WO2014067662A3 - Verfahren zur tieftemperaturzerlegung von luft in einer luftzerlegungsanlage und luftzerlegungsanlage - Google Patents

Verfahren zur tieftemperaturzerlegung von luft in einer luftzerlegungsanlage und luftzerlegungsanlage Download PDF

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Publication number
WO2014067662A3
WO2014067662A3 PCT/EP2013/003289 EP2013003289W WO2014067662A3 WO 2014067662 A3 WO2014067662 A3 WO 2014067662A3 EP 2013003289 W EP2013003289 W EP 2013003289W WO 2014067662 A3 WO2014067662 A3 WO 2014067662A3
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WO
WIPO (PCT)
Prior art keywords
air
separation
column
enriched
pressure
Prior art date
Application number
PCT/EP2013/003289
Other languages
English (en)
French (fr)
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WO2014067662A2 (de
Inventor
Tobias Lautenschlager
Original Assignee
Linde Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Linde Aktiengesellschaft filed Critical Linde Aktiengesellschaft
Priority to BR112015009379A priority Critical patent/BR112015009379A2/pt
Priority to RU2015120813A priority patent/RU2641766C2/ru
Priority to ES13786170T priority patent/ES2834478T3/es
Priority to EP13786170.4A priority patent/EP2914913B1/de
Priority to AU2013339789A priority patent/AU2013339789B2/en
Publication of WO2014067662A2 publication Critical patent/WO2014067662A2/de
Publication of WO2014067662A3 publication Critical patent/WO2014067662A3/de

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/0446—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the heat generated by mixing two different phases
    • F25J3/04466—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the heat generated by mixing two different phases for producing oxygen as a mixing column overhead gas by mixing gaseous air feed and liquid oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F25J3/04303—Lachmann expansion, i.e. expanded into oxygen producing or low pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04309—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04375—Details relating to the work expansion, e.g. process parameter etc.
    • F25J3/04393—Details relating to the work expansion, e.g. process parameter etc. using multiple or multistage gas work expansion
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04866—Construction and layout of air fractionation equipments, e.g. valves, machines
    • F25J3/04872—Vertical layout of cold equipments within in the cold box, e.g. columns, heat exchangers etc.
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/08—Processes or apparatus using separation by rectification in a triple pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/40—Air or oxygen enriched air, i.e. generally less than 30mol% of O2
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/50—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being oxygen

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

Die Erfindung schlägt ein Verfahren zur Zerlegung von Luft (AIR), bei dem abgekühlte Luft (AIR) bei einem ersten Trenndruck in einer ersten Trennsäule (S1) zumindest in eine stickstoffangereicherte Kopffraktion und eine sauerstoffangereicherte Sumpffraktion getrennt wird, und bei dem weitere abgekühlte Luft (AIR) in einer Mischsäule (M) bei einem Mischsäulendruck durch direkten Wärmetausch gegen einen flüssigen sauerstoffreichen Strom, der zumindest teilweise aus der sauerstoffangereicherten Sumpffraktion aus der ersten Trennsäule (S1) gewonnen wird, zu einer Mischsäulensumpffraktion verflüssigt wird. Es ist erfindungsgemäß vorgesehen, dass weitere abgekühlte Luft (AIR) in einer zweiten Trennsäule (S2) bei einem zweiten Trenndruck ebenfalls zumindest in eine stickstoffangereicherte Kopffraktion und eine sauerstoffangereicherte Sumpffraktion getrennt wird, wobei die stickstoffangereicherte Kopffraktion der zweiten Trennsäule (S2) zumindest teilweise mit der Mischsäulensumpffraktion aus der Mischsäule (M) gekühlt wird. Hierzu wird die stickstoffangereicherte Kopffraktion der zweiten Trennsäule (S2) zumindest teilweise durch den Verflüssigungsraum eines als Kondensatorverdampfer ausgebildeten Kopfkondensators (E2) der zweiten Trennsäule (S2) geführt, dessen Verdampfungsraum bei einem Verdampfungsraumdruck betrieben wird, der zwischen dem Mischsäulendruck und einem dritten Trenndruck liegt, bei welchem der flüssige sauerstoffreiche Strom in einer dritten Trennsäule (S3) gewonnen wird, und in welchen zumindest ein Teil der Mischsäulensumpffraktion aus der Mischsäule (M) bei dem Verdampfungsraumdruck flüssig eingespeist wird. Eine entsprechende Luftzerlegungsanlage (10) ist ebenfalls Gegenstand der Erfindung.
PCT/EP2013/003289 2012-11-02 2013-10-31 Verfahren zur tieftemperaturzerlegung von luft in einer luftzerlegungsanlage und luftzerlegungsanlage WO2014067662A2 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
BR112015009379A BR112015009379A2 (pt) 2012-11-02 2013-10-31 processo para separação de baixa temperatura de ar em uma usina de separação de ar e usina de separação de ar
RU2015120813A RU2641766C2 (ru) 2012-11-02 2013-10-31 Способ низкотемпературного разделения воздуха в установке для разделения воздуха и установка для разделения воздуха
ES13786170T ES2834478T3 (es) 2012-11-02 2013-10-31 Método de separación criogénica de aire en una planta de separación de aire y planta de separación de aire
EP13786170.4A EP2914913B1 (de) 2012-11-02 2013-10-31 Verfahren zur tieftemperaturzerlegung von luft in einer luftzerlegungsanlage und luftzerlegungsanlage
AU2013339789A AU2013339789B2 (en) 2012-11-02 2013-10-31 Process for the low-temperature separation of air in an air separation plant and air separation plant

