WO2011062449A2 - 무기 분말을 함유하는 화장료 조성물 - Google Patents
무기 분말을 함유하는 화장료 조성물 Download PDFInfo
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- WO2011062449A2 WO2011062449A2 PCT/KR2010/008215 KR2010008215W WO2011062449A2 WO 2011062449 A2 WO2011062449 A2 WO 2011062449A2 KR 2010008215 W KR2010008215 W KR 2010008215W WO 2011062449 A2 WO2011062449 A2 WO 2011062449A2
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- powder
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- cosmetic composition
- oxide
- boron nitride
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
Definitions
- the present invention relates to a cosmetic composition containing an inorganic powder capable of simultaneously blocking ultraviolet rays A, B and near infrared rays which adversely affect the skin.
- UV A 320-400 nm
- UV B 280-320 nm
- Infrared rays account for 80% of sunlight, and they are less reflected or scattered by particulates in the atmosphere than ultraviolet rays or visible rays, and air is not disturbed by molecules such as oxygen and nitrogen in the atmosphere. Penetrates the middle and reaches the ground. Infrared skin hazards known to promote blood circulation to the body and have a warming effect, such as skin wrinkles, have been discovered in recent years.
- infrared rays When infrared rays are classified according to the length of the wavelength, infrared rays with a wavelength of 780 to 3000 nm are called near-infrared rays (Near-IR), wavelengths of 3000 to 25000 nm are called infrared rays, and those having a wavelength greater than 25000 nm are called far-IR. Since the production mechanism is different from the known mechanism of skin wrinkles caused by ultraviolet rays, skin aging may be accelerated even when the existing sunscreen is applied to the skin when exposed to sunlight containing both ultraviolet and near infrared rays. There is a possibility.
- Near-IR near-infrared rays
- An object according to an embodiment of the present invention is to provide a cosmetic composition capable of simultaneously blocking ultraviolet rays A, B and near infrared rays when applied to the skin.
- One embodiment according to the present invention for achieving the above object is (i) boron nitride; And (ii) at least one inorganic powder selected from the group consisting of cerium oxide, titanium oxide, talc, aluminum oxide, iron oxide, zinc oxide and mica.
- the cosmetic composition of the present invention by simultaneously blocking the ultraviolet rays A, B and near infrared rays, it is possible to prevent the generation of wrinkles on the skin, thereby preventing the acceleration of skin aging derived from ultraviolet rays A, B and near infrared rays have.
- 1 is a graph showing the FT-IR spectrum of the cosmetic composition prepared according to an embodiment of the present invention.
- UV A having a wavelength of 320 ⁇ 400nm
- UV B and 770 ⁇ having a wavelength of 280 ⁇ 320nm It was confirmed that 1140 nm near infrared rays can be blocked at the same time.
- the cosmetic composition according to the present invention can effectively block not only ultraviolet rays but also near-infrared rays causing wrinkle formation from the skin, it is possible to prevent the formation of skin wrinkles by the near-infrared rays of such a path, thereby preventing skin aging. .
- composition according to an embodiment of the present invention may include at least one powder selected from the group consisting of cerium oxide, titanium oxide, talc, aluminum oxide, iron oxide, zinc oxide and mica together with the boron nitride powder.
- the composition according to an embodiment of the present invention is boron nitride powder and cerium oxide, titanium oxide, talc, aluminum oxide, iron oxide, zinc oxide and mica selected from the group consisting of 1, 2, 3, 4, 5, 6 or In combination with seven components, it can block near-infrared and ultraviolet rays simultaneously.
- the inventors of the present application specifically describe (i) boron nitride powders; And (ii) a cerium oxide powder; the cosmetic composition may have excellent ultraviolet (UV-A, B) and near-infrared (Near-IR) blocking effects as demonstrated by the following test examples. It was confirmed that there is.
- UV-A, B ultraviolet
- Near-IR near-infrared
- the boron nitride powder may have an average particle size of 1 to 10 ⁇ m, preferably 4 to 6 ⁇ m.
- the boron nitride powder having such an average particle size may have excellent infrared blocking efficacy.
