WO2016108286A1 - 磁気ディスク用基板の製造方法、及び研削用砥石 - Google Patents
磁気ディスク用基板の製造方法、及び研削用砥石 Download PDFInfo
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- WO2016108286A1 WO2016108286A1 PCT/JP2015/086583 JP2015086583W WO2016108286A1 WO 2016108286 A1 WO2016108286 A1 WO 2016108286A1 JP 2015086583 W JP2015086583 W JP 2015086583W WO 2016108286 A1 WO2016108286 A1 WO 2016108286A1
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- Prior art keywords
- grinding
- groove
- substrate
- end surface
- grindstone
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B9/00—Machines or devices designed for grinding edges or bevels on work or for removing burrs; Accessories therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D5/00—Bonded abrasive wheels, or wheels with inserted abrasive blocks, designed for acting only by their periphery; Bushings or mountings therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D5/00—Bonded abrasive wheels, or wheels with inserted abrasive blocks, designed for acting only by their periphery; Bushings or mountings therefor
- B24D5/14—Zonally-graded wheels; Composite wheels comprising different abrasives
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- G—PHYSICS
- G11—INFORMATION STORAGE
- G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
- G11B5/00—Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
- G11B5/84—Processes or apparatus specially adapted for manufacturing record carriers
Definitions
- the present invention relates to a method for manufacturing a magnetic disk substrate used for manufacturing a magnetic disk mounted on a magnetic recording apparatus such as a hard disk drive (hereinafter abbreviated as “HDD”), and end grinding of the magnetic disk substrate.
- the present invention relates to a grinding wheel for use in grinding.
- a magnetic disk as one of information recording media mounted on a magnetic recording apparatus such as an HDD.
- a magnetic disk is configured by forming a thin film such as a magnetic layer on a disk-shaped substrate, and an aluminum alloy substrate or a glass substrate is used as the substrate.
- a glass substrate is harder than an aluminum alloy substrate, and has an advantage of excellent impact resistance. The surfaces of these substrates are polished and smoothed with high precision so as to reduce the flying height of the magnetic head as much as possible, thereby realizing high recording density.
- the demand for further increase in recording capacity and price of HDDs has increased, and in order to realize this, it has become necessary to further improve the quality and cost of magnetic disk substrates. ing.
- a magnetic disk substrate is usually manufactured by sequentially performing steps such as shape processing (end surface grinding and chamfering), end surface polishing, main surface grinding, main surface polishing, and chemical strengthening on a disk-shaped substrate.
- shape processing end surface grinding and chamfering
- end surface polishing main surface grinding
- main surface polishing main surface polishing
- chemical strengthening on a disk-shaped substrate.
- the grinding liquid is contacted and rotated on the outer peripheral side end surface and the inner peripheral side end surface of the substrate while bringing the grinding liquid into contact with the end surface portion of the substrate, and then the substrate is processed.
- a predetermined chamfering process was performed on the outer peripheral side end surface and the inner peripheral side end surface (Patent Document 1, etc.).
- the grindstone is generally called a general grindstone, and has a groove shape for forming the end face shape of the substrate.
- the shape of the grindstone groove is transferred to the end face of the substrate.
- the grinding process is performed by being divided into a rough grinding process using a grinding wheel for rough grinding and a precision grinding process using a grinding wheel for precision grinding.
- the outer peripheral side of the substrate is brought into contact with the rough grinding groove and the precision grinding groove formed on the inner peripheral side of the cylindrical grindstone by sequentially contacting the outer peripheral end surface of the substrate.
- chipping such as scratches may occur on the end face of the substrate after precision grinding.
- the first object of the present invention is to provide a method for manufacturing a magnetic disk substrate capable of finishing the end face of the disk-shaped magnetic disk substrate with high quality from the viewpoint of ensuring reliability. It is a second object of the present invention to provide a grinding wheel that can be suitably used for end face grinding of the magnetic disk substrate.
- the present inventor uses a grindstone that is formed in a cylindrical shape and has a plurality of parallel rough grinding and precision grinding grooves on its inner peripheral side.
- a method of grinding the outer peripheral side end surface of the substrate by bringing the outer peripheral side end surface of the disk-shaped substrate into contact with the inner peripheral side of the substrate and relatively moving the substrate and the grindstone (in this specification, for convenience of explanation) This processing method was called “inscribed grinding”, and the grindstone used therefor was sometimes called “inscribed grinding wheel” for convenience.)
- the groove shape of the conventional inscribed grinding wheel includes a rough grinding region 2A including a plurality of grooves 2a, 2a, and a plurality of grooves 2b, 2b,. Including a precision grinding region 2B.
- the coarse grinding region 2A and the fine grinding region 2B have different abrasive grain sizes.
- rough grinding is performed in the coarse grinding region 2A of abrasive grains having a large abrasive grain size (coarse count abrasive grains).
- precision grinding finish grinding
- fine count abrasive grains fine count abrasive grains.
- the groove shape of the grindstone is inside the cylindrical shape in the inscribed grinding process, when grinding waste generated during grinding with the groove 2a for rough grinding is scattered around, precision grinding In some cases, it may reach the processing groove 2b (indicated by an arrow in FIG. 3). Many grinding scraps generated by rough grinding are relatively larger than those generated by precision grinding. Further, such grinding waste may be accumulated in the precision grinding groove 2b and become sludge. These foreign substances are likely to stick to the groove due to the centrifugal force generated by the rotation of the grindstone. As a result, the grinding scraps cause chipping and pit-like defects that occur during precision grinding, leading to deterioration of the end face quality.
- the present invention has the following configuration in order to solve the above problems.