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102012021694.7A DE102012021694A1 (de) 2012-11-02 2012-11-02 Verfahren zur Tieftemperaturzerlegung von Luft in einer Luftzerlegungsanlage und Luftzerlegungsanlage
DE102012021694.7 2012-11-02
EP12008101.3 2012-12-04
EP12008101 2012-12-04

Publications (2)

Publication Number Publication Date
WO2014067662A2 WO2014067662A2 (de) 2014-05-08
WO2014067662A3 true WO2014067662A3 (de) 2015-04-16

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PCT/EP2013/003289 WO2014067662A2 (de) 2012-11-02 2013-10-31 Verfahren zur tieftemperaturzerlegung von luft in einer luftzerlegungsanlage und luftzerlegungsanlage

Country Status (5)

Country Link
EP (1) EP2914913B1 (de)
AU (1) AU2013339789B2 (de)
CL (1) CL2015001109A1 (de)
DE (1) DE102012021694A1 (de)
WO (1) WO2014067662A2 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102015015684A1 (de) 2015-12-03 2016-07-21 Linde Aktiengesellschaft Verfahren zur Tieftemperaturzerlegung von Luft und Luftzerlegungsanlage
CN108120226A (zh) * 2017-12-28 2018-06-05 乔治洛德方法研究和开发液化空气有限公司 通过低温精馏从空气中生产高纯氮和氧气的方法及设备
CN108036584A (zh) * 2017-12-28 2018-05-15 乔治洛德方法研究和开发液化空气有限公司 通过低温精馏从空气中生产高纯氮、氧气和液氧的方法及设备

Citations (6)

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Publication number Priority date Publication date Assignee Title
US4783208A (en) * 1986-11-24 1988-11-08 The Boc Group Plc Air separation
US4818262A (en) * 1985-07-15 1989-04-04 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Air distillation process and plant
EP0531182A1 (de) * 1991-08-07 1993-03-10 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Verfahren und Einrichtung zur Luftdestillation und die Verwendung bei der Zuführung von Gas in Stahlwerken
US5715706A (en) * 1993-04-30 1998-02-10 The Boc Group Plc Air separation
EP1139046B1 (de) * 2000-03-29 2004-04-21 Linde Aktiengesellschaft Verfahren und Vorrichtung zur Gewinnung Sauerstoffdruckprodukt durch Tieftemperaturzerlegung von Luft
DE102009023900A1 (de) * 2009-06-04 2010-12-09 Linde Aktiengesellschaft Dreisäulenverfahren und -vorrichtung zur Tieftemperaturzerlegung von Luft

Family Cites Families (11)

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IT961138B (it) 1971-02-01 1973-12-10 Air Liquide Impianto per comprimere un fluido mediante espansione di un altro fluido
US5454227A (en) 1994-08-17 1995-10-03 The Boc Group, Inc. Air separation method and apparatus
US5490391A (en) 1994-08-25 1996-02-13 The Boc Group, Inc. Method and apparatus for producing oxygen
DE19803437A1 (de) 1998-01-29 1999-03-18 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines Druckprodukts durch Tieftemperaturzerlegung von Luft
DE19951521A1 (de) 1999-10-26 2001-05-03 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines Druckprodukts durch Tieftemperaturzerlegung von Luft
DE10139727A1 (de) 2001-08-13 2003-02-27 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines Druckprodukts durch Tieftemperaturzerlegung von Luft
DE10209421A1 (de) 2002-03-05 2003-04-03 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines Druckprodukts durch Tieftemperaturzerlegung von Luft
DE10217093A1 (de) 2002-04-17 2003-01-23 Linde Ag Verfahren zur Regelung eines Trennsäulen-Systems zur Gaszerlegung
DE10228111A1 (de) 2002-06-24 2004-01-15 Linde Ag Luftzerlegungsverfahren und -anlage mit Mischsäule und Krypton-Xenon-Gewinnung
EP1387136A1 (de) 2002-08-02 2004-02-04 Linde AG Verfahren und Vorrichtung zur Erzeugung von unreinem Sauerstoff durch Tieftemperaturzerlegung von Luft
EP1666824A1 (de) 2004-12-03 2006-06-07 Linde Aktiengesellschaft Verfahren und Vorrichtung zur Gewinnung von Argon durch Tieftemperaturzerlegung von Luft

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4818262A (en) * 1985-07-15 1989-04-04 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Air distillation process and plant
US4783208A (en) * 1986-11-24 1988-11-08 The Boc Group Plc Air separation
EP0531182A1 (de) * 1991-08-07 1993-03-10 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Verfahren und Einrichtung zur Luftdestillation und die Verwendung bei der Zuführung von Gas in Stahlwerken
US5715706A (en) * 1993-04-30 1998-02-10 The Boc Group Plc Air separation
EP1139046B1 (de) * 2000-03-29 2004-04-21 Linde Aktiengesellschaft Verfahren und Vorrichtung zur Gewinnung Sauerstoffdruckprodukt durch Tieftemperaturzerlegung von Luft
DE102009023900A1 (de) * 2009-06-04 2010-12-09 Linde Aktiengesellschaft Dreisäulenverfahren und -vorrichtung zur Tieftemperaturzerlegung von Luft

Also Published As

Publication number Publication date
CL2015001109A1 (es) 2015-07-31
AU2013339789A1 (en) 2015-04-30
EP2914913A2 (de) 2015-09-09
AU2013339789B2 (en) 2017-11-30
DE102012021694A1 (de) 2014-05-08
EP2914913B1 (de) 2020-09-23
WO2014067662A2 (de) 2014-05-08

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