WO2018113069A1 - 一种图案化碳纳米管阴极的透射式x射线源结构 - Google Patents
一种图案化碳纳米管阴极的透射式x射线源结构 Download PDFInfo
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- WO2018113069A1 WO2018113069A1 PCT/CN2017/071980 CN2017071980W WO2018113069A1 WO 2018113069 A1 WO2018113069 A1 WO 2018113069A1 CN 2017071980 W CN2017071980 W CN 2017071980W WO 2018113069 A1 WO2018113069 A1 WO 2018113069A1
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- carbon nanotube
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- ray source
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J35/00—X-ray tubes
- H01J35/02—Details
- H01J35/04—Electrodes ; Mutual position thereof; Constructional adaptations therefor
- H01J35/06—Cathodes
- H01J35/065—Field emission, photo emission or secondary emission cathodes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J35/00—X-ray tubes
- H01J35/02—Details
- H01J35/04—Electrodes ; Mutual position thereof; Constructional adaptations therefor
- H01J35/08—Anodes; Anti cathodes
Definitions
- the present invention relates to an X-ray source structure, and more particularly to a transmissive X-ray source structure for a patterned carbon nanotube cathode.
- the electron emission of the conventional X-ray source has certain drawbacks.
- a specific voltage to the tungsten wire By applying a specific voltage to the tungsten wire, the electron is excited and overflowed, and the working temperature is high and the energy loss is large, which is disadvantageous for miniaturization of the X-ray source.
- a large metal anode is used as a bombardment target, and at the same time, it is used as a cooling, so the weight is greatly increased, and the hot application of the current miniaturized X-ray in vivo treatment cannot be satisfied.
- the X-ray illumination angle is adjusted by the tilt angle of the metal anode, which cannot meet the application of forward illumination.
- the high voltage that provides an accelerating electric field for the electrons in the metal anode introduces a great safety hazard to the radiation therapy process in the body, and its application value is greatly reduced.
- the technical problem to be solved by the present invention is to provide a transmissive X-ray source structure with a low power, small size, and a patterned carbon nanotube cathode capable of meeting forward illumination and in vivo medical use.
- the present invention provides a transmissive X-ray source structure of a patterned carbon nanotube cathode, which comprises carbon nanotubes, a conductive base, an insulating cover, a sash window, a conductive ring and a bulb, the ball a top end of the tube is open, the bottom end is closed, and the sash is sealed to the ball by the conductive ring seal
- the open end of the tube forms a vacuum chamber
- the carbon nanotube, the conductive base and the insulating cover are disposed in the vacuum chamber, and the top end of the conductive base is provided with a groove, and the carbon nanotube passes through the
- An insulating cover is fixed in the recess, the conductive base is connected with a first electrode, and a side of the sidewall facing the carbon nanotube is provided with a metal film, and the metal film is connected to the conductive ring.
- the conductive ring is connected to the second electrode.
- the carbon nanotubes are micro-columns fabricated by micro-nano processing technology, and then a carbon tube is grown on the surface by a CVD process to accurately control the growth height of the carbon tubes, and Catalyst deposition on the surface of the microcolumn leads to the growth of 3D patterned carbon nanotubes.
- the size of the groove matches the size of the carbon nanotube.
- the insulating cover is provided with a through hole opposite to the carbon nanotube.
- the insulating cover is connected to the top end of the conductive base through a threaded structure; when the insulating cover is connected to the conductive base, an edge of the through hole presses the carbon nanotube.
- the first electrode is an electrode rod, one end of the first electrode is fixedly connected to the bottom end of the conductive base, and the closed end of the bulb is provided with a first electrode hole.
- the other end of the first electrode passes through the first electrode hole and extends to an external connection power source of the X-ray source structure, the first electrode is sealed and fixed to the first electrode hole, and the power source applies to the conductive base Negative potential.
- the second electrode is an electrode rod, and one of the second electrodes
- the end of the tube is fixedly connected to the conductive ring, the closed end of the tube is provided with a second electrode hole, and the other end of the second electrode passes through the second electrode hole and extends to the external power supply of the X-ray source structure.
- the second electrode is sealed and fixed to the second electrode hole, and the power source applies a zero potential to the conductive ring.
- the bottom end of the conductive base is a hollow structure.
- a cooling container is further included, the top end of the cooling container is open, and the bottom end is closed, and the window is sealed by the conductive ring to cover the open end of the cooling container, and The outer circumference of the bulb is combined to form a cooling cavity.
- the cooling container is provided with an oil inlet hole and an oil outlet hole communicating with the cooling cavity.
- the carbon nanotubes are integrated as a field emission electron source of X-rays onto the conductive base, and the electrons on the end faces of the carbon nanotubes are excited by applying a voltage to the conductive base, and the metal film is applied on the surface of the window by applying a voltage to the conductive rings. Zero potential, thereby pulling out electrons from the end faces of the carbon nanotubes, and bombarding X-rays on the surface of the metal film of the window.