- a magnetic disk substrate having a process of grinding the end surface of the substrate by bringing a grinding stone into contact with the outer peripheral side end surface of the substrate and moving it relatively while contacting the end surface portion of the disk-shaped substrate.
- the grindstone is formed in a cylindrical shape and has a plurality of parallel groove shapes on its inner peripheral side, and the plurality of groove shapes include a groove for rough grinding, and a precision A grinding groove, and has means for suppressing movement of grinding waste generated when grinding with the rough grinding groove to the precision grinding groove.
- An outer peripheral side end surface of the substrate is ground by bringing the outer peripheral side end surface of the substrate into contact with the rough grinding groove and the fine grinding groove in order. Production method.
- the means for suppressing the grinding scraps from moving to the precision grinding groove is a means for providing a wall between the rough grinding groove and the precision grinding groove.
- a magnetic disk substrate having a process of grinding the end surface of the substrate by bringing a grinding stone into contact with the outer peripheral side end surface of the substrate and moving it relatively while contacting the end surface portion of the disk-shaped substrate.
- the grindstone is formed in a cylindrical shape and has a plurality of parallel groove shapes on its inner peripheral side, and the plurality of groove shapes include a groove for rough grinding, and a precision A groove for grinding, and there is a raised portion between the groove for rough grinding and the groove for precision grinding, and the groove for rough grinding and the groove for precision grinding are sequentially formed.
- a method of manufacturing a magnetic disk substrate comprising: grinding an outer peripheral side end surface of the substrate by bringing the outer peripheral side end surface of the substrate into contact with each other.
- a magnetic disk substrate having a process of grinding the end surface of the substrate by bringing a grinding stone into contact with the outer peripheral side end surface of the substrate and moving it relatively while contacting the end surface portion of the disk-shaped substrate.
- the grindstone is formed in a cylindrical shape and has a plurality of parallel groove shapes on its inner peripheral side, and the plurality of groove shapes include a groove for rough grinding, and a precision A plurality of regions having different diameters provided with steps on the inner peripheral side of the grindstone, and arranging the grooves for rough grinding in the region having a large diameter,
- the precision grinding groove is arranged on the smaller diameter side, and the outer peripheral side end face of the substrate is brought into contact with the rough grinding groove and the fine grinding groove in sequence with the outer peripheral side end face of the substrate.
- the grinding wheel is formed in a cylindrical shape and has a plurality of parallel groove shapes on its inner peripheral side, and the plurality of groove shapes include a groove for rough grinding, A means for suppressing grinding dust generated when grinding is performed in the groove for rough grinding, to move to the groove for precision grinding.
- the grindstone is formed in a cylindrical shape and has a plurality of parallel groove shapes on the inner peripheral side thereof.
- the plurality of groove shapes include a groove for rough grinding and precision grinding.
- a grinding wheel characterized by comprising a groove for machining and having a raised portion between the groove for rough grinding and the groove for precision grinding.
- the grindstone is formed in a cylindrical shape and has a plurality of parallel groove shapes on the inner peripheral side thereof.
- the plurality of groove shapes include a groove for rough grinding and precision grinding.
- a plurality of regions having different diameters provided with steps on the inner peripheral side of the grindstone, the grooves for rough grinding are disposed in the region having a large diameter, and the diameter A grinding wheel for grinding, characterized in that the groove for precision grinding is arranged on the smaller side.
- the occurrence of chipping can be suppressed and the end surface of the magnetic disk substrate can be finished with high quality. Furthermore, stable grinding can be performed.
- the grinding wheel according to the present invention for the end face grinding of the substrate the occurrence of chipping can be suppressed and the end face of the magnetic disk substrate can be finished with high quality.
- the embodiment of the end surface grinding process of the glass substrate in the present invention is shown, and is a sectional view on a plane including a circle formed by a groove shape of a grindstone.
- FIG. 1 is a cross-sectional view of the outer peripheral end of a magnetic disk glass substrate 1 to which the present invention is applied.
- the glass substrate 1 is not shown in FIG. 1, the whole having a circular hole in the center is formed in a disc shape (see FIG. 2), and main surfaces 1a and 1a on the front and back sides thereof, It has an outer peripheral end surface and an inner peripheral end surface formed between the surfaces 1a and 1a.
- the end surface on the outer peripheral side of the glass substrate 1 has a side wall surface 1b orthogonal to the main surface 1a, and two chamfered surfaces formed between the side wall surface 1b and the front and back main surfaces 1a and 1a ( A chamfered surface) 1c and 1c are formed.
- the side wall surface orthogonal to the main surface 1a, and this side wall surface and main surface 1a, 1a of the front and back Are formed in a shape composed of two chamfered surfaces formed respectively.
- the present invention can be preferably applied to a nominal 1.8 inch disk (outer diameter 48 mm) or more.
- the glass substrate 1 is finished to have an outer diameter of 65 mm and an inner diameter of 20 mm.
- the glass substrate 1 is finished to have an outer diameter of 95 mm and an inner diameter of 25 mm.
- the inner diameter is the inner diameter of a circular hole in the center of the glass substrate 1.
- the plate thickness is about 0.6 to 1.5 mm in any size.
- the main surface 1a, the outer peripheral side end surface, and the inner peripheral side end surface of the glass substrate 1 for magnetic disk are finally polished (mirror polished) so as to have a predetermined surface roughness.
- Both the outer peripheral side end face and the inner peripheral side end face of the glass substrate 1 are finished in the end face shape as described above, and the surface roughness is finished in a mirror surface state with Rmax of 1 ⁇ m or less and Ra of 0.1 ⁇ m or less, for example. It is usually sought to be.
