WO2012016565A2 - Procédé de préparation de nanoparticules d'un métal précieux et utilisation des nanoparticules ainsi produites - Google Patents

Procédé de préparation de nanoparticules d'un métal précieux et utilisation des nanoparticules ainsi produites Download PDF

Info

Publication number
WO2012016565A2
WO2012016565A2 PCT/DE2011/001551 DE2011001551W WO2012016565A2 WO 2012016565 A2 WO2012016565 A2 WO 2012016565A2 DE 2011001551 W DE2011001551 W DE 2011001551W WO 2012016565 A2 WO2012016565 A2 WO 2012016565A2
Authority
WO
WIPO (PCT)
Prior art keywords
nanoparticles
noble metal
silver
platinum
solution
Prior art date
Application number
PCT/DE2011/001551
Other languages
German (de)
English (en)
Other versions
WO2012016565A3 (fr
Inventor
Robert Jurk
Marco Fritsch
Original Assignee
Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. filed Critical Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V.
Priority to EP11776686.5A priority Critical patent/EP2600997A2/fr
Priority to JP2013522101A priority patent/JP2013540888A/ja
Priority to KR1020137002755A priority patent/KR20140026318A/ko
Priority to US13/813,566 priority patent/US20130205950A1/en
Publication of WO2012016565A2 publication Critical patent/WO2012016565A2/fr
Publication of WO2012016565A3 publication Critical patent/WO2012016565A3/fr

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/04—Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0545—Dispersions or suspensions of nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/32—Inkjet printing inks characterised by colouring agents
    • C09D11/322—Pigment inks
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/52—Electrically conductive inks
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C1/00—Making non-ferrous alloys
    • C22C1/04—Making non-ferrous alloys by powder metallurgy
    • C22C1/0466—Alloys based on noble metals
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C5/00—Alloys based on noble metals
    • C22C5/02—Alloys based on gold
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C5/00—Alloys based on noble metals
    • C22C5/04—Alloys based on a platinum group metal
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C5/00—Alloys based on noble metals
    • C22C5/06—Alloys based on silver
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy

Abstract

L'invention concerne un procédé de préparation de nanoparticules en un métal précieux ainsi que l'utilisation des nanoparticules produites par ce procédé. L'objectif de l'invention est de définir des possibilités pour une préparation simple et bon marché de nanoparticules en un métal précieux, lesquelles permettent d'influencer de manière ciblée la taille des nanoparticules ainsi produites. Le procédé selon l'invention permet la production de nanoparticules en argent, en or et en platine, la taille des particules étant réglable. Un composé chimique du métal précieux considéré est dissout dans une solution aqueuse ou le métal précieux est dissout dans un mélange d'acides. On ajoute à la solution une solution aqueuse contenant au moins un composé tensioactif et, pour l'argent et le platine, un réducteur. Pour influencer la taille des particules, on agit sur les paramètres : concentration du composé chimique ou du métal précieux, température, pH et proportion de tensioactif. Les particules de métal précieux précipitant dans la solution peuvent être séparées par centrifugation.
PCT/DE2011/001551 2010-08-03 2011-07-29 Procédé de préparation de nanoparticules d'un métal précieux et utilisation des nanoparticules ainsi produites WO2012016565A2 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP11776686.5A EP2600997A2 (fr) 2010-08-03 2011-07-29 Procédé de préparation de nanoparticules d'un métal précieux et utilisation des nanoparticules ainsi produites
JP2013522101A JP2013540888A (ja) 2010-08-03 2011-07-29 貴金属からナノ粒子を製造するための方法及び製造されたナノ粒子の使用
KR1020137002755A KR20140026318A (ko) 2010-08-03 2011-07-29 귀금속으로부터 나노 입자를 생성하기 위한 방법 및 이와 같이 생성된 나노 입자의 이용
US13/813,566 US20130205950A1 (en) 2010-08-03 2011-07-29 Method for producing nanoparticles from a noble metal and use of the nanoparticles thus produced

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102010033924.5 2010-08-03
DE102010033924A DE102010033924A1 (de) 2010-08-03 2010-08-03 Verfahren zur Herstellung von Nanopartikeln aus einem Edelmetall und die Verwendung der so hergestellten Nanopartikel

