WO2014073767A1 - Appareil à chambre pour expériences de rejet de produits polluants - Google Patents

Appareil à chambre pour expériences de rejet de produits polluants Download PDF

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Publication number
WO2014073767A1
WO2014073767A1 PCT/KR2013/006181 KR2013006181W WO2014073767A1 WO 2014073767 A1 WO2014073767 A1 WO 2014073767A1 KR 2013006181 W KR2013006181 W KR 2013006181W WO 2014073767 A1 WO2014073767 A1 WO 2014073767A1
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WO
WIPO (PCT)
Prior art keywords
chamber
zero gas
liner
main body
product
Prior art date
Application number
PCT/KR2013/006181
Other languages
English (en)
Korean (ko)
Inventor
석광설
송기봉
김기준
이수영
김혁
김삼권
최경희
Original Assignee
대한민국(환경부 국립환경과학원장)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 대한민국(환경부 국립환경과학원장) filed Critical 대한민국(환경부 국립환경과학원장)
Priority to JP2014545842A priority Critical patent/JP5747135B2/ja
Publication of WO2014073767A1 publication Critical patent/WO2014073767A1/fr

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2226Sampling from a closed space, e.g. food package, head space
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2226Sampling from a closed space, e.g. food package, head space
    • G01N2001/2241Sampling from a closed space, e.g. food package, head space purpose-built sampling enclosure for emissions

