WO2012052149A3 - Vorrichtung und verfahren zur untersuchung von katalysatoren mit variabler prozessdruckeinstellung - Google Patents

Vorrichtung und verfahren zur untersuchung von katalysatoren mit variabler prozessdruckeinstellung Download PDF

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Publication number
WO2012052149A3
WO2012052149A3 PCT/EP2011/005208 EP2011005208W WO2012052149A3 WO 2012052149 A3 WO2012052149 A3 WO 2012052149A3 EP 2011005208 W EP2011005208 W EP 2011005208W WO 2012052149 A3 WO2012052149 A3 WO 2012052149A3
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lines
outlet side
reaction chamber
chamber outlet
pressure adjustment
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PCT/EP2011/005208
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English (en)
French (fr)
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WO2012052149A2 (de
Inventor
Armin Lange De Oliveira
Michael Dejmek
Oliver KÖCHEL
Jürgen BECHTEL
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Hte Aktiengesellschaft
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Priority to US13/880,821 priority Critical patent/US9228985B2/en
Priority to EP11771033.5A priority patent/EP2629886A2/de
Publication of WO2012052149A2 publication Critical patent/WO2012052149A2/de
Publication of WO2012052149A3 publication Critical patent/WO2012052149A3/de

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/10—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00281—Individual reactor vessels
    • B01J2219/00286—Reactor vessels with top and bottom openings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00351—Means for dispensing and evacuation of reagents
    • B01J2219/00389—Feeding through valves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00351—Means for dispensing and evacuation of reagents
    • B01J2219/00389—Feeding through valves
    • B01J2219/00391—Rotary valves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00351—Means for dispensing and evacuation of reagents
    • B01J2219/00423—Means for dispensing and evacuation of reagents using filtration, e.g. through porous frits
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00477—Means for pressurising the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00495—Means for heating or cooling the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00585—Parallel processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00596—Solid-phase processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00601—High-pressure processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00686—Automatic
    • B01J2219/00689—Automatic using computers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B01J2219/00707—Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/00747—Catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00788—Three-dimensional assemblies, i.e. the reactor comprising a form other than a stack of plates
    • B01J2219/00792—One or more tube-shaped elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00869—Microreactors placed in parallel, on the same or on different supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00952—Sensing operations
    • B01J2219/00954—Measured properties
    • B01J2219/00963—Pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00986—Microprocessor

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

Die vorliegende Erfindung betrifft eine Katalyseapparatur zur Testung von Katalysatoren mit variabler Prozessdruckeinstellung über einen Druckbereich von 0,01 Millibar bis 300 bar. Vorzugsweise verfügt die Vorrichtung über eine Mehrzahl von parallel angeordneten Reaktionsräumen (101, 102,...), deren reaktionsraumausgangsseitige Leitungen (211, 212,...) in zwei Gruppen von Unterleitungen aufgeteilt sind. Die eine Gruppe von Hauptleitungen (411, 412,...) steht mit einem allen Hauptleitungen gemeinsamen Regelventil (61) und einer Abluftleitung (62) in Wirkverbindung, und die zweite Gruppe von Nebenleitungen (311, 312, 313,...) und Schaltventilen (321, 322,...) steht mit einer Analyseneinheit (34) in Wirkverbindung. Vorzugsweise sind reaktionsraumausgangsseitige Leitungen (201, 202,...) jeweils mit einer separaten Leitungen zur Regelfluidzufuhr (211, 212,...) ausgestattet. In einer bevorzugten Ausführungsform weisen die Verbindungspunkte von den reaktionsraumausgangsseitigen Leitungen (201, 202,...) zu den jeweiligen Hauptleitungen (411, 412,...) und Nebenleitungen (311, 312,...) jeweils einen Mischbehälter (301, 302,...) auf.
PCT/EP2011/005208 2010-10-22 2011-10-17 Vorrichtung und verfahren zur untersuchung von katalysatoren mit variabler prozessdruckeinstellung WO2012052149A2 (de)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US13/880,821 US9228985B2 (en) 2010-10-22 2011-10-17 Device and method for testing catalysts with variable process pressure adjustment
EP11771033.5A EP2629886A2 (de) 2010-10-22 2011-10-17 Vorrichtung und verfahren zur untersuchung von katalysatoren mit variabler prozessdruckeinstellung

