WO2010082447A1 - Slurry regenerating device and method - Google Patents
Slurry regenerating device and method Download PDFInfo
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- WO2010082447A1 WO2010082447A1 PCT/JP2009/071792 JP2009071792W WO2010082447A1 WO 2010082447 A1 WO2010082447 A1 WO 2010082447A1 JP 2009071792 W JP2009071792 W JP 2009071792W WO 2010082447 A1 WO2010082447 A1 WO 2010082447A1
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic System or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/30—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
- H01L21/302—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26 to change their surface-physical characteristics or shape, e.g. etching, polishing, cutting
- H01L21/304—Mechanical treatment, e.g. grinding, polishing, cutting
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B57/00—Devices for feeding, applying, grading or recovering grinding, polishing or lapping agents
- B24B57/02—Devices for feeding, applying, grading or recovering grinding, polishing or lapping agents for feeding of fluid, sprayed, pulverised, or liquefied grinding, polishing or lapping agents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B27/00—Other grinding machines or devices
- B24B27/06—Grinders for cutting-off
- B24B27/0633—Grinders for cutting-off using a cutting wire
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28D—WORKING STONE OR STONE-LIKE MATERIALS
- B28D5/00—Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
- B28D5/0058—Accessories specially adapted for use with machines for fine working of gems, jewels, crystals, e.g. of semiconductor material
- B28D5/007—Use, recovery or regeneration of abrasive mediums
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
Definitions
- the present invention relates to a slurry regenerating apparatus and method, and more particularly to a waste slurry regenerating apparatus and method after cutting in a wire saw apparatus.
- waste slurry discharged from a processing apparatus using slurry has been recycled for cost reduction.
- the waste slurry in such a wire saw device is formed of a dispersion medium, abrasive grains and cutting waste mixed therein.
- two centrifuges were used to separate the abrasive grains and the cutting waste from the dispersion medium. Specifically, waste slurry is charged into the first centrifuge, and abrasive grains having a specific gravity greater than that of cutting waste are first separated with a low centrifugal force of less than 1500G.
- a mixed liquid composed of the dispersion medium and the cutting waste is put into a second centrifuge, and the cutting waste is separated with a high centrifugal force of 1500 G or more. Thereafter, the dispersion medium and abrasive grains were mixed to regenerate the slurry.
- the use of two centrifuges requires a large installation space, and it is difficult to secure the space.
- waste slurry or mixed solution it is preferable to supply the waste slurry or mixed solution to be introduced into the centrifuge at a constant flow rate. For this reason, waste slurry or a mixed liquid has been thrown into the centrifuge through the orifice pot (see, for example, Patent Document 1).
- the orifice pot adjusts the flow rate by replacing the orifice plate.
- it is necessary to select an optimum orifice plate depending on the properties of the slurry temperature, viscosity, specific gravity, abrasive grain type, coolant type, etc.
- the present invention takes the above-mentioned conventional technology into consideration, and does not require a large installation space, so that the primary separator and the secondary separator can be reliably separated from the waste slurry with only one centrifuge, and the separation is performed. It is an object of the present invention to provide a slurry regenerating apparatus and method capable of mixing a dispersed medium and a primary separated product to generate a slurry again.
- a waste slurry containing at least one of a primary separator and a secondary separator having different specific gravity to be separated from the dispersion medium is introduced into the dispersion medium, A centrifuge capable of separating the primary separated product or the secondary separated product from a waste slurry, and the centrifugal separator provided in the centrifugal separator, and discharging the primary separated product or the secondary separated product from the centrifugal separator.
- a fourth recovery tank for recovering the liquid a preparation tank for mixing the primary separated product and the dispersion medium to generate a regenerated slurry, and the first path and the discharge port.
- a slurry regenerating apparatus comprising switching means for connecting any one of the second paths.
- variable control quantitative supply means for adjusting the flow rate of the waste slurry or the mixed liquid
- mass flow meter provided between the variable control quantitative supply means and the centrifuge, and measurement of the mass flow meter
- a PID control unit is further provided for controlling the operation of the variable control type quantitative supply means so as to make the flow rate of the waste slurry or the mixed liquid constant based on the result.
- the storage tank, the fourth recovery tank, and the centrifuge are connected via a three-way valve, and the variable control type quantitative supply means and The mass flow meter is arranged between the three-way valve and the centrifuge.
- the waste slurry is a slurry used in a wire saw device that presses a workpiece against a wire and cuts the wire
- the primary separated is the Abrasive grains mixed in the slurry, wherein the secondary separation is a cutting waste of the workpiece.
