-0.12 parts, Altai Bupleurum root extract 1.0-2.0 parts, Apple fruit cell culture extract 0.2-0.6 parts, Ylang-Ylang flower extract 1.3-1.9 parts, Spring Ulmus root extract 1.2-1.8 parts of artificial leaf tree root extract 0.8-1.2 parts, Echinacea purpurea extract 1.0-1.5 parts, tree peony root bark extract 0.8-0.12 parts, butylene glycol 0.4-1.0 parts, water 10-20 parts, 0.2-0.6 parts of
  • the composition comprises the following ingredients: 60-70 parts of Rosa Turfica flower water, 0.04-0.06 parts of Portulaca oleracea extract, 1.3-1.5 parts of Dendrobium officinale extract, White Truffle fungus extract 1.2-1.4 parts, snow lotus extract 1.3-1.5 parts, Tremella fruit body extract 1.5-1.7 parts, Centella asiatica extract 1.2-1.4 parts, soybean seed extract 1.2-1.4 parts, tea extract 1.3-1.5 parts, tetrandrine extract 0.09-0.11 parts, Altai Bupleurum root extract 1.4-1.6 parts, apple fruit cell culture extract 0.3-0.5 parts, ylang-ylang flower extract 1.5-1.7 parts, spring elm root extract 1.4-1.6 parts of artificial leaf tree root extract 0.9-1.1 parts, Echinacea purpurea extract 1.2-1.3 parts, tree peony root bark extract 0.9-0.11 parts, butanediol 0.6-0.8 parts, water 14-16 parts, 0.3-
  • the composition includes the following ingredients: 65 parts of Rosa Turkica flower water, 0.05 parts of Portulaca oleracea extract, 1.4 parts of Dendrobium officinale extract, and 1.3 parts of White truffle fungus extract , Snow lotus extract 1.4 parts, Tremella fruiting body extract 1.6 parts, Centella asiatica extract 1.3 parts, soybean seed extract 1.3 parts, tea extract 1.4 parts, Fenfangji extract 0.10 parts, Altai Bupleurum root extract 1.5 parts, apple fruit cell culture extract 0.4 parts, ylang-ylang extract 1.6 parts, spring elm root extract 1.5 parts, false leaf tree root extract 1.0 part, purple echinacea extract 1.25 parts, tree peony root bark extract 0.10 Parts, 0.7 parts of butanediol, 15 parts of water, 0.4 parts of trehalose, 0.035 parts of 1,2-hexanediol, 0.05 parts of p-hydroxyacetophenone, 0.45 parts
  • the amount of rose flower water is more than that of water, and the rose flower water is used as the main functional component and also acts as a solvent.
  • the spring elm root extract, pseudoleaf tree root extract and tree peony root bark extract are all extracted by the following methods:
  • the spring elm root extract, pseudoleaf tree root extract, and tree peony root bark extract of the present invention are extracted through specific extraction methods.
  • the extract of the present invention can penetrate deep into the bottom layer of the skin to replenish moisture.
  • the composition of the present invention allows the skin to absorb quickly. It can also effectively reduce the loss of transdermal moisture, lock in moisture, and improve skin looseness and dryness.
  • the second object of the present invention provides a method for preparing the moisturizing and hydrating facial mask composition, which includes the following steps:
  • step (b) it is characterized in that in step (b), it is heated to 35-45°C.
  • the third object of the present invention is to provide a facial mask including the moisturizing and hydrating facial mask composition.
  • the facial mask of the present invention can be a film made of silk mesh, cotton or hemp fibers, can be made into an unused carrier, or can be a facial mask directly applied to the face.
  • the facial mask composition of the present invention is made of natural raw material extracts, which can make the skin deeply hydrated and the surface layer has the double moisturizing effect. Through the synergistic effect of each raw material, the skin can quickly absorb, repair skin fine lines, and improve The skin resistance ability can also reduce the loss of transdermal moisture, lock the moisture, have good moisturizing and water-locking performance, good moisturizing effect, and no irritation to the skin.
  • the composition of the present invention has a simple preparation method and can be produced on a large scale. , Easy to promote;
  • the spring elm root extract, pseudoleaf root extract, and tree peony root bark extract of the present invention are extracted by a specific extraction method.
  • the extract of the present invention can penetrate deep into the bottom of the skin to replenish moisture.
  • the composition of the present invention makes the skin Quickly absorb and dilute acne marks, it can also effectively reduce transdermal moisture loss, lock moisture, and improve skin relaxation and dryness.
  • the extract prepared by the method of the present invention can be more completely dissolved in water and easier to be absorbed by the body , Can maximize its value, has a better moisturizing and hydrating effect.
  • the moisturizing and hydrating facial mask composition of this embodiment is made from the following raw materials: 30kg of rose flower water, 0.03kg of portulaca extract, 1.2kg of Dendrobium officinale extract, 1.1kg of white truffle fungus extract, and 1.2 kg of snow lotus extract kg, Tremella fruiting body extract 1.3kg, Centella asiatica extract 1.1kg, soybean seed extract 1.1kg, tea extract 1.2kg, tetrandrine extract 0.08kg, butylene glycol 0.4kg, water 10kg, trehalose 0.2 kg, 1,2-hexanediol 0.01kg, p-hydroxyacetophenone 0.02kg, glycerol 0.1kg, squalane 0.03kg, caprylic/capric triglyceride 0.01kg, isononyl isononanoate 0.02kg, hydrogenated Lecithin 0.03kg, PEG-100.02kg, soy sterol 0.02kg, disodium EDTA 0.04kg, tocop
  • the preparation method of the moisturizing and hydrating facial mask composition of this embodiment is as follows: including the following steps:
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the moisturizing and hydrating facial mask composition of this embodiment is made from the following raw materials: Rosa Turkica flower water 60kg, Portulaca oleracea extract 0.04kg, Dendrobium officinale extract 1.3kg, White truffle fungus extract 1.2kg, Snow lotus extract 1.3 kg, Tremella fruiting body extract 1.5kg, Centella asiatica extract 1.2kg, soybean seed extract 1.2kg, tea extract 1.3kg, tetrandrine extract 0.09kg, Altai Bupleurum root extract 1.4kg, apple fruit cells Culture extract 0.3kg, Ylang ylang extract 1.5kg, Spring Ulmus root extract 1.4kg, False leaf root extract 0.9kg, Echinacea purpurea extract 1.2kg, Paeonia suffruticosa root bark extract 0.9kg, Butylene glycol 0.6 kg, water 14kg, trehalose 0.3kg, 1,2-hexanediol 0.03kg, p-hydroxyacetophenone 0.04kg, glycerol 0.4
  • the spring elm root extract, pseudoleaf tree root extract, and tree peony root bark extract described in this embodiment are all extracted by the following methods:
  • the preparation method of the moisturizing and hydrating facial mask composition of this embodiment is as follows: including the following steps:
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the moisturizing and hydrating facial mask composition of this embodiment is made from the following raw materials: 65kg of rose flower water, 0.05kg of portulaca extract, 1.4kg of Dendrobium candidum extract, 1.3kg of white truffle extract, and 1.4 kg of snow lotus extract.