- the boron nitride powder may be included in 0.1 to 30% by weight based on the total weight of the composition, preferably 5 to 30% by weight. If the amount of the boron nitride powder is too small, the infrared ray blocking effect may be inadequate, too much may cause problems in product safety.
- the cerium oxide powder may have an average particle size of, for example, 0.1 to 40 ⁇ m, preferably 1 to 30 ⁇ m, and more preferably 5 to 15 ⁇ m.
- the cerium oxide powder having such an average particle size is excellent in ultraviolet A and near infrared ray blocking effects.
- the cerium oxide powder may be included in 0.1 to 30% by weight based on the total weight of the composition, it may be included in 3 to 30% by weight preferably within the above range. If the amount of the cerium oxide powder is too small, ultraviolet A and near infrared ray blocking effect may be insufficient, if too large, there is a problem that the composition is not smooth.
- the composition comprises (i) boron nitride powder; And (ii) titanium oxide (titanium oxide) powder; may contain.
- the titanium oxide powder may have an average particle size of, for example, 1 to 50 nm, and preferably 10 to 30 nm. Titanium oxide having such an average particle size is excellent in ultraviolet B and near infrared ray blocking effect.
- the titanium oxide powder may be included in 3 to 30% by weight based on the total weight of the composition, preferably 5 to 25% by weight. If the amount of the titanium oxide powder is less than 5% by weight may be insufficient ultraviolet B and near-infrared ray blocking effect, when the amount of more than 25% by weight according to Regulation Annex 4 for the review of functional cosmetics notification No. 2008-58, 59 This may cause problems with product safety.
- the composition comprises (i) boron nitride powder; And (ii) talc powder.
- the talc powder may have an average particle size of, for example, 0.1 to 40 ⁇ m, preferably 5 to 25 ⁇ m, and more preferably 8 to 15 ⁇ m. Talc powder having such an average particle size may have excellent infrared blocking efficacy.
- the talc powder may be included in 0.1 to 10% by weight, preferably 3 to 10% by weight based on the total weight of the composition. If the amount of the talc powder is too small, the infrared ray blocking effect may be inadequate, too much may cause problems in product safety.
- the composition comprises (i) boron nitride powder; And (ii) mica powder.
- the mica powder may have an average particle size of, for example, 0.1 to 40 ⁇ m, preferably 5 to 40 ⁇ m, and more preferably 7 to 25 ⁇ m. Mica powder having such an average particle size may have excellent infrared blocking efficacy.
- the mica powder may be included in 0.1 to 10% by weight based on the total weight of the composition, preferably from 2 to 8% by weight. If the amount of the mica powder is too small, the infrared ray blocking effect may be inadequate, too much may cause problems in product safety.
- the composition comprises (i) Boron nitride powder; And (ii) aluminum oxide (Aluminum oxide) powder; may contain.
- the aluminum oxide powder may have an average particle size of, for example, 0.1 to 40 ⁇ m, preferably 5 to 15 ⁇ m, and more preferably 5 to 10 ⁇ m. Aluminum oxide powder having such an average particle size may have excellent infrared blocking efficacy.
- the aluminum oxide powder may be included in 3 to 15% by weight, preferably 2 to 8% by weight based on the total weight of the composition. If the amount of the aluminum oxide powder is too small, the infrared ray blocking effect may be insufficient, too much may cause a problem in product safety.
- the composition comprises (i) boron nitride powder; And (ii) zinc oxide (Zinc Oxide) powder; may contain.
- the zinc oxide powder may have an average particle size of, for example, 0.1 to 40 ⁇ m, preferably 0.3 to 5 ⁇ m, and more preferably 0.3 to 1.5 ⁇ m. Zinc oxide powder having such an average particle size may have excellent infrared blocking efficacy.
- the zinc oxide powder may be included in 1 to 20% by weight based on the total weight of the composition, preferably 1 to 15% by weight. If the amount of the zinc oxide powder is too small, the infrared ray blocking effect may be inadequate, too much may cause problems in product safety.