- the invention of claim 5 is a slurry regeneration method using the slurry regeneration device according to any one of claims 1 to 4, wherein the waste slurry is introduced into the centrifuge, and the centrifuge is Driving with a predetermined centrifugal force (low G), the primary separated product is centrifuged from the waste slurry, the centrifuged primary separated product is collected in the first collection tank, and the mixed solution is collected in the first collection tank. 4 is collected in the collection tank, the mixed solution is charged into the centrifuge from the fourth collection tank, and the centrifuge is driven with a centrifugal force (high G) higher than the predetermined centrifugal force.
- the centrifuge is Driving with a predetermined centrifugal force (low G)
- the primary separated product is centrifuged from the waste slurry
- the centrifuged primary separated product is collected in the first collection tank
- the mixed solution is collected in the first collection tank. 4 is collected in the collection tank
- the mixed solution is charged into the centrifuge from the fourth
- the secondary separation is centrifuged from the mixed solution, the centrifuged secondary separation is collected in the second collection tank, the dispersion medium is collected in the third collection tank, and the mixture tank is collected.
- the primary separation recovered in the first recovery tank and the recovery in the third recovery tank Wherein a dispersion medium which is a new primary isolates and a new dispersion medium were placed, to provide a slurry reproducing method characterized by generating a regenerated slurry.
- the actual flow rate value of the waste slurry or the mixed liquid is measured by the mass flow meter, and the actual flow rate value and the set flow rate value are compared by the PID control unit.
- the variable control type quantitative supply means is PID-controlled so that the actual flow rate value becomes the set flow rate value.
- the supply of the waste slurry or the mixed solution to be introduced into the centrifuge can be made pulsation-free and quantitative by PID control of the variable control type quantitative supply means and the mass flow meter. For this reason, it is not necessary to adjust the flow rate by human hands, the flow rate can be automatically stabilized, and workability is improved. In addition, in order to perform stable recovery with a centrifuge, it is important to supply the solution in a pulsating and quantitative manner.
- the storage tank for storing the waste slurry, the fourth recovery tank for recovering the mixed liquid, and the centrifuge are connected via the three-way valve. And a pipe through which the mixed solution is introduced into the centrifuge. Therefore, since the pump and the flow rate control can be used in common, the number of parts can be reduced and the cost is also efficient.
- the reusable abrasive grain contained in the waste slurry used with the wire saw apparatus is collect
- a primary separator is isolate
- the variable control type quantitative supply means is PID controlled so that the actual flow rate value of the waste slurry or the mixed solution is fed back and approaches the set flow rate value.
- the centrifuge can be charged at a flow rate.
- a stable centrifugal effect can be obtained by supplying the solution without pulsation and quantification.
- FIG. 1 is a schematic view of a slurry regenerator according to the present invention.
- the slurry regenerating apparatus 1 includes a centrifuge 2, a first recovery tank 3 for recovering abrasive grains (primary separation), and cutting waste (secondary separation).
- Second recovery tank 4 for recovery
- third recovery tank 5 for recovering the dispersion medium
- fourth recovery tank 6 for recovering the mixed liquid
- a tank 7, a branch chute 8, and switching means 9 are provided.
- the centrifuge 2 includes two motors (first motor 10 and second motor 11), respectively, and can generate centrifugal force different from low G or high G.
- the waste slurry that is the separation target consists of abrasive grains, cutting waste (sludge), and a dispersion medium (oil).
- Cutting chips are generated when a brittle material (not shown) is cut by a wire saw device (not shown) in a manufacturing process of a wafer ring made of a brittle material (for example, silicon).
- the waste slurry used in the wire saw device is stored in the storage tank 16.
- abrasive grains have a higher specific gravity than cutting waste. Accordingly, when the waste slurry is centrifuged with a small centrifugal force, abrasive grains having a large specific gravity are mainly separated. Thereafter, when the centrifugal separation is performed with a large centrifugal force, the cutting waste is mainly separated. Thereby, the abrasive grains and cutting waste having different specific gravities can be separated into two stages and separated by one centrifuge 2.
- a discharge port 12 is provided on the lower side of the centrifuge 2.
- the discharge port 12 drops and discharges the centrifuged abrasive grains or cutting waste.
- the outlet side of the branch chute 8 is connected to the discharge port 12.
- the exit side of the branch chute 8 is branched in the middle into a first path 8a through which abrasive grains (primary separation) are transferred and a second path 8b through which cutting waste (secondary separation) is transferred. .
- the opening position of the inlet side of the branch chute 8 with respect to the discharge port 12 is changed. By changing this position, the abrasive grains can be passed through the first path 8a and the cutting waste can be passed through the second path 8b.
- the first collection tank 3 for collecting abrasive grains is connected to the first path 8a.
- the second recovery tank 4 for recovering cutting waste is connected to the second path 8b. Therefore, the abrasive grains or cutting waste discharged from the discharge port 12 are collected in the first collection tank 3 or the second collection tank 4 through the first path 8a or the second path 8b, respectively.