  • Tremella fruiting body extract 1.6kg, Centella asiatica extract 1.3kg, soybean seed extract 1.3kg, tea extract 1.4kg, tetrandrine extract 0.10kg, Altai Bupleurum root extract 1.5kg, apple fruit cells Culture extract 0.4kg, Ylang ylang extract 1.6kg, Spring Ulmus root extract 1.5kg, Fake leaf tree root extract 1.0kg, Echinacea purpurea extract 1.25kg, Paeonia suffruticosa root bark extract 0.10kg, Butylene glycol 0.7 kg, water 15kg, trehalose 0.4kg, 1,2-hexanediol 0.035kg, p-hydroxyacetophenone 0.05kg, glycerol 0.45kg, squalane 0.045kg, caprylic/capric triglyceride 0.035kg, isonon Isononyl acid 0.03kg, hydrogenated lecithin 0.05kg, PEG-10 0.04kg, soy sterol 0.04kg, disodium EDTA
  • the spring elm root extract, pseudoleaf tree root extract, and tree peony root bark extract described in this embodiment are all extracted by the following methods:
  • the preparation method of the moisturizing and hydrating facial mask composition of this embodiment is as follows: including the following steps:
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the facial mask composition obtained above is injected into the film base material of the fiber facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the moisturizing and hydrating facial mask composition of the present embodiment includes the following raw materials: 70kg of rose flower water, 0.06kg of portulaca extract, 1.5kg of Dendrobium officinale extract, 1.4kg of white truffle fungus extract, and 1.5 of snow lotus extract kg, Tremella fruiting body extract 1.7kg, Centella asiatica extract 1.4kg, soybean seed extract 1.4kg, tea extract 1.5kg, tetrandrine extract 0.11kg, Altai Bupleurum root extract 1.6kg, apple fruit cells 0.5kg of culture extract, 1.7kg of ylang-ylang extract, 1.6kg of spring elm root extract, 1.1kg of pseudoleaf root extract, 1.3kg of purple echinacea extract, 0.11kg of tree peony root bark extract, 0.8kg of butanediol kg, water 16kg, trehalose 0.5kg, 1,2-hexanediol 0.04kg, p-hydroxyacetophenone 0.06kg, glycerol
  • the spring elm root extract, pseudoleaf tree root extract, and tree peony root bark extract described in this embodiment are all extracted by the following methods:
  • the preparation method of the moisturizing and hydrating facial mask composition of this embodiment is as follows: including the following steps:
  • the facial mask composition obtained above is injected into the film base material of the fiber facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the moisturizing and hydrating facial mask composition of this embodiment is made from the following raw materials: 80kg of rose flower water, 0.07kg of portulaca extract, 1.6kg of Dendrobium officinale extract, 1.5kg of white truffle extract, and 1.6kg of snow lotus extract kg, Tremella fruiting body extract 1.9kg, Centella asiatica extract 1.5kg, soybean seed extract 1.5kg, tea extract 1.6kg, tetrandrine extract 0.12kg, Altai Bupleurum root extract 2.0kg, apple fruit cells 0.6kg of culture extract, 1.9kg of ylang-ylang extract, 1.8kg of spring elm root extract, 1.2kg of pseudoleaf root extract, 1.5kg of purple echinacea extract, 0.12kg of tree peony root bark extract, butylene glycol 1.0 kg, water 20kg, trehalose 0.6kg, 1,2-hexanediol 0.06kg, p-hydroxyacetophenone 0.08kg, glycerol 0.8kg, squalane
  • the spring elm root extract, pseudoleaf tree root extract, and tree peony root bark extract described in this embodiment are all extracted by the following methods:
  • the preparation method of the moisturizing and hydrating facial mask composition of this embodiment is as follows: including the following steps:
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the facial mask composition obtained above is injected into the film substrate of the fibrous facial mask through a filling machine, and the distribution is uniform to obtain a moisturizing and hydrating facial mask.
  • the moisturizing and hydrating facial mask composition prepared in this comparative example is the same as that of Example 2, except that the spring elm root extract uses commercially available raw materials, the manufacturer Xi'an Tianrui Biotechnology Co., Ltd.
  • the moisturizing and hydrating facial mask composition prepared in this comparative example is the same as that of Example 2, except that the false leaf tree root extract uses commercially available raw materials, manufactured by Sanyuan Tianyu Biological Products Co., Ltd.
  • the moisturizing and hydrating facial mask composition prepared in this comparative example is the same as in Example 2, except that the peony root bark extract uses commercially available raw materials, manufactured by Wuhan Xinxin Jiali Biotechnology Co., Ltd.
  • Example 2-5 It can be seen from the above table that the water growth rate of Example 2-5 is higher than that of Example 1 at the same time. This is due to the addition of Altai Bupleurum root extract and apple fruit cell culture in Example 2-5
  • the synergistic effect of various raw materials such as extracts, ylang-ylang flower extract, spring elm root extract, pseudoleaf root extract, purple echinacea extract, tree peony root bark extract, the synergistic effect of various raw materials can increase the moisture content of the skin.
  • Comparative Examples 1-3 and Example 2-5 it can be seen that the skin moisture growth rate of Comparative Examples 1-3 is significantly lower than that of Example 2-5. This is due to the use of the plant extract prepared by the method of the present invention. The material has a better moisturizing and moisturizing effect.

