WO2018048062A1 - 밀착성 및 발림성이 동시에 향상된 색조 화장료 조성물 - Google Patents

밀착성 및 발림성이 동시에 향상된 색조 화장료 조성물 Download PDF

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Publication number
WO2018048062A1
WO2018048062A1 PCT/KR2017/005539 KR2017005539W WO2018048062A1 WO 2018048062 A1 WO2018048062 A1 WO 2018048062A1 KR 2017005539 W KR2017005539 W KR 2017005539W WO 2018048062 A1 WO2018048062 A1 WO 2018048062A1
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Prior art keywords
cosmetic composition
powder
weight
color cosmetic
sericite
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PCT/KR2017/005539
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English (en)
French (fr)
Korean (ko)
Inventor
송상훈
홍경우
김경섭
Original Assignee
주식회사 엘지생활건강
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Priority to CN201780049509.7A priority Critical patent/CN109562052B/zh
Publication of WO2018048062A1 publication Critical patent/WO2018048062A1/ko

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216—Solid or semisolid forms
    • A61K8/022—Powders; Compacted Powders
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42—Colour properties
    • A61K2800/43—Pigments; Dyes

Definitions

  • the present invention relates to a color cosmetic composition, and more particularly, to a color cosmetic composition excellent in adhesion and a method for producing the same, while applying smoothness and smoothness to a smooth skin makeup expression.
  • the general powder color cosmetic composition should satisfy the main functional requirements such as coverage, spreadability, adhesion, fine grain, cosmetic lifting or particle aggregation.
  • conventional color cosmetics have a disadvantage in that the adhesion decreases when the applicability is improved. That is, when the color cosmetics are applied to the face using a makeup tool such as a puff and a brush, when the applicability is very excellent, the adhesiveness, which is a relative property thereof, is inferior.
  • an ester-based oil having excellent skin affinity is applied, or magnesium myristate, magnesium stearate, zinc myristate, or zinc stearate Metal salt powders such as
  • the adhesion is improved, but there is a disadvantage that the applicability is lowered when the ester-based oil or metal salt powder is added in an excessive amount.
  • powdered color cosmetics for example, compact, powder foundation, powder pact, or compressed powder products such as two-way cake, grazing due to powder coagulation or fine dispersion such as oil when taking the contents with puff (greasing phenomenon, caking phenomenon, etc.) can occur, the amount of the ester-based oil or metal salt powder is very limited.
  • the technical problem to be achieved by the present invention is to provide a color cosmetic composition with improved application and adhesion at the same time, smooth skin expression and less makeup lifting phenomenon.
  • the present invention provides a color cosmetic composition
  • a color cosmetic composition comprising spherical powder, silicone powder and sericite.
  • the color cosmetic composition may be a powdery color cosmetic composition.
  • the inventors of the present invention have tried to improve the applicability and adhesion at the same time in the trade-off relationship with the relative properties in powdery color cosmetics.
  • the inventors of the present invention use a combination of sharp spherical powder and silicon powder which are excellent in dispersibility and not widely distributed in particle size distribution, and select and use a chorionic material having an optimal particle size for adhesion. It was.
  • the color cosmetic composition prepared as described above has excellent application properties and adhesion, while solving problems such as powdering phenomenon and molding stability when applying spherical powder, and at the same time, it has a surprising discovery that the skin adhesion and smooth cosmetic effect are excellent.
  • the present invention was completed.
  • the spherical powder may include polymethyl methacrylate (PMMA).
  • PMMA polymethyl methacrylate
  • the polymethylmethacrylate has an oil absorption force of about 0.5 to 1.5 cc / g, and non-porous, spherical powder may be used without surface treatment.
  • the polymethylmethacrylate may be uniform and sharp without having a wide distribution of fine particles.
  • the polymethacrylate may be a mono-dispersed consisting of a dispersion system having a dispersed phase of uniform size.
  • the polymethylmethacrylate may be used as spherical particles from which residual monomers have been removed.
  • the polymethacrylate may be, for example, ArtPearl K7P manufactured by NEGAMI Chemical Industrial, or GM-0800S manufactured by AICA Kogyo, but is not limited thereto.