- the third recovery tank 5 for recovering the dispersion medium and the fourth recovery tank 6 for recovering the mixed liquid are connected to the drainage port 13 of the centrifuge 2 via the three-way valve 14.
- the three-way valve 14 is an automatic switching valve (the following three-way valves 19, 22, 23, 26, 29, 30, 32, and 37 are all the same).
- the drainage port 13 is provided on the lower side of the centrifuge 2. When centrifuging the abrasive grains in the primary separation, the mixed liquid composed of the cutting waste and the dispersion medium is collected from the drainage port 13 through the three-way valve 14 into the fourth collection tank 6. The mixed liquid is put into the centrifuge 2 again for secondary separation, and the cutting waste is centrifuged.
- the dispersion medium is recovered from the drain port 13 through the three-way valve 14 to the third recovery tank 5.
- the pump 36 is driven, and the oil in the third recovery tank 5 is supplied to the three-way valve 19, the branch pipe 21, the three-way valve 22, the pump 36, the three-way valve 37, The branch pipe 38 and the valve 41 are passed in this order to return to the fourth recovery tank 6 and secondary separation is performed again.
- the pump 51 is operated to transfer the mixed solution to the mixed solution disposal tank 52.
- the blending tank 7 for blending the regenerated slurry is connected to the first collection tank 3 and the third collection tank 5.
- a new dispersion medium is accommodated in the first recovery tank 3 in advance.
- the abrasive grains recovered in the first recovery tank 3 are sent to the preparation tank 7 together with a new dispersion medium via the pump 15.
- the new abrasive grains S are sent to the mixing tank 7 not only from such regenerated abrasive grains but also from a new abrasive grain storage tank (not shown).
- the dispersion medium When the dispersion medium is sent from the third collection tank 5 to the preparation tank 7, it passes through the following flow path.
- the pump 20 When the pump 20 is driven, the three-way valve 19, the branch pipe 21, the three-way valve 22, the three-way valve 23, the pump 20, the damper 24, the mass flow meter 25, and the three-way valve 26 are passed in this order from the third recovery tank 5. It is sent to the mixing tank 7.
- the branch pipe 21 is provided with a fluid sensor 27. The fluid sensor 27 detects that the dispersion medium is flowing.
- a new dispersion medium is accommodated in the new dispersion medium tanks 28a and 28b.
- the pump 20 is driven and sent to the three-way valve 19 through the three-way valve 30. Thereafter, the flow path from the third recovery tank 5 to the preparation tank 7 is the same.
- recycled abrasive grains and recycled dispersion medium and in some cases, new abrasive grains and new dispersion medium are sent to the mixing tank 7 and stirred in the mixing tank 7 to obtain a cutting slurry used in the wire saw device. Played. Stirring is performed using a stirring member 17 that rotates as the motor 18 is driven.
- the volume of the regenerated slurry at this time is monitored by the ultrasonic sensor 31.
- the sensor 31 detects the liquid level of the regenerated slurry. Since the size of the mixing tank 7 is known in advance, the volume of the regenerated slurry can be calculated by detecting the liquid level.
- the first recovery tank 3, the third recovery tank 5, the fourth recovery tank 6, and the storage tank 16 are also provided with the same stirring member 17, motor 18, and ultrasonic sensor 31.
- the second collection tank 4 is provided with an ultrasonic sensor 31.
- the storage tank 16 is connected to the centrifuge 2 via a three-way valve 32, a variable control type quantitative supply means 33, and a mass flow meter 34.
- the supply means 33 is, for example, an air-driven or electrically-driven pump equipped with a function for preventing pulsation.
- the supply means 33 and the mass flow meter 34 are connected by wire using a PID controller 35 and a PLC or the like.
- the waste slurry is sent in a pulsating manner and in a fixed amount using the supply means 33.
- This actual flow value is measured by the mass flow meter 34.
- This actual flow rate value is compared with the set flow rate value by the PID control unit 35.
- the supply means 33 is controlled so that the actual flow rate value becomes the set flow rate value. For this reason, the supply means 33 is PID controlled so that the actual flow rate value of the waste slurry is fed back and approaches the set flow rate value, so that the waste slurry can be reliably fed into the centrifuge 2 at a constant flow rate. . For this reason, it is not necessary to adjust the flow rate by human hands, the flow rate can be automatically stabilized, and workability is improved.
- the three-way valve 32 is also connected to a fourth recovery tank 6 for recovering the mixed liquid, and the mixed liquid is also sent to the centrifuge 2 with the same flow rate control. Therefore, the flow rate control of the waste slurry and the mixed liquid can be performed by the same PID control unit 35, so that the number of parts can be reduced and the cost is also efficient.
- this PID control is an automatic control method using a touch panel and PLC, so that operability can be improved.
- You may enable it to select separation modes, such as collection
- a mode or a so-called one-stage separation oil recovery mode in which only oil is recovered may be selected.