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Abstract

提供保湿补水面膜组合物、面膜及其制备方法，所述面膜组合物包含水、辅料和植物提取物，所述的植物提取物包括突厥蔷薇花水、马齿苋提取物、铁皮石斛提取物、白松露菌提取物、雪莲花提取物、银耳子实体提取物、积雪草提取物、大豆籽提取物、茶叶提取物和粉防己提取物。该面膜组合物采用天然原料提取物制成，具有使皮肤深层补水和表层锁水双重保湿的效果，可以使皮肤迅速吸收，修复皮肤细纹，提高皮肤抵御能力，淡化痘印，对皮肤无刺激，同时其制备方法简单，易于推广。

Description

一种保湿补水面膜组合物、面膜及其制备方法 技术领域
本发明属于化妆品技术领域，具体涉及一种保湿补水面膜组合物、面膜及其制备方法。
背景技术
面膜是护肤品中的一个类别，是美容保养品的一种载体，敷在脸上用于美容功能例如补水保湿、美白、抗衰老、平衡油脂等。面膜的原理，就是利用覆盖在脸部的短暂时间，暂时隔离外界的空气与污染，提高肌肤温度，皮肤的毛孔扩张，促进汗腺分泌与新陈代谢，使肌肤的含氧量上升，有利于肌肤排除表皮细胞新陈代谢的产物和累积的油脂类物质，面膜中的水分渗入表皮的角质层，皮肤变得柔软，肌肤自然光亮有弹性。随着人们生活水平的提高，对面膜的要求也越来越高，高质量的面膜品类护肤品需求量逐渐增加。
其中，保湿是护肤永远的主题，是保证皮肤健康、延缓衰老的重要条件，一方面随着年龄的增长，皮肤保湿结构受到损失，皮肤组织细胞和细胞间的水份含量减少，当角质层水份下降到10％以下时，皮肤就会显得干燥、失去弹性、起皱、加速皮肤老化；另一方面，皮肤遭受炎热、寒冷、风吹、清洁剂、紫外线辐射等侵害，表面会变得更加干燥。因此，如何保持皮肤的水份，减少水份散失非常重要。
目前市场上的保湿补水面膜效果不佳，安全性能不稳定，没能从根本上改善皮肤问题。
鉴于以上原因，特提出本发明。
发明内容
为了解决现有技术存在的以上问题，本发明提供了一种保湿补水面膜组合物、面膜及其制备方法，本发明的组合物选择天然原料提取物，安全、有效，能被肌肤快速吸收，保湿效果卓越，同时有效锁住水分。
本发明的第一目的提供了一种保湿补水面膜组合物，包含水、辅料和植物提取物，所述的植物提取物包括突厥蔷薇花水、马齿苋提取物、铁皮石斛提取物、白松露菌提取物、雪莲花提取物、银耳子实体提取物、积雪草提取物、大豆籽提取物、茶叶提取物和粉防己提取物。
突厥蔷薇花水优选大马士革玫瑰花，经过精制蒸馏，具有天然保湿功能，可促进水分深层吸收，改善干燥皮肤，淡化细纹，具有天然的香味。马齿苋提取物具有在冬季防干燥老化、增加皮肤舒适度以及清除自由基，改善皮肤舒适感等的综合性能。
铁皮石斛提取物石斛是兰科草本植物，在古代被奉为“养生圣品”；在古代民间，它有着“救命仙草”的美誉。铁皮石斛含有的黏液质，对人体皮肤有滋润营养作用，能使人皮肤光滑、永葆青春。其核心活性成分系铁皮石斛多糖，具有活化巨噬细胞、抗氧化、增强免疫力，抗衰老、抑菌消炎等作用。
白松露菌提取物可以抑制黑色素生成，促进肌肤内在代谢，焕活细胞活力新生，为肌肤提供健康能量。
雪莲花提取物对于平滑肌也有一定的调节作用。这是因为雪莲总碱它能作用于组胺，让平滑肌痉挛有所缓解。第三，它具有着抗炎的效果和作用。
银耳子实体提取物一种物源性的类透明质酸，从银耳中提取出来的水溶性高分子异多糖具有超越透明质酸的保湿性能，能保持490倍的水，极为优异的成膜性及无比滑爽的感觉，极佳的护肤效果。增强细胞免疫功能，清除自由基抗氧化、抗衰老、补充营养，增加皮肤弹性，减小皮肤纹理。
积雪草提取物积雪草提取物能够显著增加角质层的水合程度，这主要与积雪草提取物中的三萜皂苷化合物有关，积雪草三萜皂苷是一种亲水性糖链，主要是葡萄糖和鼠李糖，能够在闭塞层内与水结合，提高表皮屏障能力，增强皮肤水分。
大豆籽提取物含有丰富的黄酮等成分，能够促进纤维芽细胞的生长，具有活肤，抗衰老的作用；同时能保持皮肤的水分，有保湿功效。
茶叶提取物它还是一种新型天然抗氧化剂，在常温和低浓度下具有很强的抗氧化作用，对胶原酶和弹性蛋白酶有抑制作用，可阻止弹性蛋白质的含量下降或变性，维持皮肤弹性，达到抗皱效果。
粉防己提取物具有亮肤、抗敏、消炎之强效，用后皮肤很健康，有光泽。
作为一种优选的实施方式，所述的植物提取物还包括阿尔泰柴胡根提取物、苹果果实细胞培养物提取物、依兰花提取物、春榆根提取物、假叶树根提取物、紫松果菊提取物、牡丹根皮提取物。
阿尔泰柴胡根提取物其含挥发油、柴胡醇、油酸、亚麻酸、棕榈酸、硬脂酸、廿四酸、葡萄糖及皂甙等，抗炎作用，抗病原体作用，植物性天然提取物，含维生素丙和多种营养成分，具有多种功效，成分多样，在植物上经过提取后，是肌肤调理上的特色成分。主要的活性成分柴胡皂苷对人体细胞的免疫体制有增强作用，可改善皮肤新陈代谢机能，增加毛细血管的通透量，使皮层细胞增殖。凝血酸、甘草酸和脲素等都能增强柴胡皂苷的功效，其协同有愈伤、柔滑粗糙皮肤、防止皮肤老化等，柴胡皂苷可吸收紫外线，体外试验表明也有抑制黑色素形成的作用。柴胡皂苷经皮渗透性好，能加速其他成分的经皮渗入。具强烈的抗氧化性、有抗炎、抗病毒等作用。其含有的尿苷能加速皮肤细胞的新陈代谢和皮肤角质层的再生。
苹果果实细胞培养物提取物对多种自由基有消除作用，可用作抗氧化剂，这与内含的若干原花青素物质有关；对荧光素酶活性的低下是皮肤易发特异性皮炎的标志，因此具有抗炎性；另可用作活肤抗皱剂、保湿剂和减肥剂。
依兰花提取物可以保持皮肤的水分，维持皮肤弹性，有保湿的功效。
春榆根提取物具有优良的抗氧化、抗菌、抗炎、分散能力。
假叶树根提取物有效成分主要是螺旋甾烷类和黄酮类化合物，促进血液循环畅通，可增强皮肤细胞新陈代谢，具有保湿的功效。
紫松果菊提取物具有优良的抗氧化、抗菌、抗炎、分散能力，作为调理剂、保湿剂、滋补剂等，应用于个人护理用品领域。
牡丹根皮提取物对金属蛋白酶和弹性蛋白酶有抑制作用，对组织蛋白酶有激活作用，均表明其具有活肤和抗衰功能，结合优秀的抗氧化性，可用于抗老化化妆品；对胶原蛋白纤维凝胶有较好的收缩作用，表示对皮肤的真皮层有收敛作用，可用于紧肤和去眼袋的化妆品中；有很好的抗菌和抗炎性，可用于粉刺的防治。