- This design is due to the large aspect ratio and extremely small radius of curvature of carbon nanotubes, which can emit large currents at relatively low electric field strength, and has low threshold voltage, high emission current density, and high stability.
- FIG. 1 is an exploded view of a transmission X-ray source structure of a patterned carbon nanotube cathode of the present invention
- FIG. 3 is an effect diagram of a 3D patterned carbon nanotube growth process.
- a transmissive X-ray source structure of a patterned carbon nanotube cathode comprising a carbon nanotube 1, a conductive base 2, an insulating cover 3, a sash 4, and a conductive ring 5 and the tube 6, the top end of the tube 6 is open, the bottom end is closed, and the window 4 is sealed and closed at the open end of the tube 6 through the conductive ring 5, and a vacuum chamber is formed.
- the carbon nanotubes 1, the conductive base 2 and the insulating cover 3 are disposed in the vacuum chamber, and the top end of the conductive base 2 is provided with a groove 21, and the carbon nanotubes 1 are fixed by the insulating cover 3
- the conductive base 2 is connected with a first electrode 7, and a side of the window 4 is provided with a metal film (not shown) on one side of the carbon nanotube 1.
- the conductive ring 5 is connected, and the conductive ring 5 is connected to the second electrode 8.
- the conductive base 2 is preferably made of a metal conductive material, and has an embedded recess on the surface thereof to match the size of the carbon nanotubes 1 to realize the limiting action of the carbon nanotubes 1 and facilitate the carbon nanotubes 1 Applying a voltage;
- the insulating cover 3 is preferably made of a ceramic material for fixing the carbon nanotubes 1;
- the bulb 9 is preferably a glass bulb 9 for vacuum encapsulating the core of the carbon nanotube 1, the conductive base 2, and the insulating cover 3.
- the structure provides a good migration environment for the electrons;
- the conductive ring 5 is preferably made of a metal conductive material for fixing the blind window 4 and closing the bulb 6 while facilitating heat dissipation.
- the transmissive X-ray source structure of the patterned carbon nanotube cathode of the present invention works by integrating the carbon nanotube 1 as a field emission electron source of X-rays onto the conductive base 2, by applying a voltage to the conductive base 2, The electrons on the end face of the carbon nanotube 1 are excited, and a voltage is applied to the conductive ring 5 to apply a zero potential to the metal film on the surface of the window 4, thereby pulling out the electrons on the end face of the carbon nanotube 1 and bombarding the metal film on the window 4. X-rays are generated on the surface.
- Such a design is due to the fact that the carbon nanotubes 1 have a large aspect ratio and a small radius of curvature, can emit a large current at a relatively low electric field intensity, and have a low threshold voltage, a large emission current density, and stability.
- the excellent field emission performance of the X-ray source can solve the problem that the conventional X-ray source uses the hot cathode as the electron source, resulting in high operating temperature, high power consumption, and unfavorable miniaturization of the radiation source.
- the X-ray source based on the carbon nanotube 1 is in operation, when the surface electric field of the carbon nanotube 1 reaches a certain threshold, free electrons can be generated from the carbon nanotube 1, and it can be said that the generation of electrons is instantaneous.
- the carbon nanotube 1X light source made by using this characteristic can control the generation of electrons by controlling the surface electric field of the carbon nanotube 1, thereby controlling the generation of X-rays.
- the metal film on the surface of the window 4 as an anode target, the electrons are pulled out from the end face of the carbon nanotube 1 so that the electrons bombard the metal film to generate X-rays and are radiated forward in a transmissive manner, thereby avoiding the conventional adoption.
- the design of a large piece of metal as an anode target greatly reduces the weight of the product and meets the needs of forward illumination and in vivo medical treatment.
- the carbon nanotubes 1 are micro-columns of a certain height (for example, 20 um) by using micro-nano processing technology, and then are grown on the surface by chemical vapor deposition (CVD).
- the high carbon tube grows the 3D patterned carbon nanotubes 1 by precisely controlling the carbon tube growth height and the catalyst deposition on the end faces and sidewalls of the microcolumns.
- the carbon tube is subjected to CVD growth on the surface of the heavily doped silicon wafer with a certain depth of micro-column, and the 3D patterned carbon tube is produced in one step, as shown in FIG. 2 .
- Figure 3 shows.
- the carbon tube and the side wall of the micro-column end surface are completely protruded, and the carbon tube extending to the periphery is formed into a 3D carbon tube structure, and the current generated between the carbon tube bundles is not affected.
- the size of the groove 21 matches the size of the carbon nanotubes 1, thereby realizing the limitation of the carbon nanotubes 1 and facilitating assembly.
- the insulating cover 3 is provided with a through hole 31 opposite to the carbon nanotube 1, and the through hole 31 serves as a window for emitting electrons from the carbon nanotube 1.