- the new dispersion medium is also used for cleaning the equipment.
- the pump 36 When used for cleaning, the pump 36 is driven, a new dispersion medium is sent from the three-way valve 22 to the three-way valve 37, and the fourth recovery tank 6 is cleaned through the branch pipe 38 through the valve 41.
- Such supply of the new dispersion medium is also used when it is desired to increase the amount of the dispersion medium in the mixed liquid.
- the valve 42 is passed through the branch pipe 39, the inside of the centrifuge 2 can be washed.
- the valve 43 when the valve 43 is passed through the branch pipe 40, the discharge port 12 can be cleaned and the branch chute 8 can also be cleaned. In particular, the discharge port 12 and the branch chute 8 are regularly cleaned during the separation because the abrasive grains are stuck.
- the cutting waste has a very high viscosity and remains in the centrifuge 2 or the branch chute 8 (second path 8b), cleaning with a dispersion medium is indispensable.
- the storage tank 16 can be washed. This can also be used when it is desired to increase the amount of the dispersion medium in the waste slurry.
- the new dispersion medium for cleaning becomes unnecessary, the new dispersion medium is circulated from the three-way valve 37 to the three-way valve 29 and returned to the new dispersion medium tank 28a or 28b.
- FIG. 2 is a schematic plan view of a centrifuge used in the slurry regenerator according to the present invention
- FIG. 3 is a schematic side view.
- the centrifuge 2 includes the first motor 10 and the second motor 11.
- 45 is an inlet through which the waste slurry flows into the centrifuge 2.
- a discharge port 12 and a drain port 13 are provided below the centrifuge 2.
- 46a and 46b are inflow ports for allowing the new dispersion medium or the regenerated dispersion medium to flow in and washing the inside of the centrifuge 2.
- Reference numeral 47 denotes an inlet for washing the outlet 12 by introducing a new dispersion medium or a regenerated dispersion medium.
- FIG. 4 is a schematic diagram showing the relationship between the branch chute and the switching means used in the slurry regenerating apparatus according to the present invention.
- the branch chute 8 is surrounded by a frame body 49 having four rollers 48.
- the switching means 9 is connected to the frame 49.
- the switching means 9 is a cylinder and is movable in the axial direction (arrow R direction). With the movement of the switching means 9, the roller 48 moves on the rail 50, and the branch chute 8 is also pushed by the frame 49 and moves in the direction of arrow R.
- the inlet side of the branch chute 8 is connected to the first path 8a or second. To the path 8b.
- FIG. 5 is a schematic view of a branch chute.
- the branch chute 8 is divided into a first path 8a and a second path 8b on the exit side. Since the cutting waste is in a lump shape, the second path 8b is formed in the vertical direction from the discharge port 12 so that it can be dropped and collected. On the other hand, since the abrasive grains are collected with some dispersion medium mixed, they flow even if there is a slight angle, so the first path 8a is formed obliquely. The angle ⁇ is about 0 ° to 45 °.
- the inner surfaces of the first path 8a and the second path 8b are mirror-finished so that abrasive grains and cutting waste do not adhere to the inside.
- FIG. 6 is a flowchart of the slurry regeneration method according to the present invention.
- Step S1 The waste slurry after use is stored in a storage tank by a wire saw device.
- Step S2 The waste slurry is put into a centrifuge and primary separation is performed. In this primary separation, only the abrasive grains (primary separation) in the waste slurry are separated. This primary separation is centrifuged at a low G of less than 1500G. The centrifuge is charged without pulsation and quantitatively by the variable control type quantitative supply means 33 (see FIG. 1). The flow rate is managed by a mass flow meter, and the actual flow rate value is fed back and controlled by the PID control unit 35 (see FIG. 1) so as to approach the set flow rate value.
- the inside of the centrifuge and the branch chute (first path) are washed with a new dispersion medium at an appropriate time.
- the separated abrasive grains are recovered in the first recovery tank 3 (see FIG. 1).
- the mixed liquid after the abrasive grain separation is recovered in the fourth recovery tank 6 (see FIG. 1).
- the storage tank becomes empty the inside of the storage tank is washed with a dispersion medium, and the dispersion medium is primarily separated again. Thereby, the abrasive grains and cutting waste remaining in the storage tank can be removed and recovered.
- Step S3 The mixed liquid recovered in step S2 is again put into the centrifuge used in step S2, and secondary separation is performed.
- the mixed liquid is separated into cutting waste (secondary separated product) and a dispersion medium.
- This secondary separation is centrifuged at a high G of 1500 G or higher.
- the input control of the mixed liquid to the centrifugal separator is the same as the flow control of the waste slurry shown in step S2.
- the inside of the centrifuge and the branch chute (second path) are washed with a new dispersion medium at an appropriate time.
- the separated cutting waste is recovered in the second recovery tank 4 (see FIG. 1).