作为一种优选的实施方式，所述的辅料包括丁二醇、海藻糖、1,2-己二醇、对羟基苯乙酮、甘油、角鲨烷、辛酸/癸酸甘油三酯、异壬酸异壬酯、氢化卵磷脂、PEG-10大豆甾醇、EDTA二钠、生育酚乙酸酯、苯氧乙醇、黄原胶、乙基己基甘油、羟基化卵磷脂、尿囊素、β-葡聚糖、木糖醇基葡糖苷、脱水木糖醇、木糖醇、葡萄糖、泛醇、羟乙基纤维素、甘草酸二钾、透明质酸钠、聚谷氨酸钠、丙二醇、牛磺酸、氨基丁酸、苏氨酸、组氨酸、天冬酰胺、瓜氨酸、柠檬酸和滨海剌芹愈伤组织培养物滤液。
作为一种优选的实施方式，所述的辅料还包括鳄梨油、水解胶原、葡萄糖酸钙、蜂蜜、鲸蜡硬脂基葡糖苷、芝麻籽油和滇山茶籽油。
作为一种优选的实施方式，按照重量份，所述的组合物包括如下成分：突厥蔷薇花水30-80份、马齿苋提取物0.03-0.07份、铁皮石斛提取物1.2-1.6份、白松露菌提取物1.1-1.5份、雪莲花提取物1.2-1.6份、银耳子实体提取物1.3-1.9份、积雪草提取物1.1-1.5份、大豆籽提取物1.1-1.5份、茶叶提取物1.2-1.6份、粉防己提取物0.08-0.12份、阿尔泰柴胡根提取物1.0-2.0份、苹果果实细胞培养物提取物0.2-0.6份、依兰花提取物1.3-1.9份、春榆根提取物1.2-1.8份、假叶树根提取物0.8-1.2份、紫松果菊提取物1.0-1.5份、牡丹根皮提取物0.8-0.12份、丁二醇0.4-1.0份、水10-20份、海藻糖0.2-0.6份、1,2-己二醇0.01-0.06份、对羟基苯乙酮0.02-0.08份、甘油0.1-0.8份、角鲨烷0.03-0.06份、辛酸/癸酸甘油三酯0.01-0.06份、异壬酸异壬酯0.02-0.04份、氢化卵磷脂0.03-0.07份、PEG-10 0.02-0.06份、大豆甾醇0.02-0.06份、EDTA二钠0.04-0.08份、生育酚乙酸酯0.03-0.05份、苯氧乙醇0.05-0.07份、黄原胶1.0-1.4份、乙基己基甘油0.02-0.06份、羟基化卵磷脂0.002-0.008份、尿囊素0.003-0.005份、β-葡聚糖0.03-0.07份、木糖醇基葡糖苷0.02-0.06份、脱水木糖醇0.003-0.005份、木糖醇0.2-0.6份、葡萄糖1.2-1.6份、泛醇0.4-0.6份、羟乙基纤维素0.04-0.08份、甘草酸二钾0.03-0.05份、透明质酸钠0.06-0.10份、聚谷氨酸钠0.03-0.07份、丙二醇0.1-0.3份、牛磺酸0.03-0.05份、氨基丁酸0.04-0.06份、苏氨酸0.02-0.06份、组氨酸0.01-0.05份、天冬酰胺0.02-0.06份、瓜氨酸0.02-0.06份、柠檬酸0.01-0.05份、滨海剌芹愈伤组织培养物滤液0.04-0.08份、鳄梨油1.2-1.8份、水解胶原0.1-0.5份、葡萄糖酸钙0.04-0.08份、蜂蜜1.2-1.8份、鲸蜡硬脂基葡糖苷0.3-0.5份、芝麻籽油0.2-0.4份和滇山茶籽油0.04-0.08份。
作为一种优选的实施方式，按照重量份，所述的组合物包括如下成分：突厥蔷薇花水60-70份、马齿苋提取物0.04-0.06份、铁皮石斛提取物1.3-1.5份、白松露菌提取物1.2-1.4份、雪莲花提取物1.3-1.5份、银耳子实体提取物1.5-1.7份、积雪草提取物1.2-1.4份、大豆籽提取物1.2-1.4份、茶叶提取物1.3-1.5份、粉防己提取物0.09-0.11份、阿尔泰柴胡根提取物1.4-1.6份、苹果果实细胞培养物提取物0.3-0.5份、依兰花提取物1.5-1.7份、春榆根提取物1.4-1.6份、假叶树根提取物0.9-1.1份、紫松果菊提取物1.2-1.3份、牡丹根皮提取物0.9-0.11份、丁二醇0.6-0.8份、水14-16份、海藻糖0.3-0.5份、1,2-己二醇0.03-0.04份、对羟基苯乙酮0.04-0.06份、甘油0.4-0.5份、角鲨烷0.04-0.05份、辛酸/癸酸甘油三酯0.03-0.04份、异壬酸异壬酯0.025-0.035份、氢化卵磷脂0.04-0.05份、PEG-10 0.03-0.05份、大豆甾醇0.03-0.05份、EDTA二钠0.05-0.07份、生育酚乙酸酯0.035-0.045份、苯氧乙醇0.055-0.065份、黄原胶1.1-1.3份、乙基己基甘油0.03-0.05份、羟基化卵磷脂0.004-0.006份、尿囊素0.0035-0.0045份、β-葡聚糖0.04-0.06份、木糖醇基葡糖苷0.03-0.05份、脱水木糖醇0.0035-0.0045份、木糖醇0.3-0.5份、葡萄糖1.3-1.5份、泛醇0.45-0.55份、羟乙基纤维素0.05-0.07份、甘草酸二钾0.035-0.045份、透明质酸钠0.07-0.09份、聚谷氨酸 钠0.04-0.06份、丙二醇0.15-0.25份、牛磺酸0.035-0.045份、氨基丁酸0.045-0.055份、苏氨酸0.03-0.05份、组氨酸0.02-0.04份、天冬酰胺0.03-0.05份、瓜氨酸0.03-0.05份、柠檬酸0.02-0.04份、滨海剌芹愈伤组织培养物滤液0.05-0.07份、鳄梨油1.4-1.6份、水解胶原0.2-0.4份、葡萄糖酸钙0.05-0.07份、蜂蜜1.4-1.6份、鲸蜡硬脂基葡糖苷0.35-0.45份、芝麻籽油0.25-0.35份和滇山茶籽油0.05-0.07份。