- the composition comprises (i) boron nitride powder; And (ii) iron oxide powder.
- the iron oxide powder may have an average particle size of, for example, 0.1 to 40 ⁇ m, preferably 0.1 to 10 ⁇ m, and more preferably 0.2 to 7 ⁇ m. Iron oxide powder having such an average particle size may have excellent infrared blocking efficacy.
- the iron oxide powder may be included in an amount of 0.001 to 5% by weight, preferably 0.001 to 2% by weight based on the total weight of the composition. If the amount of the iron oxide powder is too small, the infrared ray blocking effect may be inadequate, too much may cause problems in product safety.
- the cosmetic composition according to the present invention may be formulated without particular limitation, and may be formulated, for example, as a softener, nutrient cream, nourishing cream, massage cream, pack, sun cream, foundation or makeup base.
- a softener nutrient cream
- nourishing cream nourishing cream
- massage cream pack, sun cream, foundation or makeup base.
- other ingredients can be appropriately selected and blended by those skilled in the art according to the purpose of use.
- the water-in-oil makeup cosmetic composition of Comparative Examples and Examples 1 to 7 was prepared using the composition shown in Table 1 below.
- the manufacturing method is as follows.
- FIG. 1 is a graph showing the results of measuring near-infrared blocking ability through a Fourier transform near-infrared spectrometer (MB100, ABB).
- Near-infrared rays are wavelengths in the range of 770-1400 nm, and the lower the wavelength, the better the near-IR blocking ability.
- Example 3 boron nitride and titanium oxide (Example 3), boron nitride and cerium oxide (Example 4), boron nitride and talc (Example 6) best block and avoid light in the near infrared wavelength range. You can see that.
- UV blocking index measurement results of the compositions are shown in Table 2 below.
- Sun Protection Factor (SPF) and Protection of UVA (PFA) were measured using a SPF Analyzer (Optometrics USA, SPF290S).
- Sun Protection Factor (SPF) is an index indicating the protection effect of ultraviolet light B
- Protection of UVA (PFA) is an index indicating the blocking effect of ultraviolet light A.
- the cosmetic composition according to the present invention exhibits a higher SPF value and PFA value than the comparative example, in particular, boron nitride and oxidation Titanium (Example 3), boron nitride and cerium oxide (Example 4), boron nitride and talc (Example 6) had the highest SPF values, and boron nitride and zinc oxide (Example 2) had the highest PFA values. Confirmed high.
- Softening water was prepared according to a conventional method as shown in the table below.