- the dispersion medium is recovered in the third recovery tank 5 (see FIG. 1).
- the fourth recovery tank When the fourth recovery tank becomes empty, the inside of the storage tank is washed with the dispersion medium, and the dispersion medium is secondarily separated again. Thereby, the cutting waste remaining in the fourth recovery tank can be removed and recovered. Thereafter, the specific gravity in the third recovery tank is measured to confirm the recovery of the dispersion medium in the secondary separation.
- Step S4 Abrasive grains recovered by primary separation, a dispersion medium recovered by secondary separation, and new abrasive grains and a new dispersion medium (new oil) are added as necessary to prepare a regenerated slurry. For example, (i) new abrasive grains and new oil are automatically added, or (ii) new abrasive grains are manually supplied and new oil is automatically supplied. (Iii) There is a method in which only new oil is automatically charged, or (iv) a new slurry and new oil which are formed in advance with new abrasive grains and new oil are automatically charged.
- recycle abrasive grains from the first recovery tank are transferred to the mixing tank. This transfer is performed so that all abrasive grains are transferred while washing the first recovery tank with the dispersion medium.
- the specific gravity in the preparation tank is measured and the abrasive recovery rate in the primary separation is determined. This determination may be performed after the end of step S2.
- the regenerated slurry has a target volume and specific gravity. The amount of recovered abrasive grains that is insufficient for the set value is replenished with new abrasive grains.
- a dispersion medium is also supplied. When it reaches the target specific gravity, it is used again as a regenerated slurry in a wire saw device.
- primary separation and secondary separation can be performed by generating different centrifugal forces of low G and high G using the first motor and the second motor. For this reason, abrasive grains (primary separation) and cutting waste (secondary separation) having different specific gravities can be reliably separated and recovered with only one centrifuge. Therefore, when separating, it is only necessary to secure a space in which one centrifuge can be installed, and space efficiency is high.
- Steps S1 to S4 described above are steps for performing a so-called two-stage separation mode in which the primary separation and the secondary separation are separated.
- steps S1, S2, and S4 are performed in this order except for step S3.
- steps S1, S2, and S4 are performed in this order except for step S3.
- steps S1, S2, and S4 are performed in this order except for step S3.
Abstract
Description
請求項4の発明では、請求項1~3のいずれかの発明において、前記廃スラリーは、ワイヤに被加工物を押し付けて切断加工するワイヤソー装置で用いたスラリーであり、前記一次分離物は前記スラリーに混入する砥粒であり、前記二次分離物は前記被加工物の切削屑であることを特徴としている。 In the invention of
According to a fourth aspect of the present invention, in the invention according to any one of the first to third aspects, the waste slurry is a slurry used in a wire saw device that presses a workpiece against a wire and cuts the wire, and the primary separated is the Abrasive grains mixed in the slurry, wherein the secondary separation is a cutting waste of the workpiece.
請求項4の発明によれば、ワイヤソー装置で用いた廃スラリーに含まれる再利用可能な砥粒を一次分離物として回収し、被加工物の切削屑を二次分離物として、別に回収できる。したがって、分散媒と砥粒を再び混合して切削用スラリーとしてワイヤソー装置に再利用できる。このため、スラリーの節約ができる。 According to the invention of
According to invention of
請求項6の発明によれば、廃スラリー又は混合液の実流量値をフィードバックさせて設定流量値に近づくように可変制御式定量供給手段をPID制御するので、確実に廃スラリー又は混合液を一定流量で遠心分離機に投入することができる。また、無脈動かつ定量に液を供給することで安定した遠心分離効果が得られる。 According to invention of
According to the sixth aspect of the present invention, the variable control type quantitative supply means is PID controlled so that the actual flow rate value of the waste slurry or the mixed solution is fed back and approaches the set flow rate value. The centrifuge can be charged at a flow rate. In addition, a stable centrifugal effect can be obtained by supplying the solution without pulsation and quantification.
図示したように、本発明に係るスラリー再生装置1は、遠心分離機2と、砥粒(一次分離物)を回収するための第1の回収槽3と、切削屑(二次分離物)を回収するための第2の回収槽4と、分散媒を回収するための第3の回収槽5と、混合液を回収するための第4の回収槽6と、再生スラリーを調合するための調合槽7と、分岐シュート8と、切替手段9とを備えている。遠心分離機2は、2台のモータ(第1のモータ10、第2のモータ11)をそれぞれ備えており、低G又は高Gと異なる遠心力を発生させることができる。 FIG. 1 is a schematic view of a slurry regenerator according to the present invention.