Definitions

  • the present invention relates to a contaminant emission test chamber device of a product for taking a small product sample, such as a children's article, and more particularly, a part or whole product sample of the product is included in the product sample
  • the product sample can be accurately measured by releasing volatile harmful substances, and the liner inserted into the chamber can be inserted and detached. Since the hazardous substances are measured by replacing only the liner at the time when the hazardous substance measurement is completed, not only the continuous work is possible but also the liner and the first and second connecting tubes are formed to form the main body and the main body. Liner and agent can be installed after the hazardous substance is measured. It is related with the contaminant emission test chamber device of the product which can reduce the time required for cleaning and reduce the time required for cleaning of hazardous substances by replacing the 1, 2 connector with new ones.
  • the prior art related to the present invention discloses a tester for measuring the hazardous materials of building materials disclosed in Korean Patent Publication No. 2005-0087561, which is included in the air by forcibly sucking external air from the air generator 111 as shown in FIG.
  • Clean air supply unit 110 for supplying the clean dry air and wet air to each of the various foreign substances removed by step through the filter;
  • a temperature / humidity unit 120 for introducing dry and wet air generated by the clean air supply 110 to display and control the temperature and humidity of the controller 122 by the sensor 121;
  • the dry and wet air passing through the temperature and humidity unit 120 flows through the pipe and is ventilated to the clean air supply 110 in a state where the building material specimen A is enclosed in a hollow interior and is similar to an indoor environment.
  • the conventional building material hazardous material tester as described above is very inconvenient to clean the inside of the cell 130 and the adsorption tube 140 after the measurement by inserting the product sample (A) inside the cell (130). And because of this there was a problem that continuous operation is impossible.
  • Contaminant emission test chamber device of the product of the present invention for solving the above problems is a control unit;
  • a zero gas supply unit including a zero gas supply source, a flow control valve for adjusting a flow rate of zero gas supplied from the zero gas supply source, and a zero gas supply pipe;
  • a chamber part receiving zero gas from the zero gas supply part;
  • a main body portion formed outside the chamber portion and surrounding the chamber portion;
  • a liner formed to be inserted into and detached from the chamber part, the liner being connected to receive the zero gas supply part, and including a product sample insert part inserted therein; Is coupled to the main body portion, is connected to the chamber portion is supplied with a zero gas containing a harmful substance passing through the liner made of any one of the absorption tube containing the absorbent liquid for measuring the amount of harmful gas or the adsorption tube containing the adsorbent Sample collection unit; characterized in that consisting of.
  • control unit is characterized in that the control button is formed so that the flow control through the control of the dehumidification, preheating and flow control valve for the zero gas supplied from the zero gas supply to the chamber.
  • the main body is composed of an upper body and a lower main body
  • the chamber part and the sample collecting part formed in the main body are also composed of the upper, lower chamber and the upper and lower sample collecting parts, respectively, the lower chamber and the zero gas supply part formed in the lower main body.
  • the zero gas supply pipe is connected to supply zero gas to the liner, and the upper body and the upper sample collection unit are connected to receive zero gas containing harmful substances passing through the liner. .
  • the upper body of the main body portion is characterized in that it is configured to move in the up and down direction by the control unit and the sliding means to insert and detach the liner in the upper chamber, the lower chamber of the chamber.
  • the upper part of the body portion, the upper and lower chamber between the chamber portion coupled to the lower body, and the upper and lower sample collecting portion between the sample collecting portion is characterized in that the Teflon material further comprises a sealing material.
  • a first connecting tube of a detachable and attachable form is formed between the upper body of the main body and the upper sample collecting part of the sample collecting part, and is detached and attached between the lower chamber formed on the lower body and the zero gas supply pipe of the zero gas supply part. It is characterized in that a second connecting tube of a possible form is formed.
  • the upper and lower body formed in the main body portion is characterized in that the upper, lower chamber and the upper and lower sample collecting portion of the chamber portion is configured to be combined in an assembled form by an integral or coupling member.
  • the body portion is characterized in that it further comprises a temperature control device for adjusting the temperature of the chamber portion.
  • the liner is composed of a liner body having an open top, in which a product sample seat is formed inside the product sample insert, and a liner cover is coupled to the top of the liner body.
  • the product sample seating portion formed in the liner body of the liner is characterized in that a plurality of drilling holes are configured.
  • the present invention may be configured to be measured by releasing the volatile harmful substances contained in the product sample by mounting a part or the entire product sample on the liner to measure the product sample accurately.