- Nourishing cream was prepared according to a conventional method as shown in the table below.
Abstract
Description
성분 | 원료명 | 비교예 | 실시예 1 | 실시예 2 | 실시예 3 | 실시예 4 | 실시예 5 | 실시예 6 | 실시예 7 |
유상성분 | 데카메칠사이클로펜타실록산 | 15.00 | 15.00 | 15.00 | 15.00 | 15.00 | 15.00 | 15.00 | 15.00 |
디카프릴릴카보네이트 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | |
에칠헥실메톡시신나메이트 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | 10.00 | |
세틸 디메치콘 코폴리올(계면활성제) | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | |
다이스테아르모니움헥토라이트 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | |
파라옥시안식향산에스테르 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | |
착색제 | 질화붕소(Boron nitrite) | - | 5.00 | 5.00 | 5.00 | 5.00 | 5.00 | 5.00 | 5.00 |
산화알루미늄(Aluminum oxide) | - | 5.00 | - | - | - | - | - | - | |
산화아연(Zinc Oxide) | - | - | 5.00 | - | - | - | - | - | |
산화티탄(Titanium oxide) | - | - | 5.00 | - | |||||
산화세륨(Cerium oxide) | - | - | - | - | 5.00 | - | - | - | |
산화철(iron oxide) | - | - | - | - | - | 5.00 | - | - | |
탈크(talc) | - | - | - | - | - | 5.00 | - | ||
마이카(mica) | - | - | - | - | - | - | 5.00 | ||
수상성분 | 정제수 | To 100 | To 100 | To 100 | To 100 | To 100 | To 100 | To 100 | To 100 |
디소듐이디티에이 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | |
소듐클로라이드 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | |
페녹시에탄올 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 |
구분 | 시험관내(In-vitro) SPF | 시험관내(In-vitro) PFA |
비교예 | 10.1 | 2.1 |
실시예 1 | 11.2 | 2.2 |
실시예 2 | 13.0 | 3.7 |
실시예 3 | 16.8 | 2.6 |
실시예 4 | 16.6 | 3.0 |
실시예 5 | 11.7 | 2.9 |
실시예 6 | 13.6 | 2.7 |
실시예 7 | 11.4 | 2.6 |
배합성분 | 함량 |
정제수 | 잔량 |
실시예 3 | 5.0 |
에틸렌디아민테트라아세트산 | 0.02 |
글리세린 | 5 |
부틸렌글리콜 | 3 |
피이지/피피지-17/6코폴리머 | 3 |
에탄올 | 5 |
폴리옥시에틸렌하이드로제네이티드피마자유 | 0.4 |
메틸파라벤 | 0.1 |
방향제(fragrance) | 0.1 |
방부제, 색소, 향료 | 적량 |
배합성분 | 함량 |
정제수 | 잔량 |
실시예 4 | 5.0 |
밀납 | 4.0 |
폴리솔베이트60 | 1.5 |
솔비탄세스퀴올레이트 | 1.5 |
유동파라핀 | 0.5 |
카프릴릭/카프릭트리글리세라이드 | 5.0 |
글리세린 | 3.0 |
부틸렌글리콜 | 3.0 |
프로필렌글리콜 | 3.0 |
카르복시비닐폴리머 | 0.1 |
트리에탄올아민 | 0.2 |
방부제, 색소, 향료 | 적량 |
배합성분 | 함량 |
정제수 | 잔량 |
실시예 3 | 5.0 |
밀납 | 10.0 |
폴리솔베이트60 | 1.5 |
PEG60 경화피마자유 | 2.0 |
솔비탄세스퀴올레이트 | 0.5 |
유동파라핀 | 10.0 |
스쿠알란 | 5.0 |
카프릴릭/카프릭트리글리세라이드 | 5.0 |
글리세린 | 5.0 |
푸틸렌글리콜 | 3.0 |
프로필렌글리콜 | 3.0 |
트리에탄올아민 | 0.2 |
방부제, 색소, 향료 | 적량 |
배합성분 | 함량 |
정제수 | 잔량 |
실시예 4 | 5.0 |
밀납 | 10.0 |
폴리솔베이트60 | 1.5 |
PEG60 경화피마자유 | 2.0 |
솔비탄세스퀴올레이트 | 0.8 |
유동파라핀 | 40.0 |
스쿠알란 | 5.0 |
카프릴릭/카프릭트리글리세라이드 | 4.0 |
글리세린 | 5.0 |
부틸렌글리콜 | 3.0 |
프로필렌글리콜 | 3.0 |
트리에탄올아민 | 0.2 |
방부제, 색소, 향료 | 적량 |
배합성분 | 함량 |
정제수 | 잔량 |
실시예 3 | 5.0 |
폴리비닐알콜 | 13.0 |
소듐카르복시메틸셀룰로오스 | 0.2 |
글리세린 | 5.0 |
알란토인 | 0.1 |
에탄올 | 6.0 |
PEG-12 노닐페닐에테르 | 0.3 |
폴리솔베이트 60 | 0.3 |
방부제, 색소, 향료 | 적량 |
Claims (13)
- (i) 질화붕소 분말; 및(ii) 산화세륨, 산화티탄, 탈크, 산화알루미늄, 산화철, 산화아연 및 마이카로 이루어진 군에서 선택된 하나 이상의 분말;을 함유하는 화장료 조성물.