- the magnetic disk glass substrate 1 is formed by subjecting a glass plate 1 obtained by processing, for example, a glass plate obtained by a direct press method or a float method into a predetermined disc shape, and grinding and polishing an end face ( (Mirror polishing), grinding of the main surface, mirror polishing, chemical strengthening, etc. are performed in order.
- a glass substrate (glass base plate) obtained by processing a glass plate obtained by a direct press method or a float method into a predetermined disc shape is processed, processed, etc.
- all the steps up to the glass substrate of the final product to be manufactured are referred to as a glass substrate or a magnetic disk glass substrate.
- the grinding / polishing process of the end face of the glass substrate 1 will be described.
- a grinding stone is brought into contact with the outer peripheral side end surface of the substrate while bringing the grinding liquid into contact with the end surface portion of the disk-shaped substrate as in the above-described configuration 1.
- Means for suppressing movement of scraps into the precision grinding groove is provided, and the outer peripheral side end surface of the substrate is sequentially brought into contact with the rough grinding groove and the precision grinding groove.
- the end surface grinding performed in the present invention is an inscribed grinding process.
- the grindstone used for the end surface grinding of the present invention is an inscribed grinding grindstone.
- the end face grinding of the present invention will be described in detail.
- the outer peripheral side end surface of the glass substrate is brought into contact with the inner peripheral side of the grindstone formed in a cylindrical shape, and the glass substrate and the grindstone are relatively moved, whereby the outer periphery of the glass substrate.
- the grindstone (rotary grindstone) 3 for processing the substrate outer peripheral side is in the direction of the arrow 13 (cutting direction) in the figure with respect to the outer peripheral side end surface of the glass substrate 1.
- the grindstone (rotary grindstone) 3 for processing the substrate outer peripheral side is in the direction of the arrow 13 (cutting direction) in the figure with respect to the outer peripheral side end surface of the glass substrate 1.
- the grindstone 3 is formed in a cylindrical shape and has a plurality of parallel groove shapes for forming the end face shape of the glass substrate on the inner peripheral surface thereof.
- the groove shape is such that both the side wall surface and the chamfered surface can be transferred to the outer peripheral side end surface. That is, the grindstone 3 is formed in a predetermined dimensional shape in consideration of a target dimensional shape of the ground surface of the glass substrate 1.
- the peripheral speed and the peripheral speed ratio may be appropriately set so as to be suitable for processing the outer peripheral side end face.
- the glass substrate 1 is rotated in the direction of arrow 10 and the grindstone 3 is rotated in the direction of arrow 11, but the rotation direction is not particularly limited.
- the rotation direction of the grindstone 3 and the glass substrate 1 may be either the same direction (down cut) or a different direction (up cut) at the processing position (contact position).
- the peripheral speed of the grindstone 3 is preferably 300 to 3000 m / min, and the peripheral speed at the processing position of the glass substrate 1 is preferably about 3 to 100 m / min.
- the cooling effect is high and the water-soluble grinding fluid with high safety
- the grindstone 3 has a cross-sectional shape as shown in FIG.
- FIG. 4 is a cross-sectional view showing an embodiment of the grindstone of the present invention used in the end face machining step. That is, the grindstone 3 is formed in a cylindrical shape as a whole and has a plurality of parallel groove shapes on the inner peripheral side thereof.
- the plurality of groove shapes include a groove for rough grinding and a precision grinding process. And a groove for use.
- a rough grinding region 3A and a precision grinding (finish grinding) region 3B are provided, and the rough grinding region 3A includes a plurality of grooves 3a, 3a,. ..
- the precision grinding region 3B has a plurality of grooves 3b, 3b.
- Each of the plurality of groove shapes of the grindstone 3 may be formed so that both the side wall surface and the chamfered surface of the outer peripheral side end surface of the glass substrate 1 can be ground simultaneously.
- the coarse grinding region 3A and the fine grinding region 3B have different abrasive grain sizes.
- rough grinding is performed in the coarse grinding region 3A of abrasive grains having a large abrasive grain size (coarse count abrasive grains).
- precision grinding finish grinding
- the grindstone 3 according to the present invention has means for suppressing the grinding waste generated when grinding is performed in the rough grinding groove 3a from moving to the precision grinding groove 3b. ing.
- the present embodiment includes a rough grinding region 3A including a plurality of grooves 3a for rough grinding and a plurality of grooves 3b for precision grinding.
- a step 31 serving as a wall is provided between the precision grinding region 3B and the diameter of the grindstone is made different. Therefore, the rough grinding groove 3a is disposed in the region having the larger grindstone diameter, and the precision grinding groove 3b is disposed in the region having the smaller grindstone diameter.
- the step 31 prevents the grinding scraps from reaching the groove 3b for precision grinding. Can be suppressed.
- a conventional configuration is used in order to suppress movement of grinding waste generated when grinding is performed in the rough grinding groove 3a to the precision grinding groove 3b. As shown in FIG. 3, in the precision grinding, it is possible to effectively reduce the occurrence of chipping due to the influence of the coarse grinding sludge accumulated in the precision grinding groove 2b.
- the grinding wheel diameter (hereinafter referred to as “the diameter of the precision grinding wheel”) of the precision grinding region 3 ⁇ / b> B including the plurality of grooves 3 b for precision grinding is preferably as follows. . That is, when the diameter of the glass substrate 1 to be processed is L (mm), the diameter of the precision grinding wheel is preferably L + 1 (mm) or more and 300 mm or less. More preferably, it is L + 5 (mm) or more and 2 L (mm) or less.
- the diameter of the precision grinding wheel is smaller than L + 1 (mm), the grinding wheel wears out quickly and the productivity may deteriorate.
- the diameter of the precision grinding wheel is larger than 300 mm, the size of the grinding wheel becomes large and the cost may increase. Moreover, it may be difficult to move the grindstone with high accuracy.
