WO2015052212A3 - Apparatur und verfahren zur untersuchung von diskontinuierlichen produktfluidströmen bei der umsetzung von eduktfluidströmen an feststoffkatalysatoren - Google Patents

Apparatur und verfahren zur untersuchung von diskontinuierlichen produktfluidströmen bei der umsetzung von eduktfluidströmen an feststoffkatalysatoren Download PDF

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Publication number
WO2015052212A3
WO2015052212A3 PCT/EP2014/071502 EP2014071502W WO2015052212A3 WO 2015052212 A3 WO2015052212 A3 WO 2015052212A3 EP 2014071502 W EP2014071502 W EP 2014071502W WO 2015052212 A3 WO2015052212 A3 WO 2015052212A3
Authority
WO
WIPO (PCT)
Prior art keywords
fluid flows
outlet pipe
studying
product fluid
reaction
Prior art date
Application number
PCT/EP2014/071502
Other languages
English (en)
French (fr)
Other versions
WO2015052212A2 (de
Inventor
Armin Lange De Oliveira
Nadine Brem
Mario Soorholtz
Johannes Lieberknecht
Original Assignee
Hte Gmbh The High Throughput Experimentation Company
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hte Gmbh The High Throughput Experimentation Company filed Critical Hte Gmbh The High Throughput Experimentation Company
Priority to EP14781876.9A priority Critical patent/EP3055057A2/de
Priority to US15/028,242 priority patent/US10338042B2/en
Publication of WO2015052212A2 publication Critical patent/WO2015052212A2/de
Publication of WO2015052212A3 publication Critical patent/WO2015052212A3/de

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/10—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00281—Individual reactor vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00281—Individual reactor vessels
    • B01J2219/00286—Reactor vessels with top and bottom openings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00477—Means for pressurising the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00479—Means for mixing reactants or products in the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B01J2219/00704—Processes involving means for analysing and characterising the products integrated with the reactor apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B01J2219/00707—Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/00747—Catalysts
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B30/00—Methods of screening libraries
    • C40B30/08—Methods of screening libraries by measuring catalytic activity
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B60/00—Apparatus specially adapted for use in combinatorial chemistry or with libraries
    • C40B60/12—Apparatus specially adapted for use in combinatorial chemistry or with libraries for screening libraries

Abstract

Die Erfindung betrifft eine Apparatur und ein Verfahren zur Untersuchung von Feststoffkatalysatoren und Prozessen, bei denen diskontinuierliche Fluidströme auftreten. Die erfindungsgemäße Apparatur, die vorzugsweise zur parallelen Untersuchung von einer Mehrzahl von Katalysatoren ausgelegt ist, weist zumindest einen Reaktionsraumauf, wobei jedem Reaktionsraum ein oder mehrere Fluidmischräume nachgeschaltet sind. Die Ausgangsleitung des Fluidmischraums oder auch die Ausgangsleitung einer Sequenz von Fluidmischräumen steht mit einem Drosselelement (11) in Wirkverbindung, wobei das Drosselelement (11) mit einem Analysengerät sowie einer Ausgangsleitung in Wirkverbindung steht und die Ausgangsleitung eine Regeleinrichtung aufweist. Das erfindungsgemäße Verfahren ist durch eine zyklische Betriebsweise gekennzeichnet, bei der einekontrollierte Zuführung von zumindest einem Produktfluid in den zumindest einen Fluidmischraum erfolgt, der Produktfluidstrom im Mischraum durchmischt wird und der zumindest eine durchmischte Produkfluidstrom der Ausgangsleitung und dem Analysengerät zugeführt wird. Ein Zyklus hat eine Zeitdauer im Bereich von 0,2bis 7200 Sekunden und kann dabei mehrere Phasen mit unterschiedlicher Zusammensetzung aufweisen. Das Verfahren kanneine Mehrzahl von Zyklen umfassen.
PCT/EP2014/071502 2013-10-08 2014-10-08 Apparatur und verfahren zur untersuchung von diskontinuierlichen produktfluidströmen bei der umsetzung von eduktfluidströmen an feststoffkatalysatoren WO2015052212A2 (de)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP14781876.9A EP3055057A2 (de) 2013-10-08 2014-10-08 Apparatur und verfahren zur untersuchung von diskontinuierlichen produktfluidströmen bei der umsetzung von eduktfluidströmen an feststoffkatalysatoren
US15/028,242 US10338042B2 (en) 2013-10-08 2014-10-08 Apparatus and method for investigating discontinuous product fluid streams in the reaction of reactant fluid streams over solid catalysts