- the insulating cover 3 and the top end of the conductive base 2 are connected by a screw structure, and when the insulating cover 3 is connected to the conductive base 2, The edge of the through hole 31 presses the carbon nanotube 1 to achieve a compact packaging effect of the carbon nanotube 1.
- the first electrode 7 is an electrode rod, one end of the first electrode 7 is fixedly connected to the bottom end of the conductive base 2, and the closed end of the bulb 6 is provided with a first electrode. a hole, the other end of the first electrode 7 passes through the first electrode hole and extends to an external connection power source of the X-ray source structure, the first electrode 7 is sealed and fixed to the first electrode hole, and the power source pair
- the conductive base 2 applies a negative potential.
- the conductive base 2 is electrically connected to the carbon nanotubes 1 .
- the second electrode 8 is an electrode rod, one end of the second electrode 8 is fixedly connected to the conductive ring 5, and the closed end of the bulb 6 is provided with a second electrode hole.
- the other end of the second electrode 8 passes through the second electrode hole and extends to the external connection power source of the X-ray source structure, the second electrode 8 is sealed and fixed to the second electrode hole, and the power source is opposite to the conductive Ring 5 applies a zero potential.
- the conductive ring 5 is electrically connected to the metal film. Therefore, the voltage requirement of the metal thin film is provided by the design of the second electrode 8, and the metal thin film is used as the anode to achieve zero potential, which is less harmful to the human body and can ensure the safety in the radiation therapy process in the body.
- the bottom end of the conductive base 2 is a hollow structure, thereby greatly reducing the overall weight of the product.
- a cooling container 9 is further included, the top end of the cooling container 9 is open, the bottom end is closed, and the window 4 is sealed and closed at the open end of the cooling container 9 through the conductive ring 5 And forming a cooling cavity around the outer periphery of the bulb 6.
- the cooling container 9 is provided with an oil inlet hole 91 and an oil outlet hole 92 communicating with the cooling cavity. Thereby, the replacement of the cooling oil can be realized, and the heat of the metal film of the conductive ring 5 and the window 4 can be taken away, thereby ensuring normal operation at high power operation.
- the transmissive X-ray source structure of the patterned carbon nanotube cathode provided by the invention has the advantages of compact structure, simple assembly, small size, convenient use, low power, low cost, etc., and can be deeply penetrated into the body as a tumor radiotherapy treatment.
- the X-ray source used for the purpose can also be used as a function to eliminate static electricity such as an X-ray tube.
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Abstract
Description
Claims (10)
- 一种图案化碳纳米管阴极的透射式X射线源结构,其特征在于,包括碳纳米管、导电底座、绝缘罩、铍窗、导电环和球管,所述球管的顶端开口,底端封闭,所述铍窗通过所述导电环密封盖合在所述球管的开口端,并形成一真空腔体,所述碳纳米管、导电底座和绝缘罩均设置在所述真空腔体内,所述导电底座的顶端设有凹槽,所述碳纳米管通过所述绝缘罩固定在所述凹槽内,所述导电底座连接有第一电极,所述铍窗朝向所述碳纳米管的一面设有金属薄膜,所述金属薄膜与所述导电环连接,所述导电环连接有第二电极。
- 如权利要求1所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述碳纳米管是利用微纳加工技术制作出一定高度的微柱,然后利用CVD工艺在其表面生长一定高度的碳管,通过精确控制碳管生长高度,以及微柱表面的催化剂沉积,进而长出3D图案化的碳纳米管。
- 如权利要求1所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述凹槽的尺寸与所述碳纳米管的尺寸匹配。
- 如权利要求1所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述绝缘罩设有与所述碳纳米管相对的通孔。
- 如权利要求4所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述绝缘罩与所述导电底座的顶端通过螺纹结构连接;所述绝缘罩与所述导电底座连接时,所述通孔的边缘压紧所述碳纳米管。
- 如权利要求1所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述第一电极为电极杆,所述第一电极的一端固定连接于所述导电 底座的底端,所述球管的封闭端设有第一电极孔,所述第一电极的另一端穿过所述第一电极孔并伸至X射线源结构外部连接电源,所述第一电极与所述第一电极孔密封固定,所述电源对所述导电底座施加负电位。
- 如权利要求1所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述第二电极为电极杆,所述第二电极的一端固定连接于所述导电环,所述球管的封闭端设有第二电极孔,所述第二电极的另一端穿过所述第二电极孔并伸至X射线源结构外部连接电源,所述第二电极与所述第二电极孔密封固定,所述电源对所述导电环施加零电位。
- 如权利要求1所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述导电底座的底端为掏空结构。
- 如权利要求1至8任一项所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,还包括有冷却容器,所述冷却容器的顶端开口,底端封闭,所述铍窗通过所述导电环密封盖合在所述冷却容器的开口端,并在所述球管外周围合形成一冷却腔体。
- 如权利要求9所述的图案化碳纳米管阴极的透射式X射线源结构,其特征在于,所述冷却容器设有与所述冷却腔体连通的进油孔和出油孔。
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