Publications (2)

Publication Number Publication Date
WO2012016565A2 true WO2012016565A2 (fr) 2012-02-09
WO2012016565A3 WO2012016565A3 (fr) 2013-03-28

Family

ID=44903022

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2011/001551 WO2012016565A2 (fr) 2010-08-03 2011-07-29 Procédé de préparation de nanoparticules d'un métal précieux et utilisation des nanoparticules ainsi produites

Country Status (6)

Country Link
US (1) US20130205950A1 (fr)
EP (1) EP2600997A2 (fr)
JP (1) JP2013540888A (fr)
KR (1) KR20140026318A (fr)
DE (1) DE102010033924A1 (fr)
WO (1) WO2012016565A2 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014120868A1 (fr) * 2013-02-04 2014-08-07 Eastman Kodak Company Composition de nanoparticules métalliques d'argent

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5733622B2 (ja) * 2011-05-31 2015-06-10 学校法人 関西大学 金属ナノ粒子含有蛍光体組成物の製造方法、並びにこの蛍光体組成物を用いた金属センサー及び蛍光フィルム
EP2610366A3 (fr) * 2011-12-31 2014-07-30 Rohm and Haas Electronic Materials LLC Catalyseur de placage et procédé
KR101535154B1 (ko) * 2014-02-13 2015-07-16 (주) 유천테크 금 나노입자 및 그의 제조 방법
CN104128616B (zh) 2014-08-12 2016-03-23 苏州思美特表面材料科技有限公司 一种金属粉末的制备方法
WO2019131435A1 (fr) * 2017-12-26 2019-07-04 コニカミノルタ株式会社 Procédé de production d'un liquide de dispersion de nanoparticules d'argent, liquide de dispersion de nanoparticules d'argent, encre pour jet d'encre et procédé de formation d'image utilisant celle-ci
ES2724358A1 (es) * 2018-03-02 2019-09-10 Torrecid Sa Procedimiento de obtencion de particulas submicrometricas para dispositivos electroluminiscentes
CN108962422B (zh) * 2018-08-30 2020-05-22 浙江纳沛新材料有限公司 一种用于ltcc陶瓷基板的导电银浆及其制备方法
CN111014721A (zh) * 2019-12-27 2020-04-17 海南医学院 一种铂纳米颗粒及其制备方法
CN112662231B (zh) * 2020-12-24 2022-12-02 华中科技大学 一种氨基酸修饰的金纳米墨水及其制备方法和应用
CN113290252A (zh) * 2021-05-28 2021-08-24 金川集团股份有限公司 一种低振实高比表超细银粉的制备方法
CN113579243B (zh) * 2021-06-01 2023-08-01 广东省科学院健康医学研究所 一种金银纳米花及其制备方法与应用
CN114570936B (zh) * 2022-03-02 2023-04-28 南通大学 一种谷胱甘肽硫转移酶-金铂纳米簇的制备方法及其在金霉素检测中的应用

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6090858A (en) * 1998-03-18 2000-07-18 Georgia Tech Reseach Corporation Shape control method for nanoparticles for making better and new catalysts
US6660058B1 (en) * 2000-08-22 2003-12-09 Nanopros, Inc. Preparation of silver and silver alloyed nanoparticles in surfactant solutions
KR100401335B1 (en) * 2003-03-08 2003-10-10 Mijitech Co Ltd Metal nanoparticle surface-coated with silicon oxides and preparation thereof
CN101124061B (zh) * 2004-06-30 2010-06-02 西北大学 具有预定厚度的金属纳米棱柱的制造方法
US7270694B2 (en) * 2004-10-05 2007-09-18 Xerox Corporation Stabilized silver nanoparticles and their use
US7824466B2 (en) * 2005-01-14 2010-11-02 Cabot Corporation Production of metal nanoparticles
FR2893263B1 (fr) * 2005-11-14 2013-05-03 Inst Francais Du Petrole Methode de synthese d'un catalyseur a base de nanoparticules metalliques anisotropes par voie micellaire.
MXNL06000107A (es) * 2006-12-20 2008-10-08 Ind Penoles Sa De Cv Proceso para la fabricacion de plata metalica nanometrica, monodispersa y estable y producto obtenido.
JP5203769B2 (ja) * 2008-03-31 2013-06-05 富士フイルム株式会社 銀ナノワイヤー及びその製造方法、並びに水性分散物及び透明導電体
US20100092372A1 (en) * 2008-05-21 2010-04-15 Northwestern University Halide ion control of seed mediated growth of anisotropic gold nanoparticles
DE102009015470A1 (de) * 2008-12-12 2010-06-17 Byk-Chemie Gmbh Verfahren zur Herstellung von Metallnanopartikeln und auf diese Weise erhaltene Metallnanopartikel und ihre Verwendung
CN102371356B (zh) * 2010-08-23 2014-12-24 清华大学 金纳米粒子的制备方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
YU-CHIEH LU U.A.: "A simple and effective route for the synthesis of nano-silver colloidal dispersions", JOURNAL OF THE CHINESE INSTITUTE OF CHEMICAL ENGINEERS, vol. 39, 2008, pages 673 - 678