作为一种优选的实施方式，按照重量份，所述的组合物包括如下成分：突厥蔷薇花水65份、马齿苋提取物0.05份、铁皮石斛提取物1.4份、白松露菌提取物1.3份、雪莲花提取物1.4份、银耳子实体提取物1.6份、积雪草提取物1.3份、大豆籽提取物1.3份、茶叶提取物1.4份、粉防己提取物0.10份、阿尔泰柴胡根提取物1.5份、苹果果实细胞培养物提取物0.4份、依兰花提取物1.6份、春榆根提取物1.5份、假叶树根提取物1.0份、紫松果菊提取物1.25份、牡丹根皮提取物0.10份、丁二醇0.7份、水15份、海藻糖0.4份、1,2-己二醇0.035份、对羟基苯乙酮0.05份、甘油0.45份、角鲨烷0.045份、辛酸/癸酸甘油三酯0.035份、异壬酸异壬酯0.03份、氢化卵磷脂0.05份、PEG-10 0.04份、大豆甾醇0.04份、EDTA二钠0.06份、生育酚乙酸酯0.04份、苯氧乙醇0.06份、黄原胶1.2份、乙基己基甘油0.04份、羟基化卵磷脂0.005份、尿囊素0.004份、β-葡聚糖0.05份、木糖醇基葡糖苷0.04份、脱水木糖醇0.004份、木糖醇0.4份、葡萄糖1.4份、泛醇0.5份、羟乙基纤维素0.06份、甘草酸二钾0.04份、透明质酸钠0.08份、聚谷氨酸钠0.05份、丙二醇0.2份、牛磺酸0.04份、氨基丁酸0.05份、苏氨酸0.04份、组氨酸0.03份、天冬酰胺0.04份、瓜氨酸0.04份、柠檬酸0.03份、滨海剌芹愈伤组织培养物滤液0.06份、鳄梨油1.5份、水解胶原0.3份、葡萄糖酸钙0.06份、蜂蜜1.5份、鲸蜡硬脂基葡糖苷0.4份、芝麻籽油0.3份和滇山茶籽油0.06份。
本发明采用突厥蔷薇花水用量比水的多，突厥蔷薇花水作为主要的功效成分，同时也充当溶剂的角色。
作为一种优选的实施方式，所述的春榆根提取物、假叶树根提取物和牡丹根皮提取物均采用如下方法提取：
(1)分别将春榆根、假叶树根和牡丹根皮粉碎，过30-50目筛，加入其重量10-14倍的水浸泡8-12h，用水蒸汽蒸馏，收集馏出液，剩余物进行过滤，收集滤饼；
(2)将所述的滤饼加入其重量6-8倍的体积浓度为95％的乙醇进行超声提取，将提取液与蒸馏液合并，得到所述的提取物。
本发明的春榆根提取物、假叶树根提取物和牡丹根皮提取物经过特定的提取方法提取而成，本发明的提取物可以深入肌肤底层补充水分，本发明的组合物使皮肤迅速吸收，还可以有效减少透皮水分流失，锁住水分，改善肌肤松弛、干燥等状况。
本发明的第二目的提供了一种所述的保湿补水面膜组合物的制备方法，包括如下步骤：
(a)按照各原料的重量分别称取备用；
(b)将水和辅料混合，加热至完全溶解，得到混合溶液A；
(c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
作为一种优选的实施方式，其特征在于，步骤(b)中加热至35-45℃。
本发明的第三目的提供了一种面膜，包括所述的保湿补水面膜组合物。
本发明的面膜可以是以蚕丝网、棉或麻纤维的薄膜，可以制成不用的载体，也可以是直接涂抹在脸上的面膜。
与现有技术相比，本发明的有益效果为：
(1)本发明的面膜组合物采用天然原料提取物制成，可以使皮肤深层补水和表层锁水双重保湿的效果，通过各原料的协同作用，可以使皮肤迅速吸收，修复皮肤细纹，提高皮肤抵御能力，还可以减少透皮水分的流失，锁住水分， 具有很好的保湿锁水性能，保湿效果较好，对皮肤无刺激，同时本发明的组合物制备方法简单，可以大规模生产，易于推广；
(2)本发明的春榆根提取物、假叶树根提取物和牡丹根皮提取物经过特定的提取方法提取而成，本发明的提取物可以深入肌肤底层补充水分，本发明的组合物使皮肤迅速吸收，淡化痘印，还可以有效减少透皮水分流失，锁住水分，改善肌肤松弛、干燥等状况，通过本发明的方法制备的提取物可以更完全溶解在水中，也更容易被人体吸收，能最大限度的发挥其价值，具有更好的保湿补水的作用。
具体实施方式
为使本发明的目的、技术方案和优点更加清楚，下面将对本发明的技术方案进行详细的描述。显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动的前提下所得到的所有其它实施方式，都属于本发明所保护的范围。
实施例1
本实施例的保湿补水面膜组合物，包括如下原料制成：突厥蔷薇花水30kg、马齿苋提取物0.03kg、铁皮石斛提取物1.2kg、白松露菌提取物1.1kg、雪莲花提取物1.2kg、银耳子实体提取物1.3kg、积雪草提取物1.1kg、大豆籽提取物1.1kg、茶叶提取物1.2kg、粉防己提取物0.08kg、丁二醇0.4kg、水10kg、海藻糖0.2kg、1,2-己二醇0.01kg、对羟基苯乙酮0.02kg、甘油0.1kg、角鲨烷0.03kg、辛酸/癸酸甘油三酯0.01kg、异壬酸异壬酯0.02kg、氢化卵磷脂0.03kg、PEG-100.02kg、大豆甾醇0.02kg、EDTA二钠0.04kg、生育酚乙酸酯0.03kg、苯氧乙醇0.05kg、黄原胶1.0kg、乙基己基甘油0.02kg、羟基化卵磷脂0.002kg、尿囊素0.003kg、β-葡聚糖0.03kg、木糖醇基葡糖苷0.02kg、脱水木糖醇0.003kg、木糖醇0.2kg、葡萄糖1.2kg、泛醇0.4kg、羟乙基纤维素0.04kg、甘草酸二钾0.03kg、透明质酸钠0.06kg、聚谷氨酸钠0.03kg、丙二醇0.1kg、牛磺酸0.03kg、氨基丁酸0.04kg、苏氨酸0.02kg、组氨酸0.01kg、天冬酰胺0.02kg、瓜氨酸0.02kg、 柠檬酸0.01kg、滨海剌芹愈伤组织培养物滤液0.04kg。
本实施例的保湿补水面膜组合物的制备方法如下：包括如下步骤：
(a)按照各原料的重量分别称取备用；
(b)将水和辅料混合，加热至35℃完全溶解，得到混合溶液A；
(c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
实施例2
本实施例的保湿补水面膜组合物，包括如下原料制成：突厥蔷薇花水60kg、马齿苋提取物0.04kg、铁皮石斛提取物1.3kg、白松露菌提取物1.2kg、雪莲花提取物1.3kg、银耳子实体提取物1.5kg、积雪草提取物1.2kg、大豆籽提取物1.2kg、茶叶提取物1.3kg、粉防己提取物0.09kg、阿尔泰柴胡根提取物1.4kg、苹果果实细胞培养物提取物0.3kg、依兰花提取物1.5kg、春榆根提取物1.4kg、假叶树根提取物0.9kg、紫松果菊提取物1.2kg、牡丹根皮提取物0.9kg、丁二醇0.6kg、水14kg、海藻糖0.3kg、1,2-己二醇0.03kg、对羟基苯乙酮0.04kg、甘油0.4kg、角鲨烷0.04kg、辛酸/癸酸甘油三酯0.03kg、异壬酸异壬酯0.025kg、氢化卵磷脂0.04kg、PEG-10 0.03kg、大豆甾醇0.03kg、EDTA二钠0.05kg、生育酚乙酸酯0.035kg、苯氧乙醇0.055kg、黄原胶1.1kg、乙基己基甘油0.03kg、羟基化卵磷脂0.004kg、尿囊素0.0035kg、β-葡聚糖0.04kg、木糖醇基葡糖苷0.03kg、脱水木糖醇0.0035kg、木糖醇0.3kg、葡萄糖1.3kg、泛醇0.45kg、羟乙基纤维素0.05kg、甘草酸二钾0.035kg、透明质酸钠0.07kg、聚谷氨酸钠0.04kg、丙二醇0.15kg、牛磺酸0.035kg、氨基丁酸0.045kg、苏氨酸0.03kg、组氨酸0.02kg、天冬酰胺0.03kg、瓜氨酸0.03kg、柠檬酸0.02kg、滨海剌芹愈伤组织培养物滤液0.05kg、鳄梨油1.4kg、水解胶原0.2kg、葡萄糖酸钙0.05kg、蜂蜜1.4kg、鲸蜡硬脂基葡糖苷0.35kg、芝麻籽油0.25kg和滇山茶籽油0.05kg。