- the diameter of the grindstone here means the diameter at the position of the groove bottom surface of the grindstone.
- the groove bottom surface of the grindstone is the deepest bottom surface of the groove, and is usually a processing surface for grinding the side wall surface of the substrate end surface. In the following, the same meaning is used.
- the grinding wheel diameter (hereinafter referred to as “rough grinding wheel diameter”) of the rough grinding region 3 ⁇ / b> A including the plurality of rough grinding grooves 3 a and the diameter of the precision grinding wheel are as follows.
- the difference is preferably as follows.
- the value obtained by subtracting the diameter of the precision grinding wheel from the diameter of the rough grinding wheel, that is, the difference between the diameter of the coarse grinding wheel and the diameter of the precision grinding wheel is preferably 0.4 mm or more and 60 mm or less. More preferably, it is 4 mm or more and 20 mm or less.
- the difference between the diameter of the coarse grinding wheel and the diameter of the precision grinding wheel is less than 0.4 mm, the grinding dust generated when grinding with the coarse grinding groove will become a precision grinding groove. The effect of suppressing movement cannot be sufficiently obtained.
- the difference between the diameter of the coarse grinding wheel and the diameter of the precision grinding wheel is larger than 60 mm, the processing becomes difficult and the cost increases, and the moving distance of the glass substrate to be processed increases, so that the productivity may deteriorate. There is sex.
- the grinding scraps generated by precision grinding do not affect the generation of defects by precision grinding. That is, when the size of the grinding waste depending on the abrasive grain size in a certain grinding process is larger than the size of the grinding waste generated by the grinding, a defect is generated in the glass substrate. In short, the problem is that grinding scrap generated by rough grinding accumulates in the grooves for precision grinding, which causes defects such as chipping on the glass substrate by precision grinding.
- Examples of the grindstone 3 used in the inscribed end face grinding of the present invention include, for example, a so-called electrodeposition grindstone obtained by electrodeposition of diamond, Al 2 O 3 , SiC, CBN or the like, which is a high-rigidity material, or composite abrasive grains thereof.
- a so-called metal grindstone in which abrasive grains are hardened with a metallic binder is suitable.
- the abrasive grain layer can be made relatively thin with respect to the base metal, so that the groove-shaped transfer shape can be maintained relatively accurately over the entire usable period of the grindstone.
- the grinding action is performed by the abrasive grains protruding from the metallic bond layer, which is preferable because the roughness is suppressed.
- the grain size of the abrasive grains for example, # 200 to # 800 for rough grinding, and for example # 800 to # 4000 for precision grinding are suitable.
- the height of the raised portion 41 is preferably 0.2 mm or more and 30 mm or less. More preferably, it is 2 mm or more and 10 mm or less.
- the height of the raised part said here shall say the length from the lower end (position of the grindstone surface in a place without a groove
- the height of the raised portion 41 is smaller than 0.2 mm, it is possible to prevent the grinding dust generated when grinding is performed in the rough grinding groove from moving to the precision grinding groove. The effect cannot be obtained sufficiently.
- the height of the raised portion 41 is larger than 30 mm, processing is difficult and cost is increased, and the moving distance of the glass substrate to be processed is increased, so that productivity may be deteriorated.
- the coarse grinding region 4A and the precision grinding are performed. Since it is blocked by the raised portion 41 provided between the processing region 4B and the grinding scrap generated in the rough grinding groove 4a, it is prevented from reaching and accumulating in the precision grinding groove 4b. Can do.
- a rough grinding region 5A including a plurality of grooves 5a for rough grinding As shown in FIG. 6, a rough grinding region 5A including a plurality of grooves 5a for rough grinding, A step 51 is provided between the precision grinding region 5B including the plurality of grooves 5b, and the grindstone diameter is different from that in the embodiment shown in FIG.
- the coarse grinding region 5A and the precision grinding are performed. Since it is obstructed by the step 51 between the processing region 5B, it is possible to suppress the grinding waste generated in the rough grinding groove 5a from reaching and accumulating in the precision grinding groove 5b.
- a rough grinding region 6A including a plurality of grooves 6a for rough grinding and a plurality of grooves 6b for precision grinding are included.
- a step 61 having a cross-sectional shape as shown in the figure is provided between the precision grinding region 6B and the grindstone diameter is different from that in the embodiment shown in FIG.
- rough grinding is performed. It is possible to suppress grinding waste generated in the grinding groove 6a from reaching and accumulating in the precision grinding groove 6b.
- the present invention includes an embodiment in which a plurality of steps are provided in a plurality of steps and there are a plurality of regions having different grindstone diameters.
- the rough grinding groove is disposed in a region having a larger grinding wheel diameter
- the precise grinding groove is disposed in a region having a smaller grinding wheel diameter.
- the coarse grinding groove is disposed in the region having the largest grindstone diameter
- the precision grinding groove is disposed in the region having the smallest grindstone diameter.
- a groove for processing in the second stage of rough grinding is arranged.
- the grinding may be performed while rotating both of the glass substrates while the rotation axis of the glass substrate is inclined with respect to the rotation axis of the cylindrical grinding wheel.
- the trajectory of the grindstone that comes into contact with the end surface of the glass substrate 1 does not become constant, and the convex portions (abrasive grains) of the grindstone come into contact with and act at random positions on the end surface of the substrate. Therefore, the surface roughness and in-plane variation of the ground surface can be reduced, and the ground surface can be finished with higher smoothness.
- a conventional brush polishing process or the like may be performed as necessary.
- the glass type used for the magnetic disk glass substrate is not particularly limited.