- 제 1 항에 있어서,상기 질화붕소 분말은 평균 입자 크기가 1 내지 10㎛인 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 질화붕소 분말은 조성물의 총 중량을 기준으로 0.1 내지 30중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화세륨, 탈크, 산화알루미늄, 산화철, 산화아연 및 마이카로 이루어진 군에서 선택된 하나 이상의 분말의 평균 입자 크기는 0.1 내지 40㎛인 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화티탄 분말의 평균 입자 크기는 1 내지 50nm인 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화세륨 분말은 조성물의 총 중량을 기준으로 0.1 내지 30중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화티탄 분말은 조성물의 총 중량을 기준으로 5 내지 25중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 탈크 분말은 조성물의 총 중량을 기준으로 0.1 내지 10중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화알루미늄 분말은 조성물의 총 중량을 기준으로 3 내지 15중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화철 분말은 조성물의 총 중량을 기준으로 0.001 내지 5중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 산화아연 분말은 조성물의 총 중량을 기준으로 1 내지 20중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 마이카 분말은 조성물의 총 중량을 기준으로 0.1 내지 10중량%로 포함되는 것을 특징으로 하는 화장료 조성물.
- 제 1 항에 있어서,상기 화장료 조성물은 자외선 및 근적외선을 동시에 차단하는 것을 특징으로 하는 화장료 조성물.
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201080056639.1A CN102753136B (zh) | 2009-11-20 | 2010-11-19 | 包含无机粉末的化妆组合物 |
US13/510,747 US20120231058A1 (en) | 2009-11-20 | 2010-11-19 | Cosmetic Composition Containing Inorganic Powder |
JP2012539817A JP2013511515A (ja) | 2009-11-20 | 2010-11-19 | 無機粉末を含有する化粧料組成物 |
US14/454,690 US9480632B2 (en) | 2009-11-20 | 2014-08-07 | Cosmetic composition containing inorganic powder |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
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KR20090112396 | 2009-11-20 | ||
KR10-2009-0112396 | 2009-11-20 | ||
KR20100115782A KR101061289B1 (ko) | 2009-11-20 | 2010-11-19 | 무기 분말을 함유하는 화장료 조성물 |
KR10-2010-0115782 | 2010-11-19 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
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US13/510,747 A-371-Of-International US20120231058A1 (en) | 2009-11-20 | 2010-11-19 | Cosmetic Composition Containing Inorganic Powder |
US14/454,690 Division US9480632B2 (en) | 2009-11-20 | 2014-08-07 | Cosmetic composition containing inorganic powder |
Publications (2)
Publication Number | Publication Date |
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WO2011062449A2 true WO2011062449A2 (ko) | 2011-05-26 |
WO2011062449A3 WO2011062449A3 (ko) | 2011-11-10 |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2000086210A (ja) * | 1998-07-09 | 2000-03-28 | Kinya Adachi | 窒化ホウ素・酸化物複合粒子とその製造方法、及びそれを用いた紫外線遮断剤 |
US20050053571A1 (en) * | 2003-09-10 | 2005-03-10 | Dainichiseika Color & Chemicals Mfg. Co., Ltd. | Cosmetic composition |
US20070269454A1 (en) * | 2003-06-26 | 2007-11-22 | Mitsuru Maeda | Composition for External Use |
WO2009017104A1 (ja) * | 2007-07-30 | 2009-02-05 | Yohei Tanaka | 生体組織の近赤外線損傷の防止剤及びそれを用いた製品 |
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- 2010-11-19 WO PCT/KR2010/008215 patent/WO2011062449A2/ko active Application Filing
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000086210A (ja) * | 1998-07-09 | 2000-03-28 | Kinya Adachi | 窒化ホウ素・酸化物複合粒子とその製造方法、及びそれを用いた紫外線遮断剤 |
US20070269454A1 (en) * | 2003-06-26 | 2007-11-22 | Mitsuru Maeda | Composition for External Use |
US20050053571A1 (en) * | 2003-09-10 | 2005-03-10 | Dainichiseika Color & Chemicals Mfg. Co., Ltd. | Cosmetic composition |
WO2009017104A1 (ja) * | 2007-07-30 | 2009-02-05 | Yohei Tanaka | 生体組織の近赤外線損傷の防止剤及びそれを用いた製品 |
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