本实施例中所述的春榆根提取物、假叶树根提取物和牡丹根皮提取物均采用如下方法提取：
(1)分别将春榆根、假叶树根和牡丹根皮粉碎，过30-50目筛，加入其重量10倍的水浸泡8h，用水蒸汽蒸馏，收集馏出液，剩余物进行过滤，收集滤饼；
(2)将所述的滤饼加入其重量6倍的体积浓度为95％的乙醇进行超声提取，将提取液与蒸馏液合并，得到所述的提取物。
本实施例的保湿补水面膜组合物的制备方法如下：包括如下步骤：
(a)按照各原料的重量分别称取备用；
(b)将水和辅料混合，加热至40℃完全溶解，得到混合溶液A；
(c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
实施例3
本实施例的保湿补水面膜组合物，包括如下原料制成：突厥蔷薇花水65kg、马齿苋提取物0.05kg、铁皮石斛提取物1.4kg、白松露菌提取物1.3kg、雪莲花提取物1.4kg、银耳子实体提取物1.6kg、积雪草提取物1.3kg、大豆籽提取物1.3kg、茶叶提取物1.4kg、粉防己提取物0.10kg、阿尔泰柴胡根提取物1.5kg、苹果果实细胞培养物提取物0.4kg、依兰花提取物1.6kg、春榆根提取物1.5kg、假叶树根提取物1.0kg、紫松果菊提取物1.25kg、牡丹根皮提取物0.10kg、丁二醇0.7kg、水15kg、海藻糖0.4kg、1,2-己二醇0.035kg、对羟基苯乙酮0.05kg、甘油0.45kg、角鲨烷0.045kg、辛酸/癸酸甘油三酯0.035kg、异壬酸异壬酯0.03kg、 氢化卵磷脂0.05kg、PEG-10 0.04kg、大豆甾醇0.04kg、EDTA二钠0.06kg、生育酚乙酸酯0.04kg、苯氧乙醇0.06kg、黄原胶1.2kg、乙基己基甘油0.04kg、羟基化卵磷脂0.005kg、尿囊素0.004kg、β-葡聚糖0.05kg、木糖醇基葡糖苷0.04kg、脱水木糖醇0.004kg、木糖醇0.4kg、葡萄糖1.4kg、泛醇0.5kg、羟乙基纤维素0.06kg、甘草酸二钾0.04kg、透明质酸钠0.08kg、聚谷氨酸钠0.05kg、丙二醇0.2kg、牛磺酸0.04kg、氨基丁酸0.05kg、苏氨酸0.04kg、组氨酸0.03kg、天冬酰胺0.04kg、瓜氨酸0.04kg、柠檬酸0.03kg、滨海剌芹愈伤组织培养物滤液0.06kg、鳄梨油1.5kg、水解胶原0.3kg、葡萄糖酸钙0.06kg、蜂蜜1.5kg、鲸蜡硬脂基葡糖苷0.4kg、芝麻籽油0.3kg和滇山茶籽油0.06kg。
本实施例中所述的春榆根提取物、假叶树根提取物和牡丹根皮提取物均采用如下方法提取：
(1)分别将春榆根、假叶树根和牡丹根皮粉碎，过30-50目筛，加入其重量12倍的水浸泡10h，用水蒸汽蒸馏，收集馏出液，剩余物进行过滤，收集滤饼；
(2)将所述的滤饼加入其重量7倍的体积浓度为95％的乙醇进行超声提取，将提取液与蒸馏液合并，得到所述的提取物。
本实施例的保湿补水面膜组合物的制备方法如下：包括如下步骤：
(a)按照各原料的重量分别称取备用；
(b)将水和辅料混合，加热至40℃完全溶解，得到混合溶液A；
(c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
实施例4
本实施例的保湿补水面膜组合物，包括如下原料制成：突厥蔷薇花水70kg、马齿苋提取物0.06kg、铁皮石斛提取物1.5kg、白松露菌提取物1.4kg、雪莲花提取物1.5kg、银耳子实体提取物1.7kg、积雪草提取物1.4kg、大豆籽提取物1.4kg、茶叶提取物1.5kg、粉防己提取物0.11kg、阿尔泰柴胡根提取物1.6kg、苹果果实细胞培养物提取物0.5kg、依兰花提取物1.7kg、春榆根提取物1.6kg、假叶树根提取物1.1kg、紫松果菊提取物1.3kg、牡丹根皮提取物0.11kg、丁二醇0.8kg、水16kg、海藻糖0.5kg、1,2-己二醇0.04kg、对羟基苯乙酮0.06kg、甘油0.5kg、角鲨烷0.05kg、辛酸/癸酸甘油三酯0.04kg、异壬酸异壬酯0.035kg、氢化卵磷脂0.05kg、PEG-10 0.05kg、大豆甾醇0.05kg、EDTA二钠0.07kg、生育酚乙酸酯0.045kg、苯氧乙醇0.065kg、黄原胶1.3kg、乙基己基甘油0.05kg、羟基化卵磷脂0.006kg、尿囊素0.0045kg、β-葡聚糖0.06kg、木糖醇基葡糖苷0.05kg、脱水木糖醇0.0045kg、木糖醇0.5kg、葡萄糖1.5kg、泛醇0.55kg、羟乙基纤维素0.07kg、甘草酸二钾0.045kg、透明质酸钠0.09kg、聚谷氨酸钠0.06kg、丙二醇0.25kg、牛磺酸0.045kg、氨基丁酸0.055kg、苏氨酸0.05kg、组氨酸0.04kg、天冬酰胺0.05kg、瓜氨酸0.05kg、柠檬酸0.04kg、滨海剌芹愈伤组织培养物滤液0.07kg、鳄梨油1.6kg、水解胶原0.4kg、葡萄糖酸钙0.07kg、蜂蜜1.6kg、鲸蜡硬脂基葡糖苷0.45kg、芝麻籽油0.35kg和滇山茶籽油0.07kg。
本实施例中所述的春榆根提取物、假叶树根提取物和牡丹根皮提取物均采用如下方法提取：
(1)分别将春榆根、假叶树根和牡丹根皮粉碎，过30-50目筛，加入其重量14倍的水浸泡12h，用水蒸汽蒸馏，收集馏出液，剩余物进行过滤，收集滤饼；