  • the average particle diameter of the spherical powder may be 5 to 25 ⁇ m, preferably 6 to 20 ⁇ m, more preferably 8 to 12 ⁇ m.
  • the cosmetic composition of the present invention comprises a spherical powder having an average particle diameter as described above, it can be exhibited the most excellent application.
  • the spherical powder may be included in 0.5 to 5% by weight, preferably 1.5 to 4% by weight, more preferably 2 to 3% by weight relative to the total weight of the cosmetic composition.
  • a makeup tool such as a puff and a brush
  • there is a powder blowing phenomenon, and molding stability is also reduced.
  • the content of the spherical powder is less than 0.5% by weight, the soft spreadability is not sufficiently exhibited when applied to the skin.
  • the silicone powder may be a spherical silicone powder having elasticity, specifically, polymethylsilsesquioxane, silsesquioxane polymer, vinyl dimethicone / methicone silsesquioxane crosspolymer, dimethicone It may include any one or more selected from the group consisting of / vinyl dimethicone crosspolymer and diphenyl dimethicone / vinyl diphenyl dimethicone / silsesquioxane crosspolymer, but is not limited thereto.
  • the silicon powder may include diphenyldimethicone / vinyldiphenyldimethicone / silsesquioxane crosspolymer.
  • the cosmetic composition of the present invention is soft when the texture includes diphenyl dimethicone / vinyl diphenyl dimethicone / silsesquioxane cross-polymer and creamy feeling can be exhibited the most excellent application.
  • the silicone powder may be included in 1 to 20% by weight, preferably 3 to 17% by weight, more preferably 5 to 15% by weight relative to the total weight of the cosmetic composition.
  • the silicone powder is less than 1% by weight, the spreadability of the cosmetic composition is lowered.
  • the silicone powder is more than 20% by weight, powder blowing may occur and molding stability may be inhibited.
  • sericite exhibits a fine and soft feeling when used in cosmetic compositions, and the mica that has an average particle diameter of about 5 to 15 ⁇ m, preferably 6 to 14 ⁇ m and more preferably 8 to 12 ⁇ m is used. Can be.
  • the sericite may be wet coated.
  • the sericite may be wet coated with lauroyl lysine, sodium cocoyl glutamate, or a mixture thereof.
  • the lauroyl lysine has excellent skin affinity, and sodium cocoyl glutamate is a mild ingredient derived from coconut and can be used for sensitive skin.
  • the sericite may be wet coated with 0.5 to 2% by weight of laurolysine and 1 to 6% by weight of sodium cocoylglutamate relative to the total weight of the cosmetic composition.
  • the cosmetic composition of the present invention comprises sericite wet-coated with lauroyl lysine and sodium cocoylglutamate in the above weight ratio, the skin adhesion of the cosmetic composition can be best exhibited.
  • the solvent used when wet coating the sericite may be used any one or more selected from the group consisting of purified water, ethanol and isopropyl alcohol (isopropyl alchohol), but is not limited thereto.
  • the type and content of the coating material used for the wet coating of sericite are factors that affect physical properties such as the feeling of use of the cosmetic, application properties and stability, and the sericite used in the present invention may be modified using various coating materials.
  • the sericite may be included in 5 to 20% by weight, preferably 5 to 15% by weight, more preferably 10 to 15% by weight relative to the total weight of the cosmetic composition.
  • the sericite content is more than 20% by weight, the skin is not smooth when the product is applied to the skin, and the cosmetics are thickly expressed or unnaturally applied to pores or wrinkles, so that pores and wrinkles are highlighted. Occurs.
  • the sericite content is less than 5% by weight, the spreadability and soft feel of the cosmetic composition are deteriorated.
  • the color cosmetic composition of the present invention has a weight ratio of the spherical powder and the silicone powder in the range of 1: 0.2 to 1:10, preferably 1: 0.5 to 1: 9, more preferably 1: 1 to 1: 8, and most preferably Such as 1: 2 to 1: 7 (spherical powder: silicone powder).
  • spherical powder silicone powder
  • the applicability of the cosmetic composition may be best exhibited.
  • the color cosmetic composition of the present invention is a weight ratio of the spherical powder and silicone powder and sericite 1: 0.5 to 1: 2, preferably 1: 0.7 to 1: 1.8, more preferably 1: 0.9 to 1: 1.6 ( Spherical powder and silicon powder: sericite).
  • the cosmetic composition may simultaneously satisfy excellent applicability and adhesion.
  • the powder may mean an aggregate of solid materials having a particle size of usually 1 mm or less.