- the glass substrate material include aluminosilicate glass, soda lime glass, soda aluminosilicate glass, aluminoborosilicate glass, borosilicate glass, Examples thereof include glass ceramics such as quartz glass, chain silicate glass, or crystallized glass. Of these, aluminosilicate glass is particularly preferable because it is excellent in impact resistance and vibration resistance.
- the glass substrate that has been subjected to the grinding and polishing steps of the outer peripheral side and inner peripheral side end surfaces of the substrate as described above is then subjected to a mirror polishing step, a chemical strengthening step, and the like of the main surface, as shown in FIG. Such a magnetic disk glass substrate 1 is obtained.
- the aluminum alloy substrate includes an aluminum alloy substrate and an aluminum alloy substrate having a NiP alloy formed on the surface thereof.
- the present invention also provides a magnetic disk manufacturing method in which at least a magnetic layer is formed on the main surface of the magnetic disk glass substrate manufactured by the above-described method for manufacturing a magnetic disk glass substrate according to the present invention. That is, for example, a magnetic disk can be obtained by forming at least a magnetic layer on a glass substrate for a magnetic disk obtained by the above-described embodiment of the present invention. Usually, for example, a magnetic disk in which an adhesion layer, a soft magnetic layer, an underlayer, a magnetic layer, a protective layer, a lubricating layer, and the like are provided on a glass substrate is preferable.
- the magnetic layer may be, for example, an alloy having a Co-based hcp crystal structure for a perpendicular magnetic recording medium.
- a protective layer a carbon-type protective layer etc. are mentioned preferably, for example.
- the lubricant that forms the lubricating layer on the protective layer include PFPE (perfluoropolyether) compounds.
- PFPE perfluoropolyether
- a plasma CVD method is also preferably used for forming the carbon-based protective layer.
- a dipping method or the like can be used for forming the lubricating layer.
- the end surface of the substrate can be finished with high quality, and the surface state of the substrate end surface is caused. Therefore, it is possible to provide a magnetic disk capable of preventing the occurrence of the failure and realizing higher recording density and higher reliability.
- Example 1 a glass substrate (glass base plate) made of a disc-shaped aluminosilicate glass having a diameter of 66 mm ⁇ and a plate thickness of 0.9 mm was obtained from molten glass by a direct press method.
- the outer peripheral end face of the substrate was ground.
- an electrodeposition grindstone having a diameter difference as shown in FIG. 4 was selected.
- the diameter of the precision grinding wheel was 110 mm
- the diameter of the rough grinding wheel was 116 mm.
- the definition of the diameter of the grindstone is as described above.
- the depth of the grindstone groove is 0.5 mm
- the width of the groove bottom is 0.5 mm
- the opening angle of the groove is 45 degrees.
- the groove shape can be either a rough grinding region or a precision grinding region. The same is true.
- the size (count) of the abrasive grains for rough grinding is # 500
- the size (count) of the abrasive grains for precision grinding is # 1000. Grinding is performed by the positional relationship between the glass substrate and the grindstone shown in FIG. 2, and the peripheral speed, rotation direction, and cutting speed of each of the glass substrate and the grindstone can be appropriately set.
- the rotation speed of the glass substrate was 200 rpm
- the rotation speed of the grindstone was 6000 rpm
- the rotation direction of the glass substrate and the grindstone was reversed.
- Example 2 Grinding was performed in the same manner as in Example 1 except that the electrodeposition grindstone having a cross-sectional shape as shown in FIG. 5 was used. Both the diameter of the precision grinding wheel and the diameter of the rough grinding wheel were 110 mm, and the height of the raised portion was 3 mm. The definition of the height of the raised portion is as described above.
- the depth of the grindstone groove is 0.5 mm, the width of the groove bottom is 0.5 mm, and the opening angle of the groove is 45 degrees.
- the groove shape can be either a rough grinding region or a precision grinding region. The same is true.
- End face processing of 100 glass substrates is performed, and the corner portion A formed by the side wall surface and the chamfered surface and the main surface and the chamfered surface are formed on the 100 glass substrates obtained in the same manner as in Example 1.
- the presence or absence of chipping at the corner B was examined by visual observation and microscopic observation.
- Example 2 Further, as a comparative example, grinding was performed in the same manner as in Example 1 except that an electrodeposited grinding stone having a cross-sectional shape as shown in FIG. 3 was used. Both the diameter of the precision grinding wheel and the diameter of the rough grinding wheel were 110 mm. The depth of the grindstone groove is 0.5 mm, the width of the groove bottom is 0.5 mm, and the opening angle of the groove is 45 degrees. The groove shape can be either a rough grinding region or a precision grinding region. The same is true. End face processing of 100 glass substrates is performed, and the corner portion A formed by the side wall surface and the chamfered surface and the main surface and the chamfered surface are formed on the 100 glass substrates obtained in the same manner as in Example 1. The presence or absence of chipping at the corner B (see FIG. 1) was examined by visual observation and microscopic observation.
- Example 1 and Example 2 were both 3% or less, whereas in the comparative example, they were very high at 60%. In particular, chipping occurred frequently after the 20th sheet.
- the grindstone after the processing was finished, the grooves for precision grinding were observed in detail. In the grindstone used in Example 1 and Example 2, almost no sludge was found, but this was used in the comparative example. In the grindstone, sludge accumulation was observed.
- the present invention there is provided means for suppressing the movement of the grinding scrap generated when grinding is performed in the rough grinding groove to the precision grinding groove. Since a grinding wheel was used, the occurrence of chipping could be suppressed and grinding with good finished surface quality could be performed. On the other hand, in the processing using the conventional inscribed grinding wheel, since sludge of grinding scraps in coarse grinding accumulates in the grooves for precision grinding, the occurrence rate of chipping is high, and the yield is significantly reduced. In Example 2 described above, there is a possibility that the flow of the grinding fluid may be hindered by the raised portion of the grindstone, and there is a possibility that the supply method of the grinding fluid may be complicated in order to sufficiently distribute the grinding fluid to the processing surface. is there. On the other hand, in the first embodiment, since the grinding fluid is supplied from the precision grinding wheel side, the grinding fluid is sufficiently supplied to the rough grinding stone side, and the supply method is not complicated, which is more preferable. .