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014120868A1 (fr) * 2013-02-04 2014-08-07 Eastman Kodak Company Composition de nanoparticules métalliques d'argent

Also Published As

Publication number Publication date
JP2013540888A (ja) 2013-11-07
KR20140026318A (ko) 2014-03-05
US20130205950A1 (en) 2013-08-15
EP2600997A2 (fr) 2013-06-12
DE102010033924A1 (de) 2012-02-09
WO2012016565A3 (fr) 2013-03-28

Similar Documents

Publication Publication Date Title
WO2012016565A2 (fr) Procédé de préparation de nanoparticules d'un métal précieux et utilisation des nanoparticules ainsi produites
EP2614904B1 (fr) Procédé de fabrication de poudre de cuivre pour pâte conductrice
EP2087490B1 (fr) Formulation aqueuse contenant de l'argent et son utilisation pour la préparation de revêtements électriquement conducteurs ou réfléchissants
JP4449676B2 (ja) 銅微粒子の製造方法
KR101533860B1 (ko) 구리 미립자와 그 제조 방법 및 구리 미립자 분산액
EP2010314A1 (fr) Procédé de fabrication de particules métalliques, les particules métalliques ainsi fabriquées et leur utilisation
JP2008513565A (ja) インクジェット印刷が可能な組成物
JP5176824B2 (ja) 銀被覆銅微粒子とその分散液及びその製造方法
DE60307753T2 (de) Verfahren zur Herstellung von Metallpulver durch thermische Zersetzung
EP2303492A1 (fr) Nanoparticules métalliques coeur-écorce, leurs procédés de production, et compositions d encre les contenant
JP2008527169A (ja) 金属ナノ粒子の水系分散物
DE112004001403T5 (de) Feinpartikuläres Silberpulver und Verfahren zu dessen Herstellung
US20090158890A1 (en) Process of making metal nanoparticles
DE112004001399T5 (de) Feinpartikuläres Silberpulver und Verfahren zu dessen Herstellung
US20080193667A1 (en) Ink Jet Printable Compositions
JP5424545B2 (ja) 銅微粒子及びその製造方法、並びに銅微粒子分散液
JP4853152B2 (ja) ニッケル被覆銅微粒子とその製造方法、それを用いた分散液とその製造方法、及びそれを用いたペースト
TW201341087A (zh) 銀微粒子及其製造法與含有該銀微粒子之導電性糊劑、導電性膜及電子裝置
JP2005330552A (ja) 銅微粒子とその製造方法及び銅微粒子分散液
JP2008179851A (ja) 銀粉の製造方法及び銀粉
EP0537502B1 (fr) Poudre de métal ou d'alliage métallique sous forme microcristalline, sphérique et dense ainsi que procédé et installation pour sa préparation
AT508253B1 (de) Inkjet-tinte
JP2021501267A (ja) 銀粉末の製造方法及び銀粉末を含む導電性ペースト

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 2011776686

Country of ref document: EP

ENP Entry into the national phase

Ref document number: 2013522101

Country of ref document: JP

Kind code of ref document: A

ENP Entry into the national phase

Ref document number: 20137002755

Country of ref document: KR

Kind code of ref document: A

WWE Wipo information: entry into national phase

Ref document number: 13813566

Country of ref document: US