  • Powders that can be used in the composition of the present invention may include any one or more selected from the group consisting of extender pigments, colored pigments and white pigments commonly used in the cosmetic field.
  • the cosmetic composition of the present invention may comprise the extender pigment.
  • the extender pigments include inorganic pigments including talc, mica, kaolin, alumina, barium silicate, mica, synthetic mica, magnesium carbonate, zeolite, and the like, and polyethylene powder, nylon powder, polystyrene powder, and polymethacrylate powder. Any one or more selected from the group consisting of organic pigments and the like may be used.
  • extender pigments commonly known in the art, for example, extender pigments described in [Modern Cosmetic Science, Cho Wan-gu, Rang Moon-jung, co-authored by Bae Duk-hwan, Korea Research Information, 2007.02 published] and the like It can be used as a extender pigment in the composition.
  • the extender pigment may be included in 30 to 50% by weight, preferably 32 to 48% by weight, more preferably 35 to 45% by weight relative to the total weight of the cosmetic composition. When the extender pigment is less than 30% by weight may lower the applicability, when more than 50% by weight powder agglomeration may occur.
  • the extender pigment may be one that has been hydrophobized.
  • the extender pigment may be used by modifying the surface with any one or more selected from the group consisting of silicones, hydrocarbons, fluorine, alkyl hydrogen polysiloxanes, surfactants, and natural and synthetic waxes.
  • the white pigment is silicones, ester oils, aluminum hydroxide and stearic acid Titanium dioxide or zinc oxide coated with one or more selected from the group consisting of the above may be used, but is not limited thereto.
  • the cosmetic composition according to the present invention may include an oil, preferably an oil binder, so that the powder is combined and molded.
  • the oil is not limited in kind, and oils commonly used in cosmetic compositions may be used.
  • the oil may be a hydrocarbon-based oil including a mineral oil and the like; Diisostearyl malate, hydrogenated polyisobutene, phytosteryl / isostearyl / cetyl / stearyl / behenyldimerdilinoleate (phytosteryl / isostearyl / cetyl / stearyl / behenyl dimer dilinoleate, methyl hydrogenated rosinate, caprylic / capric triglyceride, isopropyl myristate, neopentylglycol dicaprate ester crab oil, including glycol dicaprate) and octyldodecyl stearoyl stearate; Vegetable oils including olive oil
  • the oil may be included in an amount of 0.1 to 15% by weight, preferably 1 to 12% by weight, and more preferably 2 to 10% by weight, based on the total weight of the cosmetic composition.
  • the oil is less than 0.1% by weight, the binding of the powder may not occur sufficiently, and when the amount is more than 15% by weight, powder agglomeration by oil may occur.
  • the color cosmetic composition of the present invention may further include any one or more selected from the group consisting of fragrances, colorants, preservatives, oxidative stabilizers, sunscreens and pearlescent agents within a range that does not reduce the effect of the composition.
  • the cosmetic composition may be a solid stick or cake formulation, and specifically, may be a powder formulation of any one selected from the group consisting of a pressed powder, a pressed pact, a powder pact, a powder foundation, a foundation pact, and a pressed powder foundation. It is not limited to this.
  • the present invention is 0.5 to 5% by weight of polymethyl methacrylate (PMMA) relative to the total weight of the cosmetic composition, diphenyldimethicone / vinyldiphenyldimethicone / silsesquioxane crosspolymer 1 to 20% by weight, lauro
  • PMMA polymethyl methacrylate
  • diphenyldimethicone / vinyldiphenyldimethicone / silsesquioxane crosspolymer 1 to 20% by weight
  • lauro There is provided a color cosmetic composition containing 5 to 20% by weight of sericite, 30 to 50% by weight sieving pigment and 0.1 to 15% by weight of oil coated with lysine and sodium cocoylglutamate.
  • the color cosmetic composition including a combination of components having a specific weight ratio as described above is soft and smooth, and has excellent applicability while being able to express smooth skin makeup.
  • the present invention comprises the steps of stirring the powder portion comprising (s1) spherical powder, silicon powder and sericite; (s2) spraying an oil part on the powder part; And (s3) mixing, pulverizing and filtering the product of step (s2).
  • the color cosmetic composition of the present invention is excellent in application property and dropping stability while being excellent in application property and adhesion to the skin at the same time.