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102013016585.7 2013-10-08
DE102013016585.7A DE102013016585A1 (de) 2013-10-08 2013-10-08 Apparatur und Verfahren zur Untersuchung von diskontinuierllichen Produktfluidströmen bei der Umsetzung von Eduktfluidströmen an Feststoffkatalysatoren

Publications (2)

Publication Number Publication Date
WO2015052212A2 WO2015052212A2 (de) 2015-04-16
WO2015052212A3 true WO2015052212A3 (de) 2015-07-16

Family

ID=51688058

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2014/071502 WO2015052212A2 (de) 2013-10-08 2014-10-08 Apparatur und verfahren zur untersuchung von diskontinuierlichen produktfluidströmen bei der umsetzung von eduktfluidströmen an feststoffkatalysatoren

Country Status (4)

Country Link
US (1) US10338042B2 (de)
EP (1) EP3055057A2 (de)
DE (1) DE102013016585A1 (de)
WO (1) WO2015052212A2 (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021501686A (ja) * 2017-11-03 2021-01-21 ハーテーエー・ゲーエムベーハー・ザ・ハイ・スループット・イクスペリメンテイション・カンパニー 触媒プロセスの特性評価のための装置および方法
EP3960286B1 (de) 2020-08-26 2023-08-16 HTE GmbH The High Throughput Experimentation Company Vorrichtung und verfahren zur untersuchung von feststoffen

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002092220A1 (en) * 2001-05-11 2002-11-21 Avantium International B.V. Reactor assembly
US20030040116A1 (en) * 2000-02-08 2003-02-27 Canos Avelino Corma Catalytic testing device and method for its use in material testing
US6551832B1 (en) * 1999-06-28 2003-04-22 Institut Francais Du Petrole Automatic multi-reactor catalyst evaluation method and device with a heavy feedstock
US20050169815A1 (en) * 2002-05-13 2005-08-04 Avantium International B.V. System for chemical experiments
DE102006053078A1 (de) * 2006-11-10 2008-05-15 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur kontinuierlichen Überführung und Analyse von Fluiden
WO2012052149A2 (de) * 2010-10-22 2012-04-26 Hte Aktiengesellschaft Vorrichtung und verfahren zur untersuchung von katalysatoren mit variabler prozessdruckeinstellung

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7141217B2 (en) 2002-12-05 2006-11-28 Uop Llc Elevated pressure apparatus and method for generating a plurality of isolated effluents
DE10361003B3 (de) 2003-12-23 2005-07-28 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur Druck- und Flusskontrolle in Parallelreaktoren
DE102004039378A1 (de) 2004-08-13 2006-02-23 Hte Ag The High Throughput Experimentation Company Vorrichtung zur kontrollierten Entnahme von Fluidproben aus Druckbehältern
DE102006034172B3 (de) 2006-07-24 2007-09-20 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur Handhabung von Multikomponenten-Gemischen
DE102010050599B4 (de) 2009-11-07 2014-11-13 Hte Gmbh The High Throughput Experimentation Company Vorrichtung und Verfahren zur Testung von Katalysatoren mit verbesserter Prozessdruckeinstellung
DE102011109454A1 (de) * 2011-08-04 2013-02-07 Hte Aktiengesellschaft Verfahren zur Behandlung von Produktfluidströmen

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6551832B1 (en) * 1999-06-28 2003-04-22 Institut Francais Du Petrole Automatic multi-reactor catalyst evaluation method and device with a heavy feedstock
US20030040116A1 (en) * 2000-02-08 2003-02-27 Canos Avelino Corma Catalytic testing device and method for its use in material testing
WO2002092220A1 (en) * 2001-05-11 2002-11-21 Avantium International B.V. Reactor assembly
US20050169815A1 (en) * 2002-05-13 2005-08-04 Avantium International B.V. System for chemical experiments
DE102006053078A1 (de) * 2006-11-10 2008-05-15 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur kontinuierlichen Überführung und Analyse von Fluiden
WO2012052149A2 (de) * 2010-10-22 2012-04-26 Hte Aktiengesellschaft Vorrichtung und verfahren zur untersuchung von katalysatoren mit variabler prozessdruckeinstellung

Also Published As

Publication number Publication date
US20160252485A1 (en) 2016-09-01
US10338042B2 (en) 2019-07-02
WO2015052212A2 (de) 2015-04-16
DE102013016585A1 (de) 2015-04-09
EP3055057A2 (de) 2016-08-17

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