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- Grinding And Polishing Of Tertiary Curved Surfaces And Surfaces With Complex Shapes (AREA)
Abstract
Description
上記のように安価で高記録密度を達成できる磁気ディスクが求められているが、磁気ディスクの高記録密度化のためには、基板の加工精度にも高度なものが要求されており、それは基板の主表面のみならず、端面形状においても同様である。
従来の内接型研削用砥石の溝形状は、例えば図3に示すように、複数の溝2a,2a・・・を含む粗研削加工用領域2Aと、複数の溝2b,2b・・・を含む精密研削加工用領域2Bとを備えている。粗研削加工用領域2Aと精密研削加工用領域2Bでは砥粒径が異なり、最初に砥粒径が大きい砥粒(粗い番手の砥粒)の粗研削加工用領域2Aで粗研削を行い、続いて、砥粒径が小さい砥粒(細かい番手の砥粒)の精密研削加工用領域2Bで精密研削(仕上げ研削)を行うことができる。
本発明者は、さらに鋭意検討した結果、粗研削加工用の溝で研削加工を行っている際に発生する研削屑が精密研削加工用の溝に移動することを抑制する手段を設けることで上記の問題を解決できることを見出し、本発明を完成するに到ったものである。
すなわち、本発明は、前記課題を解決するため、以下の構成としている。
円板状の基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理を有する磁気ディスク用基板の製造方法であって、前記砥石は、円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削加工用の溝で研削加工を行っている際に発生する研削屑が前記精密研削加工用の溝に移動することを抑制する手段を有しており、前記粗研削加工用の溝と前記精密研削加工用の溝に順次前記基板の外周側端面を接触させることにより、前記基板の外周側端面を研削加工することを特徴とする磁気ディスク用基板の製造方法。
前記研削屑が前記精密な研削加工用の溝に移動することを抑制する手段は、前記粗研削用の溝と前記精密研削加工用の溝との間に壁を設ける手段であることを特徴とする構成1に記載の磁気ディスク用基板の製造方法。
前記研削屑が前記精密な研削加工用の溝に移動することを抑制する手段は、前記粗研削用の溝と前記精密研削加工用の溝との間に壁となる段差を設けて砥石直径を異ならしめ、砥石直径の大きい方に前記粗研削加工用の溝を配置し、砥石直径の小さい方に前記精密研削用の溝を配置する手段であることを特徴とする構成1又は2に記載の磁気ディスク用基板の製造方法。
円板状の基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理を有する磁気ディスク用基板の製造方法であって、前記砥石は、円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削用の溝と前記精密研削加工用の溝との間には隆起部があり、前記粗研削加工用の溝と前記精密研削加工用の溝に順次前記基板の外周側端面を接触させることにより、前記基板の外周側端面を研削加工することを特徴とする磁気ディスク用基板の製造方法。
円板状の基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理を有する磁気ディスク用基板の製造方法であって、前記砥石は、円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記砥石の内周側には段差が設けられて直径の異なる複数の領域が存在し、前記直径の大きい領域に前記粗研削加工用の溝を配置し、前記直径の小さい方に前記精密研削用の溝を配置し、前記粗研削加工用の溝と前記精密研削加工用の溝に順次前記基板の外周側端面を接触させることにより、前記基板の外周側端面を研削加工することを特徴とする磁気ディスク用基板の製造方法。
前記砥石として、電着砥石を用いることを特徴とする構成1乃至5のいずれかに記載の磁気ディスク用基板の製造方法。
円板状の磁気ディスク用基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理に用いる研削用砥石であって、前記研削用砥石は、円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削加工用の溝で研削加工を行っている際に発生する研削屑が前記精密研削加工用の溝に移動することを抑制する手段を有していることを特徴とする研削用砥石。
円板状の磁気ディスク用基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理に用いる研削用砥石であって、前記砥石は、円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削用の溝と前記精密研削加工用の溝との間には隆起部を有することを特徴とする研削用砥石。
円板状の磁気ディスク用基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理に用いる研削用砥石であって、前記砥石は、円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記砥石の内周側には段差が設けられて直径の異なる複数の領域が存在し、前記直径の大きい領域に前記粗研削加工用の溝を配置し、前記直径の小さい方に前記精密研削用の溝を配置していることを特徴とする研削用砥石。
図1は、本発明が適用される磁気ディスク用ガラス基板1の外周側端部の断面図である。該ガラス基板1は、図1には示されていないが、中心部に円孔を有する全体が円板状に形成され(図2を参照)、その表裏の主表面1a,1aと、これら主表面1a,1a間に形成される外周側の端面と内周側の端面を有する。
なお、本明細書においては、ダイレクトプレス法やフロート法等により得られたガラス板を所定の円板状に加工したガラス基板(ガラス素板)から、このガラス基板に加工、処理等を施して作製される最終製品のガラス基板にいたるまで、説明の便宜上、すべてガラス基板もしくは磁気ディスク用ガラス基板と呼ぶこととする。
まず、上記ガラス基板1の端面の研削・研磨工程について説明する。