As shown in the figure, the slurry regenerating apparatus 1 according to the present invention includes a
上述したように、遠心分離機2には、第1のモータ10及び第2のモータ11が備わっている。45は、廃スラリーが遠心分離機2内に流入する流入口である。遠心分離機2の下側には、上述しように、排出口12、排液口13が備わっている。46a、46bは、新分散媒又は再生分散媒を流入させて遠心分離機2内を洗浄するための流入口である。47は、新分散媒又は再生分散媒を流入させて排出口12を洗浄するための流入口である。 FIG. 2 is a schematic plan view of a centrifuge used in the slurry regenerator according to the present invention, and FIG. 3 is a schematic side view.
As described above, the
分岐シュート8は、4本のローラ48を備えた枠体49に囲まれて配設されている。枠体49に切替手段9が接続されている。切替手段9は、シリンダであり、軸方向(矢印R方向)に移動可能である。切替手段9の移動に伴い、ローラ48がレール50上を移動し、分岐シュート8も枠体49に押されて矢印R方向に移動する。分岐シュート8の上方に位置する遠心分離機2の排出口12(図1、図3参照)から落下してくる分離物に応じて、分岐シュート8の入口側を第1の経路8a又は第2の経路8bに切替える。分岐シュート8を枠体49で囲むことにより、分岐シュート8のみの修理や交換が独立して容易に行うことができ、メンテナンス性が向上する。 FIG. 4 is a schematic diagram showing the relationship between the branch chute and the switching means used in the slurry regenerating apparatus according to the present invention.
The
図示したように、分岐シュート8は、出口側が第1の経路8aと第2の経路8bに分かれている。切削屑は塊状なので、落下させて回収できるように、第2の経路8bは排出口12から鉛直方向に形成されている。一方、砥粒は若干分散媒が混じって回収されるので、多少角度があっても流れるため、第1の経路8aは斜めに形成されている。その角度θは、0°~45°程度である。なお、第1の経路8a及び第2の経路8bの内面は、内側に砥粒や切削屑が付着しないように、鏡面仕上げされている。 FIG. 5 is a schematic view of a branch chute.
As illustrated, the
ステップS1:
ワイヤソー装置にて使用後の廃スラリーを収容槽に収容する。
ステップS2:
廃スラリーを遠心分離機に投入し、一次分離を行う。この一次分離にて、廃スラリー中の砥粒(一次分離物)のみを分離する。この一次分離は、1500G未満の低Gで遠心分離される。遠心分離機への投入は、可変制御式定量供給手段33(図1参照)によって無脈動かつ定量で行われる。その流量は質量流量計によって管理され、実流量値がフィードバックされ設定流量値に近づくようにPID制御部35(図1参照)にて制御される。一次分離中、適時に新分散媒等で遠心分離機内や分岐シュート(第1の経路)内が洗浄される。分離された砥粒は、第1の回収槽3(図1参照)に回収される。砥粒分離後の混合液は、第4の回収槽6(図1参照)に回収される。収容槽が空になった場合は、分散媒にて収容槽内を洗浄し、この分散媒を再び一次分離する。これにより、収容槽内に残った砥粒や切削屑を取り除き、回収することができる。 FIG. 6 is a flowchart of the slurry regeneration method according to the present invention.
Step S1:
The waste slurry after use is stored in a storage tank by a wire saw device.
Step S2:
The waste slurry is put into a centrifuge and primary separation is performed. In this primary separation, only the abrasive grains (primary separation) in the waste slurry are separated. This primary separation is centrifuged at a low G of less than 1500G. The centrifuge is charged without pulsation and quantitatively by the variable control type quantitative supply means 33 (see FIG. 1). The flow rate is managed by a mass flow meter, and the actual flow rate value is fed back and controlled by the PID control unit 35 (see FIG. 1) so as to approach the set flow rate value. During the primary separation, the inside of the centrifuge and the branch chute (first path) are washed with a new dispersion medium at an appropriate time. The separated abrasive grains are recovered in the first recovery tank 3 (see FIG. 1). The mixed liquid after the abrasive grain separation is recovered in the fourth recovery tank 6 (see FIG. 1). When the storage tank becomes empty, the inside of the storage tank is washed with a dispersion medium, and the dispersion medium is primarily separated again. Thereby, the abrasive grains and cutting waste remaining in the storage tank can be removed and recovered.