  • the liner inserted into the chamber part is configured to be inserted and detached, the hazardous substances are measured by replacing only the liner at the time when the hazardous substance measurement is completed after inserting a product sample into a plurality of liners in advance. Because of the loss, continuous work is possible.
  • the liner and the first and second connectors are formed so that the main body and the chamber formed in the main body are not exposed by harmful substances, and the liner and the first and second connectors are replaced with new ones after measuring the harmful substances. Since the measurement of harmful substances in the sample is made, it is a useful invention to shorten the time due to cleaning and to perform the hazardous substance measurement work quickly.
  • FIG. 1 is a block diagram showing a conventional test equipment for measuring harmful substances in building materials.
  • Figure 2 is a perspective view showing a contaminant emission test chamber device of the product according to the present invention.
  • FIG. 3 is a sectional view taken along the line A-A in FIG.
  • FIG. 5 is a sectional view taken along the line BB of FIG. 2.
  • FIG. 6 is a cross-sectional view taken along the line C-C in FIG.
  • FIG. 7 is a cross-sectional view showing another embodiment of the main body according to the present invention.
  • FIG. 8 is a state diagram illustrating a state in which the main body of FIG. 3 is coupled
  • FIG. 9 is a state diagram illustrating a state in which the main body of FIG. 7 is coupled.
  • the present invention is to measure the hazardous substances of small products, such as children's products.
  • the zero gas supply part 20, the chamber part 30, the main body part 40, and the sample collection part 60 which are the components of this invention are smaller overall than the test apparatus for measuring the conventional hazardous substance. Is formed.
  • the zero gas supply unit 20 has a zero gas supply source 21 for generating zero gas as shown in FIGS. 2 to 3, and zeros for supplying zero gas generated by the zero gas supply source 21.
  • a gas supply pipe 23 is formed, and the zero gas supply pipe 23 includes a flow control valve 22 capable of adjusting a supply amount of zero gas.
  • the zero gas supply source 21 of the above-described zero gas supply unit 20 sucks air made of gas such as nitrogen and oxygen to remove trace chemicals contained in the air by using an adsorbent (not shown).
  • an adsorbent not shown
  • the zero gas supply unit 20 is configured to be connected to the control unit 10 so that the flow rate by the dehumidification, preheating and control of the flow control valve 22 of the zero gas moving to the zero gas supply pipe 23 can be adjusted. do.
  • the control unit 10 is provided with a plurality of control buttons 11 is configured to facilitate the above-described control of zero gas.
  • the chamber unit 30 is configured to receive zero gas from the zero gas supply pipe 23 of the zero gas supply unit 20.
  • the above-described chamber part 30 maintains a sealed shape that can accommodate the zero gas as a whole, but has a structure that can be connected to the zero gas supply pipe 23 of the zero gas supply part 20 on one side.
  • the body portion 40 is formed on the outside of the chamber portion 30, it is configured in a form surrounding the chamber portion (30).
  • the body portion 40 is configured such that the temperature control device 43 can maintain a constant temperature of the chamber portion 30.
  • the liner 50 is configured to include a product sample inserting portion 51 which is coupled to the inside of the chamber portion 30 to insert a product sample.
  • Such a liner 50 is coupled to the insertable and detachable form in the chamber unit 30 to receive the product sample directly.
  • the liner 50 should be maintained in a closed state because it should be configured to move the harmful substances included in the product sample through the zero gas passes through the product sample is seated.
  • the liner 50 has a product sample seat 52 formed inside the product sample insert 51 as shown in FIG. 4, and a liner body 53 having an open top is formed. It is composed of a liner cover 54 for closing the open portion of the liner body 53.
  • the product sample mounting portion 52 is configured to include a plurality of drilling holes (52a) so that zero gas can flow.
  • the liner 50 may be formed of various materials, but it is preferable that the liner 50 is made of glass of transparent material that can visually check the product sample therein without generating harmful substances.
  • the sample collection unit 60 receives the zero gas containing the harmful substances contained in the product sample of the liner 50, and the adsorption liquid is contained therein so as to measure the amount of the harmful substances in the product sample. It consists of either an absorption tube or an adsorption tube in which an adsorbent is accommodated.
  • the sample collection unit 60 is made of a structure connected to the liner 50 in the chamber portion 30 as shown in FIGS.
  • the main body 40 is separated to combine the liner 50, and the upper and lower main bodies 41 and 42 are formed, and the chamber part 30 and the sample formed on the main body 40 are provided.
  • the collecting unit 60 may be configured by separating the upper and lower chambers 31 and 32 and the upper and lower sample collecting units 61 and 62.
  • the liner 50 may be inserted into and detached from the inside of the chamber part 30 by separately separating the chamber part 30 and the sample collecting part 60 formed on the main body part 40 and the main body part 40. To be configured.
  • the upper body 41 of the control unit 10 and the upper body 41 of the main body portion 40 is formed with a sliding means S, such as a wedge shape or a linear bearing, so that the upper body 41 is a conventional power source (not shown in the drawing).
  • a sliding means S such as a wedge shape or a linear bearing
  • the upper body 41 is a conventional power source (not shown in the drawing).
  • the sealing member 70 may be further configured between the upper and lower sample collecting portions 61 and 62.