  • the color cosmetic composition of the present invention has no makeup agglomeration phenomenon due to the aggregation of particles, and the skin makeup is smoothly expressed, so that the curved portion is not seen or raised, and the skin expression power is excellent.
  • Figure 1 shows the average particle diameter and particle size distribution of Example 1 and Comparative Example 1.
  • the inventors of the present invention produced powder color tone cosmetics using the components shown in Table 1 below.
  • Table 1 below.
  • Examples 1 and 2 by varying the content of lauroyl lysine and sodium cocoyl glutamate, the usability, application and stability of the cosmetic composition was analyzed.
  • the above examples and comparative examples were prepared according to the content composition of each of the above components.
  • the powder part was put in a Henschel mixer, mixed at high speed (800-1200 rpm) for about 5 minutes, and then spray-sprayed while stirring the oil part at low speed (400-600 rpm).
  • the mixture was mixed at a high speed (800 to 1200 rpm) for about 3 minutes on a Henschel mixer, and then crushed twice using an atomizer, followed by filtration at 30 mesh.
  • the semifinished product through the series of manufacturing processes was molded for 1 to 3 seconds at a pressure of 30-50 kgf / cm 2 .
  • Examples 1 to 2 and Comparative Examples 2 to 3 including polymethylmethacrylate and diphenyldimethicone / vinyldiphenyldimethicone / silsesquioxane crosspolymer are soft and easy to apply. It was found that the feeling of use was very improved.
  • Examples 1 and 2 including sericite coated with laurolysine and sodium cocoyl glutamate showed the best effect in adhesion, makeup aggregation and makeup lifting.
  • a cosmetic composition comprising polymethylmethacrylate and diphenyldimethicone / vinyldiphenyldimethicone / silsesquioxane crosspolymer only and a sericite coated with laurolysine and sodium cocoylglutamate
  • Examples 1 to 2 showed a soft texture on the surface of the product, maintaining the appropriate hardness and appeared as a product pass level even in drop stability, showing good results in terms of physical properties and stability.
  • Comparative Example 1 having a low spherical powder content was relatively high in hardness, but as described in Table 3, the application and adhesion were lower than in the Examples.
  • Comparative Examples 2 and 3 The polymethyl methacrylate, silica and nylon powder content was excessively compounded, resulting in low hardness and very poor dropping stability. The grazing and caking phenomena caused by the agglomeration of particulates and excess oil showed good results in both Examples and Comparative Examples.
  • the cosmetic conditions ie, a uniform makeup film, naturalness and makeup sustainability, which were obtained by applying the cosmetic compositions of Examples 1, Comparative Examples 1 and 3 to the actual skin, were evaluated.
  • the subjects were 25 females aged 20 to 45 years who checked the feeling and condition of applying the product and the persistence after makeup.
  • Example 1 produced according to the present invention showed a very excellent cosmetic effect in a uniform cosmetic film, it was confirmed that it is excellent in the naturalness and satisfaction of makeup persistence.
  • Comparative Example 1 was confirmed to be good in terms of uniform makeup and makeup persistence, but appeared to be moderate in the naturalness evaluation.
  • Comparative Example 3 it was confirmed that the makeup film was not uniform and the makeup persistence was not good because the powder blowing phenomenon was severe.
  • the cosmetic composition of the present invention has a suitable average particle diameter and uniformity of particle size distribution by including polymethylmethacrylate and diphenyldimethicone / vinyldiphenyldimethicone / silsesquioxane crosspolymer An improved and uniform cosmetic film is formed.
  • the cosmetic composition of the present invention includes a sericite wet coated with laurolysine and sodium cocoyl glutamate to significantly improve skin adhesion and persistence.
  • the average particle diameter and particle size distribution map of Example 1 and Comparative Example 1 are shown in FIG.

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PCT/KR2017/005539 2016-09-07 2017-05-26 밀착성 및 발림성이 동시에 향상된 색조 화장료 조성물 WO2018048062A1 (ko)

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CN201780049509.7A CN109562052B (zh) 2016-09-07 2017-05-26 同时提高了贴合性和涂展性的彩妆品组合物

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KR1020160115285A KR101859284B1 (ko) 2016-09-07 2016-09-07 밀착성 및 발림성이 동시에 향상된 색조 화장료 조성물
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