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP10013897 2010-10-22
EP10013897.3 2010-10-22

Publications (2)

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WO2012052149A2 WO2012052149A2 (de) 2012-04-26
WO2012052149A3 true WO2012052149A3 (de) 2012-06-21

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US (1) US9228985B2 (de)
EP (1) EP2629886A2 (de)
WO (1) WO2012052149A2 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL2009659C2 (en) 2012-10-18 2014-04-22 Avantium Technologies B V System and method for operating parallel reactors.
US20140335626A1 (en) * 2013-05-10 2014-11-13 Cdti Test Bench Gas Flow Control System and Method
DE102013016585A1 (de) 2013-10-08 2015-04-09 Hte Gmbh The High Throughput Experimentation Company Apparatur und Verfahren zur Untersuchung von diskontinuierllichen Produktfluidströmen bei der Umsetzung von Eduktfluidströmen an Feststoffkatalysatoren
JP6141234B2 (ja) * 2014-03-26 2017-06-07 フロンティア・ラボ株式会社 気相成分分析装置
JP2020528347A (ja) * 2017-07-28 2020-09-24 ハーテーエー・ゲーエムベーハー・ザ・ハイ・スループット・イクスペリメンテイション・カンパニー ０．１〜１０秒の範囲の滞留時間で化学物質を触媒転換するための装置および方法
WO2020064624A1 (de) * 2018-09-24 2020-04-02 Hte Gmbh The High Throughput Experimentation Company Vorrichtung und verfahren zur analyse von reaktionen
WO2022184909A1 (en) * 2021-03-04 2022-09-09 Hte Gmbh The High Throughput Experimentation Company Apparatus for analyzing reaction systems

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WO2003095087A1 (en) * 2002-05-13 2003-11-20 Avantium International B.V. A sampling apparatus
US20040077102A1 (en) * 2002-10-18 2004-04-22 Coute Nicolas P. Chemical reaction and analysis system
WO2004052530A1 (en) * 2002-12-05 2004-06-24 Uop Llc Elevated pressure apparatus and method for generating a plurality of isolated effluents
WO2008055585A1 (de) * 2006-11-10 2008-05-15 Hte Aktiengesellschaft The High Throughput Experimentation Company Vorrichtung und verfahren zur kontinuierlichen überführung und analyse von fluiden
DE102010050599A1 (de) * 2009-11-07 2011-06-30 hte Aktiengesellschaft, 69123 Vorrichtung und Verfahren zur Testung von Katalysatoren mit verbesserter Prozessdruckeinstellung

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US6063633A (en) * 1996-02-28 2000-05-16 The University Of Houston Catalyst testing process and apparatus
ES2166310B1 (es) 2000-02-08 2003-10-16 Univ Valencia Politecnica Dipositivo automatico y metodo de test catalitico multiple
DE10361003B3 (de) * 2003-12-23 2005-07-28 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur Druck- und Flusskontrolle in Parallelreaktoren
DE112010003613T5 (de) * 2009-09-10 2012-11-08 Cummins Ip, Inc. Niedertemperatur-Katalysator für die selektive katalytische Reduktion sowie dazugehörige Systeme und Verfahren

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003095087A1 (en) * 2002-05-13 2003-11-20 Avantium International B.V. A sampling apparatus
US20040077102A1 (en) * 2002-10-18 2004-04-22 Coute Nicolas P. Chemical reaction and analysis system
WO2004052530A1 (en) * 2002-12-05 2004-06-24 Uop Llc Elevated pressure apparatus and method for generating a plurality of isolated effluents
WO2008055585A1 (de) * 2006-11-10 2008-05-15 Hte Aktiengesellschaft The High Throughput Experimentation Company Vorrichtung und verfahren zur kontinuierlichen überführung und analyse von fluiden
DE102010050599A1 (de) * 2009-11-07 2011-06-30 hte Aktiengesellschaft, 69123 Vorrichtung und Verfahren zur Testung von Katalysatoren mit verbesserter Prozessdruckeinstellung

Also Published As

Publication number Publication date
WO2012052149A2 (de) 2012-04-26
US20130273662A1 (en) 2013-10-17
EP2629886A2 (de) 2013-08-28
US9228985B2 (en) 2016-01-05

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