(2)将所述的滤饼加入其重量8倍的体积浓度为95％的乙醇进行超声提取，将提取液与蒸馏液合并，得到所述的提取物。
本实施例的保湿补水面膜组合物的制备方法如下：包括如下步骤：
(a)按照各原料的重量分别称取备用；
(b)将水和辅料混合，加热至45℃完全溶解，得到混合溶液A；
(c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
实施例5
本实施例的保湿补水面膜组合物，包括如下原料制成：突厥蔷薇花水80kg、马齿苋提取物0.07kg、铁皮石斛提取物1.6kg、白松露菌提取物1.5kg、雪莲花提取物1.6kg、银耳子实体提取物1.9kg、积雪草提取物1.5kg、大豆籽提取物1.5kg、茶叶提取物1.6kg、粉防己提取物0.12kg、阿尔泰柴胡根提取物2.0kg、苹果果实细胞培养物提取物0.6kg、依兰花提取物1.9kg、春榆根提取物1.8kg、假叶树根提取物1.2kg、紫松果菊提取物1.5kg、牡丹根皮提取物0.12kg、丁二醇1.0kg、水20kg、海藻糖0.6kg、1,2-己二醇0.06kg、对羟基苯乙酮0.08kg、甘油0.8kg、角鲨烷0.06kg、辛酸/癸酸甘油三酯0.06kg、异壬酸异壬酯0.04kg、氢化卵磷脂0.07kg、PEG-10 0.06kg、大豆甾醇0.06kg、EDTA二钠0.08kg、生育酚乙酸酯0.05kg、苯氧乙醇0.07kg、黄原胶1.4kg、乙基己基甘油0.06kg、羟基化卵磷脂0.008kg、尿囊素0.005kg、β-葡聚糖0.07kg、木糖醇基葡糖苷0.06kg、脱水木糖醇0.005kg、木糖醇0.6kg、葡萄糖1.6kg、泛醇0.6kg、羟乙基纤维素0.08kg、甘草酸二钾0.05kg、透明质酸钠0.10kg、聚谷氨酸钠0.07kg、丙二醇0.3kg、牛磺酸0.05kg、氨基丁酸0.06kg、苏氨酸0.06kg、组氨酸0.05kg、天冬酰胺0.06kg、瓜氨酸0.06kg、柠檬酸0.05kg、滨海剌芹愈伤组织培养物滤液0.08kg、鳄梨油1.8kg、水解胶原0.5kg、葡萄糖酸钙0.08kg、蜂蜜1.8kg、鲸蜡硬脂基葡糖苷0.5kg、芝麻籽油0.4kg和滇山茶籽油0.08kg。
本实施例中所述的春榆根提取物、假叶树根提取物和牡丹根皮提取物均采用如下方法提取：
(1)分别将春榆根、假叶树根和牡丹根皮粉碎，过30-50目筛，加入其重量11倍的水浸泡11h，用水蒸汽蒸馏，收集馏出液，剩余物进行过滤，收集滤饼；
(2)将所述的滤饼加入其重量6.5倍的体积浓度为95％的乙醇进行超声提取，将提取液与蒸馏液合并，得到所述的提取物。
本实施例的保湿补水面膜组合物的制备方法如下：包括如下步骤：
(a)按照各原料的重量分别称取备用；
(b)将水和辅料混合，加热至42℃完全溶解，得到混合溶液A；
(c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
将上述得到的面膜组合物通过灌装机注入纤维面膜的膜基材，分布均匀，得到保湿补水面膜。
对比例1
本对比例制备的保湿补水面膜组合物与实施例2均相同，不同之处在于，春榆根提取物采用市售的原料，生产厂家西安天瑞生物技术有限公司。
对比例2
本对比例制备的保湿补水面膜组合物与实施例2均相同，不同之处在于，假叶树根提取物采用市售的原料，生产厂家三原天域生物制品有限公司。
对比例3
本对比例制备的保湿补水面膜组合物与实施例2均相同，不同之处在于， 牡丹根皮提取物采用市售的原料，生产厂家武汉欣欣佳丽生物科技有限公司。
试验例1
在温度为25℃，相对湿度50％的环境下，分布将实施例1-5制备的组合物均匀涂抹在4×4cm方形无纺棉上，然后敷在脸上，分别测试在贴敷30min、1h、2h、3h敷贴区的皮肤水分含量，水分含量测试采用水分含量测试仪(Corneometer CM825)，研究不同时间皮肤水分含量的增长率，皮肤水分含量的增长率＝(测试值-空白值)/空白值×100％，结果参见表1。
表1
Figure PCTCN2020101349-appb-000001
从上表可以看出实施例2-5的水分增长率与实施例1相同时刻的水分增长率均高，这是由于实施例2-5中加入了阿尔泰柴胡根提取物、苹果果实细胞培养物提取物、依兰花提取物、春榆根提取物、假叶树根提取物、紫松果菊提取物、牡丹根皮提取物，各种原料的协同作用可以提高皮肤水分的含量。从对比例1-3与实施例2-5的数据中可以看出，对比例1-3的皮肤水分增长率明显低于实施例2-5，这是由于采用本发明的方法制备的植物提取物具有较好的补水保湿的作用。
以上所述，仅为本发明的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，可轻易想到 变化或替换，都应涵盖在本发明的保护范围之内。因此，本发明的保护范围应以所述权利要求的保护范围为准。

Claims (10)

  1. 一种保湿补水面膜组合物，包含水、辅料和植物提取物，其特征在于，所述的植物提取物包括突厥蔷薇花水、马齿苋提取物、铁皮石斛提取物、白松露菌提取物、雪莲花提取物、银耳子实体提取物、积雪草提取物、大豆籽提取物、茶叶提取物和粉防己提取物。
  2. 根据权利要求1所述的保湿补水面膜组合物，其特征在于，所述的植物提取物还包括阿尔泰柴胡根提取物、苹果果实细胞培养物提取物、依兰花提取物、春榆根提取物、假叶树根提取物、紫松果菊提取物、牡丹根皮提取物。
  3. 根据权利要求1所述的保湿补水面膜组合物，其特征在于，所述的辅料包括丁二醇、海藻糖、1,2-己二醇、对羟基苯乙酮、甘油、角鲨烷、辛酸/癸酸甘油三酯、异壬酸异壬酯、氢化卵磷脂、PEG-10大豆甾醇、EDTA二钠、生育酚乙酸酯、苯氧乙醇、黄原胶、乙基己基甘油、羟基化卵磷脂、尿囊素、β-葡聚糖、木糖醇基葡糖苷、脱水木糖醇、木糖醇、葡萄糖、泛醇、羟乙基纤维素、甘草酸二钾、透明质酸钠、聚谷氨酸钠、丙二醇、牛磺酸、氨基丁酸、苏氨酸、组氨酸、天冬酰胺、瓜氨酸、柠檬酸和滨海剌芹愈伤组织培养物滤液。