  • the sealing member 70 may be formed of a Teflon material having excellent sealing properties and no harmful substances. good.
  • sealing material 70 is illustrated in the form of a ring in the drawing, the present invention is not limited thereto, and the sealing material 70 may be formed in the upper and lower chambers 31 and 32 and the upper and lower sample collecting parts 61 and 62 in a compact manner. It may be in any form.
  • the chamber portion 30 formed in the main body portion 40 can be configured in an integral form or in the form of coupling by the coupling member (J) as shown in FIG.
  • the flow control valve 22 and the zero gas supply pipe 23 of the zero gas supply part 20 are exposed to the lower side of the main body part 40. It may be configured in the form, or not shown in the drawings, but may be further formed by forming a separate auxiliary body, alternatively, the chamber portion 30 is coupled to the body portion 40 and the coupling member (J) When the structure is made, the flow rate control valve 22 and the zero gas supply pipe 23 of the zero gas supply unit 20 may be inserted into the lower main body 42.
  • the first connecting pipe (L1) for coupling in a detachable, attachable form between the upper body 41 of the main body portion 40 and the upper sample collecting portion 61 of the sample collecting portion 60 The second connecting pipe further formed and detachable between the lower chamber 32 formed on the lower main body 42 of the main body part 40 and the zero gas supply pipe 23 of the zero gas supply part 20. (L2) can be formed.
  • Pollutant emission experiment chamber apparatus 100 of the product according to the present invention is a device for detecting the amount of harmful substances contained in a small product sample, such as children's goods.
  • the chamber part is formed in the main body 40 by receiving a product sample in the liner 50 in the present invention After being seated on the 30, the harmful substances of the product sample stored in the liner 50 are transferred to the sample collecting unit 60 in which the adsorption liquid is stored through the zero gas supplied from the zero gas supply unit 20. (50) It functions to detect the amount of harmful substances inside.
  • the zero gas supply unit 20 generates a zero gas of a form suitable for sending to the product sample through the control of the humidity, temperature and flow control valve 22 of the zero gas by the control button of the control unit 10 liner
  • the body portion 40 is a temperature control device 43 is configured to control the temperature of the chamber portion 30 formed in the body portion 40 is contained in the product sample
  • the product sample from which the whole or part of the children's article is collected is stored in the liner 50.
  • the liner cover on the liner body 53 A product sample can be stored in a sealed state by covering (54).
  • the product sample may be previously stored in the product sample seat 52 formed in the liner body 53 of the liner 50 as described above.
  • a plurality of perforation holes 52a are formed in the product sample seat 52 of the liner 50 having the above structure, and are supplied through the zero gas supply pipe 23 of the zero gas supply unit 20. Zero gas is to act to smoothly pass through the product sample.
  • the liner 50 containing the product sample as described above is seated on the chamber portion 30 formed in the main body portion 40.
  • the above-described main body portion 40 and the chamber portion 30 are composed of upper and lower main bodies 41 and 42 and upper and lower chambers 31 and 32, respectively.
  • the upper main body 41 of the main body 40 is operated to be formed in the upper main body 41.
  • the upper and lower chambers 31 and 32 act to maintain a tight state.
  • the sealing material 70 in the present invention is made of a Teflon material that can maintain a closed state without containing a hazardous substance, the efficiency of detecting the hazardous substance in the product sample because the sealing effect and additional harmful substances are not released. It will work to improve.
  • the first connecting pipe L1 is formed between the lower chamber 31 of the chamber part 30 that couples the liner 50 and the zero gas supply pipe of the zero gas supply part 20, and the chamber part (
  • a second connecting tube L2 is coupled between the upper chamber 32 of the 30 and the upper sample collecting unit 61 of the sample collecting unit 60 to partition the liner 50 from the chamber unit 30. It is configured to.
  • the harmful substances emitted from the product sample contained in the liner 50 are not exposed to the chamber part 30, the harmful substances emitted from the product sample do not affect the chamber part 30.
  • the existing liner 50 inserted into the chamber part 30 to detect the amount of the hazardous substance is again detected.
  • the first and second connecting pipes (L1, L2) and the new liner 60 containing the new product sample is coupled to the chamber portion 30, the continuous operation is possible.
  • the existing liner 50 and the first and second connection pipes L1 and L2 separated as described above are separately washed in the process of inspecting a new product sample, so that the liner 50 and the first, 2
  • the connectors L1 and L2 may be reused.
  • the present invention since the liner 50 for accommodating the product sample is separately configured to store the product sample, the present invention is harmful to the inside of the chamber part 30 formed in the main body part 40 and the main body part 30. By acting so that the material is not released, the washing operation of the body portion 40 and the chamber portion 30 is not required separately, so that continuous work may be performed.
  • the liner 50 and the first and second connecting pipes L1 and L2 are separated from each other.
  • the new liner 50 and the first and second connecting pipes L1 and L2 may be installed to perform continuous work.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