本発明で行う端面研削加工は、内接型研削加工である。また、本発明の端面研削加工に用いる砥石は、内接型研削加工用砥石である。以下、かかる本発明の端面研削加工について詳しく説明する。
また、このような研削加工に使用する研削液(クーラント)については、冷却効果が高く、生産現場において安全性の高い水溶性の研削液が好適である。
すなわち、上記砥石3は、全体が円筒状に形成されているとともにその内周側に複数の並列した溝形状を有し、この複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含む。具体的には、図4に示すように、粗研削加工用領域3Aと精密研削(仕上げ研削)加工用領域3Bとを備えており、粗研削加工用領域3Aには複数の溝3a,3a・・・を有し、精密研削加工用領域3Bには同じく複数の溝3b,3b・・・を有している。砥石3の複数の溝形状の夫々は、ガラス基板1の外周側端面の側壁面と面取面の両方を同時に研削加工できるように形成されていてもよい。
本発明に係る上記砥石3は、上記粗研削加工用の溝3aで研削加工を行っている際に発生する研削屑が上記精密研削加工用の溝3bに移動することを抑制する手段を有している。
すなわち、加工するガラス基板1の直径をL(mm)とするとき、精密研削砥石の直径は、L+1(mm)以上、300mm以下であることが好ましい。より好ましくは、L+5(mm)以上、2L(mm)以下であることが望ましい。
粗研削砥石の直径から精密研削砥石の直径を引いた値、すなわち、粗研削砥石の直径と精密研削砥石の直径の差は、0.4mm以上、60mm以下であることが好ましい。より好ましくは、4mm以上、20mm以下であることが望ましい。
なお、ここで言う隆起部の高さとは、隆起部の下端(溝のないところの砥石面の位置)から先端(頂点)までの長さを言うものとする。以下においても、同様の意味で用いる。
上記隆起部41の高さが、0.2mmよりも小さいと、粗研削加工用の溝で研削加工を行っている際に発生する研削屑が精密研削加工用の溝に移動することを抑制する効果が十分に得られない。一方、上記隆起部41の高さが、30mmよりも大きいと、加工が難しくコストが高くなったり、加工するガラス基板の移動距離が大きくなるので、生産性が悪化する可能性がある。
本実施形態では、粗研削加工用の溝5aで研削加工を行っている際に発生する研削屑がたとえ精密研削加工用領域5Bの方へ飛散したとしても、粗研削加工用領域5Aと精密研削加工用領域5Bとの間の段差51によって阻まれるので、粗研削用の溝5aで発生した研削屑が精密研削加工用の溝5bに到達し、堆積することを抑制することができる。
本実施形態においても、粗研削加工用の溝6aで研削加工を行っている際に発生する研削屑が精密研削加工用領域6Bの方へ飛散したとしても、上記段差61によって阻まれるので、粗研削用の溝6aで発生した研削屑が精密研削加工用の溝6bに到達し、堆積することを抑制することができる。
また、必要に応じて、上述の本発明の端面研削加工に加えて、従来のブラシ研磨加工等を行ってもよい。
以上のようにして、基板の外周側及び内周側端面の研削、研磨工程を終えたガラス基板に、続いて主表面の鏡面研磨工程、化学強化工程、等を施すことにより、図1に示すような磁気ディスク用ガラス基板1が得られる。
すなわち、例えば上述の本発明に係る実施の形態により得られる磁気ディスク用ガラス基板上に、少なくとも磁性層を形成することにより磁気ディスクが得られる。通常は、例えばガラス基板上に、付着層、軟磁性層、下地層、磁性層、保護層、潤滑層などを設けた磁気ディスクとするのが好適である。
また、保護層としては、例えば、炭素系保護層などが好ましく挙げられる。また、保護層上の潤滑層を形成する潤滑剤としては、PFPE(パーフロロポリエーテル)系化合物が挙げられる。
ガラス基板上に上記各層を成膜する方法については、公知のスパッタリング法などを用いることができる。炭素系保護層の成膜についてはプラズマCVD法も好ましく用いられる。また、潤滑層の成膜にはディップ法などを用いることができる。
(実施例1)
まず、溶融ガラスからダイレクトプレス法により直径66mmφ、板厚0.9mmの円板状のアルミノシリケートガラスからなるガラス基板(ガラス素板)を得た。
使用した砥石は、前述の図4に示したような直径差のある電着砥石を選択した。精密研削砥石の直径は110mm、粗研削砥石の直径は116mmとした。砥石の直径の定義は前記のとおりである。また、砥石の溝の深さは0.5mm、溝底面の幅は0.5mm、溝の開口角は45度であり、これら溝形状は、粗研削加工用領域と精密研削加工用領域のいずれもおいても同じである。なお、粗研削用の砥粒の大きさ(番手)は#500、精密研削用の砥粒の大きさ(番手)は#1000である。
研削加工は、前述の図2に示すガラス基板と砥石との配置関係で行い、ガラス基板と砥石の各々の周速度、回転方向、切込み速度は適宜設定することができるが、本実施例では、ガラス基板回転数は200rpm、砥石回転数は6000rpm、ガラス基板と砥石の回転方向は逆回転とした。
得られた100枚のガラス基板について、側壁面と面取面との成す角部Aおよび主表面と面取面との成す角部B(図1参照)でのチッピングの発生の有無を目視と顕微鏡観察により調査した。
前述の図5に示すような断面形状の電着砥石を用いたこと以外は上記実施例1と同様に研削加工を行った。
精密研削砥石の直径、粗研削砥石の直径とも110mmとし、隆起部の高さは3mmとした。隆起部の高さの定義は前記のとおりである。また、砥石の溝の深さは0.5mm、溝底面の幅は0.5mm、溝の開口角は45度であり、これら溝形状は、粗研削加工用領域と精密研削加工用領域のいずれもおいても同じである。
100枚のガラス基板の端面加工を行い、実施例1と同様に、得られた100枚のガラス基板について、側壁面と面取面との成す角部Aおよび主表面と面取面との成す角部B(図1参照)でのチッピングの発生の有無を目視と顕微鏡観察により調査した。
また、比較例として、前述の図3に示すような断面形状の電着砥石を用いたこと以外は上記実施例1と同様に研削加工を行った。
精密研削砥石の直径、粗研削砥石の直径とも110mmとした。また、砥石の溝の深さは0.5mm、溝底面の幅は0.5mm、溝の開口角は45度であり、これら溝形状は、粗研削加工用領域と精密研削加工用領域のいずれもおいても同じである。