ステップS2で回収した混合液をステップS2で用いた遠心分離機に再び投入し、二次分離を行う。この二次分離にて、混合液を切削屑(二次分離物)と分散媒とに分離する。この二次分離は、1500G以上の高Gで遠心分離される。混合液の遠心分離機への投入制御は、ステップS2で示した廃スラリーの流量制御と同様である。二次分離中、適時に新分散媒等で遠心分離機内や分岐シュート(第2の経路)内が洗浄される。分離された切削屑は、第2の回収槽4(図1参照)に回収される。分散媒は、第3の回収槽5(図1参照)に回収される。第4の回収槽が空になった場合は、分散媒にて収容槽内を洗浄し、この分散媒を再び二次分離する。これにより、第4の回収槽内に残った切削屑を取り除き、回収することができる。この後、第3の回収槽内の比重を計測し、二次分離における分散媒の回収を確認する。 Step S3:
The mixed liquid recovered in step S2 is again put into the centrifuge used in step S2, and secondary separation is performed. In this secondary separation, the mixed liquid is separated into cutting waste (secondary separated product) and a dispersion medium. This secondary separation is centrifuged at a high G of 1500 G or higher. The input control of the mixed liquid to the centrifugal separator is the same as the flow control of the waste slurry shown in step S2. During the secondary separation, the inside of the centrifuge and the branch chute (second path) are washed with a new dispersion medium at an appropriate time. The separated cutting waste is recovered in the second recovery tank 4 (see FIG. 1). The dispersion medium is recovered in the third recovery tank 5 (see FIG. 1). When the fourth recovery tank becomes empty, the inside of the storage tank is washed with the dispersion medium, and the dispersion medium is secondarily separated again. Thereby, the cutting waste remaining in the fourth recovery tank can be removed and recovered. Thereafter, the specific gravity in the third recovery tank is measured to confirm the recovery of the dispersion medium in the secondary separation.
一次分離にて回収した砥粒、二次分離にて回収した分散媒、さらに必要に応じて新砥粒及び新分散媒(新オイル)を加えて再生スラリーを調合する。この新砥粒や新オイル等の投入の仕方は、例えば、(i)新砥粒及び新オイルを自動で投入したり、(ii)新砥粒を手動で、新オイルを自動で投入したり、(iii)新オイルのみを自動で投入したり、(iv)新砥粒と新オイルで予め形成された新スラリー及び新オイルを自動で投入する方法がある。 Step S4:
Abrasive grains recovered by primary separation, a dispersion medium recovered by secondary separation, and new abrasive grains and a new dispersion medium (new oil) are added as necessary to prepare a regenerated slurry. For example, (i) new abrasive grains and new oil are automatically added, or (ii) new abrasive grains are manually supplied and new oil is automatically supplied. (Iii) There is a method in which only new oil is automatically charged, or (iv) a new slurry and new oil which are formed in advance with new abrasive grains and new oil are automatically charged.
2 遠心分離機
3 第1の回収槽
4 第2の回収槽
5 第3の回収槽
6 第4の回収槽
7 調合槽
8 分岐シュート
8a 第1の経路
8b 第2の経路
9 切替手段
10 第1のモータ
11 第2のモータ
12 排出口
13 排液口
14 三方弁
15 ポンプ
16 収容槽
17 攪拌部材
18 モータ
19 三方弁
20 ポンプ
21 分岐管
22 三方弁
23 三方弁
24 ダンパー
25 質量流量計
26 三方弁
27 流体センサ
28a 新分散媒槽
28b 新分散媒槽
29 三方弁
30 三方弁
31 超音波センサ
32 三方弁
33 可変制御式定量供給手段
34 質量流量計
35 PID制御部
36 ポンプ
37 三方弁
38 分岐管
39 分岐管
40 分岐管
41 バルブ
42 バルブ
43 バルブ
44 バルブ
45 流入口
46a 流入口
46b 流入口
47 流入口
48 ローラ
49 枠体
50 レール
51 ポンプ
52 混合液廃棄槽 DESCRIPTION OF SYMBOLS 1 Slurry reproduction |
Claims (6)
- 分散媒中に前記分散媒から分離されるべき互いに比重の異なる一次分離物及び二次分離物の少なくとも一方を含む廃スラリーが投入され、前記廃スラリーから前記一次分離物又は前記二次分離物を分離可能な遠心分離機と、
前記遠心分離機に設けられ、前記遠心分離機から分離後の前記一次分離物又は前記二次分離物を排出する排出口と、
該排出口に前記一次分離物を移送するための第1の経路を介して連通可能な前記一次分離物を回収するための第1の回収槽と、
前記排出口に前記二次分離物を移送するための第2の経路を介して連通可能な前記二次分離物を回収するための第2の回収槽と、
前記遠心分離機に設けられ、前記遠心分離機から前記廃スラリーを分離した後の前記分散媒又は該分散媒と前記二次分離物の混合液を排液する排液口と、
該排液口に対して選択的に連通可能な前記分散媒を回収するための第3の回収槽及び前記混合液を回収するための第4の回収槽と、
前記一次分離物と前記分散媒とを混合して再生スラリーを生成するための調合槽と、
前記排出口に対して、前記第1の経路と前記第2の経路のいずれかを接続させる切替手段とを備えたことを特徴とするスラリー再生装置。 A waste slurry containing at least one of a primary separator and a secondary separator having different specific gravity to be separated from the dispersion medium is introduced into the dispersion medium, and the primary separator or the secondary separator is removed from the waste slurry. A separable centrifuge,
Provided in the centrifuge, and a discharge port for discharging the primary separated product or the secondary separated product after separation from the centrifuge;