  4. 根据权利要求1所述的保湿补水面膜组合物，其特征在于，所述的辅料还包括鳄梨油、水解胶原、葡萄糖酸钙、蜂蜜、鲸蜡硬脂基葡糖苷、芝麻籽油和滇山茶籽油。
  5. 根据权利要求4所述的保湿补水面膜组合物，其特征在于，按照重量份，所述的组合物包括如下成分：突厥蔷薇花水30-80份、马齿苋提取物0.03-0.07份、铁皮石斛提取物1.2-1.6份、白松露菌提取物1.1-1.5份、雪莲花提取物1.2-1.6份、银耳子实体提取物1.3-1.9份、积雪草提取物1.1-1.5份、大豆籽提取物1.1-1.5份、茶叶提取物1.2-1.6份、粉防己提取物0.08-0.12份、阿尔泰柴胡根提取物1.0-2.0份、苹果果实细胞培养物提取物0.2-0.6份、依兰花提取物1.3-1.9份、春榆根提取物1.2-1.8份、假叶树根提取物0.8-1.2份、紫松果菊提取物1.0-1.5份、牡丹根皮提取物0.8-0.12份、丁二醇0.4-1.0份、水10-20份、海藻糖0.2-0.6 份、1,2-己二醇0.01-0.06份、对羟基苯乙酮0.02-0.08份、甘油0.1-0.8份、角鲨烷0.03-0.06份、辛酸/癸酸甘油三酯0.01-0.06份、异壬酸异壬酯0.02-0.04份、氢化卵磷脂0.03-0.07份、PEG-10 0.02-0.06份、大豆甾醇0.02-0.06份、EDTA二钠0.04-0.08份、生育酚乙酸酯0.03-0.05份、苯氧乙醇0.05-0.07份、黄原胶1.0-1.4份、乙基己基甘油0.02-0.06份、羟基化卵磷脂0.002-0.008份、尿囊素0.003-0.005份、β-葡聚糖0.03-0.07份、木糖醇基葡糖苷0.02-0.06份、脱水木糖醇0.003-0.005份、木糖醇0.2-0.6份、葡萄糖1.2-1.6份、泛醇0.4-0.6份、羟乙基纤维素0.04-0.08份、甘草酸二钾0.03-0.05份、透明质酸钠0.06-0.10份、聚谷氨酸钠0.03-0.07份、丙二醇0.1-0.3份、牛磺酸0.03-0.05份、氨基丁酸0.04-0.06份、苏氨酸0.02-0.06份、组氨酸0.01-0.05份、天冬酰胺0.02-0.06份、瓜氨酸0.02-0.06份、柠檬酸0.01-0.05份、滨海剌芹愈伤组织培养物滤液0.04-0.08份、鳄梨油1.2-1.8份、水解胶原0.1-0.5份、葡萄糖酸钙0.04-0.08份、蜂蜜1.2-1.8份、鲸蜡硬脂基葡糖苷0.3-0.5份、芝麻籽油0.2-0.4份和滇山茶籽油0.04-0.08份。
  6. 根据权利要求5所述的保湿补水面膜组合物，其特征在于，按照重量份，所述的组合物包括如下成分：突厥蔷薇花水60-70份、马齿苋提取物0.04-0.06份、铁皮石斛提取物1.3-1.5份、白松露菌提取物1.2-1.4份、雪莲花提取物1.3-1.5份、银耳子实体提取物1.5-1.7份、积雪草提取物1.2-1.4份、大豆籽提取物1.2-1.4份、茶叶提取物1.3-1.5份、粉防己提取物0.09-0.11份、阿尔泰柴胡根提取物1.4-1.6份、苹果果实细胞培养物提取物0.3-0.5份、依兰花提取物1.5-1.7份、春榆根提取物1.4-1.6份、假叶树根提取物0.9-1.1份、紫松果菊提取物1.2-1.3份、牡丹根皮提取物0.9-0.11份、丁二醇0.6-0.8份、水14-16份、海藻糖0.3-0.5份、1,2-己二醇0.03-0.04份、对羟基苯乙酮0.04-0.06份、甘油0.4-0.5份、角鲨烷0.04-0.05份、辛酸/癸酸甘油三酯0.03-0.04份、异壬酸异壬酯0.025-0.035份、氢化卵磷脂0.04-0.05份、PEG-10 0.03-0.05份、大豆甾醇0.03-0.05份、EDTA二钠0.05-0.07份、生育酚乙酸酯0.035-0.045份、苯氧乙醇0.055-0.065份、黄原胶1.1-1.3份、乙基己基甘油0.03-0.05份、羟基化卵磷脂0.004-0.006份、尿囊素0.0035-0.0045份、β-葡聚糖0.04-0.06份、木糖醇基葡糖苷0.03-0.05份、 脱水木糖醇0.0035-0.0045份、木糖醇0.3-0.5份、葡萄糖1.3-1.5份、泛醇0.45-0.55份、羟乙基纤维素0.05-0.07份、甘草酸二钾0.035-0.045份、透明质酸钠0.07-0.09份、聚谷氨酸钠0.04-0.06份、丙二醇0.15-0.25份、牛磺酸0.035-0.045份、氨基丁酸0.045-0.055份、苏氨酸0.03-0.05份、组氨酸0.02-0.04份、天冬酰胺0.03-0.05份、瓜氨酸0.03-0.05份、柠檬酸0.02-0.04份、滨海剌芹愈伤组织培养物滤液0.05-0.07份、鳄梨油1.4-1.6份、水解胶原0.2-0.4份、葡萄糖酸钙0.05-0.07份、蜂蜜1.4-1.6份、鲸蜡硬脂基葡糖苷0.35-0.45份、芝麻籽油0.25-0.35份和滇山茶籽油0.05-0.07份。
  7. 根据权利要求5或6所述的保湿补水面膜组合物，其特征在于，所述的春榆根提取物、假叶树根提取物和牡丹根皮提取物均采用如下方法提取：
    (1)分别将春榆根、假叶树根和牡丹根皮粉碎，过30-50目筛，加入其重量10-14倍的水浸泡8-12h，用水蒸汽蒸馏，收集馏出液，剩余物进行过滤，收集滤饼；
    (2)将所述的滤饼加入其重量6-8倍的体积浓度为95％的乙醇进行超声提取，将提取液与蒸馏液合并，得到所述的提取物。
  8. 一种权利要求1-7任一所述的保湿补水面膜组合物的制备方法，其特征在于，包括如下步骤：
    (a)按照各原料的重量分别称取备用；
    (b)将水和辅料混合，加热至完全溶解，得到混合溶液A；
    (c)将植物提取物加入到混合溶液A中，进行搅拌均匀，得到所述的保湿补水面膜组合物。
  9. 根据权利要求8所述的保湿补水面膜组合物的制备方法，其特征在于，步骤(b)中加热至35-45℃。
  10. 一种面膜，其特征在于，包括权利要求1-7任意一项所述的保湿补水面膜组合物。
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