100枚のガラス基板の端面加工を行い、実施例1と同様に、得られた100枚のガラス基板について、側壁面と面取面との成す角部Aおよび主表面と面取面との成す角部B(図1参照)でのチッピングの発生の有無を目視と顕微鏡観察により調査した。
また、加工終了後の砥石について、精密研削加工用の溝を詳細に観察したところ、実施例1および実施例2に使用した砥石では、スラッジの堆積はほとんど認められなかったが、比較例に使用した砥石では、スラッジの堆積が認められた。
これに対し、従来の内接型研削砥石による加工では、精密研削加工用の溝に粗研削での研削屑のスラッジが堆積するため、チッピングの発生率が高く、歩留りが著しく低下してしまう。
なお、上記実施例2では、研削液の流れが砥石の隆起部によって妨げられる可能性があり、十分に研削液を加工面に行き渡らせるためには研削液の供給方法が複雑になる可能性がある。これに対し、上記実施例1では、研削液の供給を精密研削砥石側から行うことにより、粗研削砥石側へも研削液が十分に供給され、供給方法は複雑にならなくて済むのでより好ましい。
2~6 外周側端面研削用砥石
1a ガラス基板の主表面
1b 側壁面
1c 面取面
31 段差
41 隆起部(壁)
Claims (9)
- 円板状の基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理を有する磁気ディスク用基板の製造方法であって、
前記砥石は、円筒状に形成されているとともにその内周側に複数の溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削加工用の溝で研削加工を行っている際に発生する研削屑が前記精密研削加工用の溝に移動することを抑制する手段を有しており、
前記粗研削加工用の溝と前記精密研削加工用の溝に順次前記基板の外周側端面を接触させることにより、前記基板の外周側端面を研削加工することを特徴とする磁気ディスク用基板の製造方法。 - 前記研削屑が前記精密な研削加工用の溝に移動することを抑制する手段は、前記粗研削用の溝と前記精密研削加工用の溝との間に壁を設ける手段であることを特徴とする請求項1に記載の磁気ディスク用基板の製造方法。
- 前記研削屑が前記精密な研削加工用の溝に移動することを抑制する手段は、前記粗研削用の溝と前記精密研削加工用の溝との間に壁となる段差を設けて砥石直径を異ならしめ、砥石直径の大きい方に前記粗研削加工用の溝を配置し、砥石直径の小さい方に前記精密研削用の溝を配置する手段であることを特徴とする請求項1又は2に記載の磁気ディスク用基板の製造方法。
- 円板状の基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理を有する磁気ディスク用基板の製造方法であって、
前記砥石は、円筒状に形成されているとともにその内周側に複数の溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削用の溝と前記精密研削加工用の溝との間には隆起部があり、
前記粗研削加工用の溝と前記精密研削加工用の溝に順次前記基板の外周側端面を接触させることにより、前記基板の外周側端面を研削加工することを特徴とする磁気ディスク用基板の製造方法。 - 円板状の基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理を有する磁気ディスク用基板の製造方法であって、
前記砥石は、円筒状に形成されているとともにその内周側に複数の溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、
前記砥石の内周側には段差が設けられて直径の異なる複数の領域が存在し、前記直径の大きい領域に前記粗研削加工用の溝を配置し、前記直径の小さい方に前記精密研削用の溝を配置し、
前記粗研削加工用の溝と前記精密研削加工用の溝に順次前記基板の外周側端面を接触させることにより、前記基板の外周側端面を研削加工することを特徴とする磁気ディスク用基板の製造方法。 - 前記砥石として、電着砥石を用いることを特徴とする請求項1乃至5のいずれかに記載の磁気ディスク用基板の製造方法。
- 円板状の磁気ディスク用基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理に用いる研削用砥石であって、
前記研削用砥石は、円筒状に形成されているとともにその内周側に複数の溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削加工用の溝で研削加工を行っている際に発生する研削屑が前記精密研削加工用の溝に移動することを抑制する手段を有していることを特徴とする研削用砥石。 - 円板状の磁気ディスク用基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理に用いる研削用砥石であって、
前記砥石は、円筒状に形成されているとともにその内周側に複数の溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、前記粗研削用の溝と前記精密研削加工用の溝との間には隆起部を有することを特徴とする研削用砥石。 - 円板状の磁気ディスク用基板の端面部分に研削液を接触させつつ、前記基板の外周側端面に砥石を接触させて相対的に移動させることにより前記基板の端面を研削加工する処理に用いる研削用砥石であって、
前記砥石は、円筒状に形成されているとともにその内周側に複数の溝形状を有し、前記複数の溝形状は、粗研削加工用の溝と、精密研削加工用の溝とを含み、
前記砥石の内周側には段差が設けられて直径の異なる複数の領域が存在し、前記直径の大きい領域に前記粗研削加工用の溝を配置し、前記直径の小さい方に前記精密研削用の溝を配置していることを特徴とする研削用砥石。
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| CN117620785A (zh) * | 2023-12-15 | 2024-03-01 | 先导薄膜材料(广东)有限公司 | 一种靶材的加工方法 |
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| JP6645935B2 (ja) | 2020-02-14 |
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