La présente invention concerne un appareil à chambre pour expériences de rejet de produits polluants, qui est utilisé pour prélever de petits échantillons de produits, par exemple des articles pour enfants. L'appareil à chambre pour expériences de rejet de produits polluants comporte une partie de chambre formée dans une partie de corps principal et un revêtement intérieur, capable de recevoir un échantillon de produits de manière remplaçable, disposé dans la partie de chambre de telle façon que des substances nocives contenues dans l'échantillon de produit puissent être mesurées après que l'échantillon de produit a été recueilli et reçu par le revêtement intérieur. Il est ainsi possible de réaliser une mesure précise sur un produit ou un échantillon de petite taille. De plus, comme le revêtement intérieur inséré dans la partie de chambre présente une forme qui permet son insertion et son retrait, le revêtement intérieur ainsi que des premier et deuxième conduits de raccordement sont formés de telle façon que la partie de corps principal et la partie de chambre formée dans la partie de corps principal ne soient pas exposées à la substance nocive.
PCT/KR2013/006181 2012-11-07 2013-07-11 Appareil à chambre pour expériences de rejet de produits polluants WO2014073767A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2014545842A JP5747135B2 (ja) 2012-11-07 2013-07-11 製品の汚染物質放出実験チャンバー装置

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020120125132A KR101270669B1 (ko) 2012-11-07 2012-11-07 제품의 오염물질 방출실험 챔버장치
KR10-2012-0125132 2012-11-07

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WO2014073767A1 true WO2014073767A1 (fr) 2014-05-15

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PCT/KR2013/006181 WO2014073767A1 (fr) 2012-11-07 2013-07-11 Appareil à chambre pour expériences de rejet de produits polluants

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JP (1) JP5747135B2 (fr)
KR (1) KR101270669B1 (fr)
WO (1) WO2014073767A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109870330A (zh) * 2019-03-11 2019-06-11 成都智胜欣业环保科技有限公司 一种油烟在线监测系统

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102645836B1 (ko) * 2021-11-12 2024-03-08 강창국 대기 시료 채취장치

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JP2002071534A (ja) * 2000-06-26 2002-03-08 Berger Instruments Inc 流体流からのサンプル採集方法と装置
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KR100764519B1 (ko) * 2006-03-03 2007-10-08 주식회사 에코프로 대형 챔버식 오염물질 방출자재 시험장치
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Publication number Priority date Publication date Assignee Title
JP2002071534A (ja) * 2000-06-26 2002-03-08 Berger Instruments Inc 流体流からのサンプル採集方法と装置
KR20040089318A (ko) * 2003-04-11 2004-10-21 학교법인 한양학원 오염물질을 측정하기 위한 오염물질 포집장치 및 방법
KR100764519B1 (ko) * 2006-03-03 2007-10-08 주식회사 에코프로 대형 챔버식 오염물질 방출자재 시험장치
KR20100057184A (ko) * 2008-11-21 2010-05-31 한국표준과학연구원 휘발성 유기물의 표준 방산량 측정을 위한 표준 확산용기 및 휘발성 유기물 방산량 측정능력 평가방법
KR101032758B1 (ko) * 2010-03-16 2011-05-06 이소영 유해가스 탈취 및 흡착성능 실험을 위한 다기능 가스실험장치

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109870330A (zh) * 2019-03-11 2019-06-11 成都智胜欣业环保科技有限公司 一种油烟在线监测系统

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JP2015503103A (ja) 2015-01-29
KR101270669B1 (ko) 2013-06-03
JP5747135B2 (ja) 2015-07-08

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