A first recovery tank for recovering the primary separator that can be communicated via a first path for transferring the primary separator to the outlet;
A second recovery tank for recovering the secondary separator that can be communicated via a second path for transferring the secondary separator to the discharge port;
A drainage port provided in the centrifuge, for draining the dispersion medium after separating the waste slurry from the centrifuge, or a mixture of the dispersion medium and the secondary separation;
A third recovery tank for recovering the dispersion medium that can selectively communicate with the drainage port, and a fourth recovery tank for recovering the mixed liquid;
A mixing tank for mixing the primary separation and the dispersion medium to produce a regenerated slurry;
A slurry regenerator comprising switching means for connecting either the first path or the second path to the discharge port. - 前記廃スラリーを収容するための収容槽と前記遠心分離機の間、及び前記第4の回収槽と前記遠心分離機の間にそれぞれ設けられ、前記廃スラリー又は前記混合液の流量を調整する可変制御式定量供給手段と、該可変制御式定量供給手段と前記遠心分離機の間に設けられた質量流量計と、前記質量流量計の計測結果に基づき、前記廃スラリー又は前記混合液の流量を一定にすべく前記可変制御式定量供給手段の作動を制御するPID制御部とを更に備えることを特徴とする請求項1に記載のスラリー再生装置。 Variable between the storage tank for storing the waste slurry and the centrifuge, and between the fourth recovery tank and the centrifuge, and for adjusting the flow rate of the waste slurry or the mixed liquid. The flow rate of the waste slurry or the mixed liquid is controlled based on the measurement result of the control type quantitative supply unit, the mass flow meter provided between the variable control type quantitative supply unit and the centrifuge, and the mass flow meter. The slurry regenerating apparatus according to claim 1, further comprising a PID control unit that controls the operation of the variable control type quantitative supply unit so as to be constant.
- 前記収容槽と前記第4の回収槽、及び前記遠心分離機は、三方弁を介して接続され、前記可変制御式定量供給手段及び前記質量流量計は、前記三方弁と前記遠心分離機の間に配置されていることを特徴とする請求項1又は2に記載のスラリー再生装置。 The storage tank, the fourth recovery tank, and the centrifuge are connected via a three-way valve, and the variable control quantitative supply means and the mass flow meter are disposed between the three-way valve and the centrifuge. The slurry regenerator according to claim 1 or 2, wherein
- 前記廃スラリーは、ワイヤに被加工物を押し付けて切断加工するワイヤソー装置で用いたスラリーであり、前記一次分離物は前記スラリーに混入する砥粒であり、前記二次分離物は前記被加工物の切削屑であることを特徴とする請求項1~3のいずれかに記載のスラリー再生装置。 The waste slurry is a slurry used in a wire saw device that presses and cuts a workpiece against a wire, the primary separation is abrasive grains mixed in the slurry, and the secondary separation is the workpiece. The slurry reclaiming device according to any one of claims 1 to 3, wherein the slurry reclaiming device is any of the above.
- 請求項1~4のいずれかに記載のスラリー再生装置を用いたスラリー再生方法であって、
前記遠心分離機に前記廃スラリーを投入し、
前記遠心分離機を所定の遠心力(低G)で駆動して、前記一次分離物を前記廃スラリーから遠心分離し、
該遠心分離した一次分離物を前記第1の回収槽に回収し、
前記混合液を前記第4の回収槽に回収し、
該第4の回収槽から前記混合液を前記遠心分離機に投入し、
前記遠心分離機を前記所定の遠心力より高い遠心力(高G)で駆動して前記二次分離物を前記混合液から遠心分離し、
該遠心分離した二次分離物を前記第2の回収槽に回収し、
前記分散媒を前記第3の回収槽に回収し、
前記調合槽に、前記第1の回収槽に回収された前記一次分離物と、前記第3の回収槽に回収された前記分散媒と、新しい一次分離物及び新しい分散媒とを投入し、再生スラリーを生成することを特徴とするスラリー再生方法。 A slurry regeneration method using the slurry regeneration apparatus according to any one of claims 1 to 4,
Throwing the waste slurry into the centrifuge,
Driving the centrifuge at a predetermined centrifugal force (low G) to centrifuge the primary separation from the waste slurry;
Collecting the centrifuged primary separation in the first collection tank;
The mixed liquid is recovered in the fourth recovery tank;
Throwing the mixed solution from the fourth recovery tank into the centrifuge;
Driving the centrifuge at a centrifugal force (high G) higher than the predetermined centrifugal force to centrifuge the secondary separation from the mixture;
Collecting the centrifuged secondary separation in the second recovery tank;
Collecting the dispersion medium in the third collection tank;
The primary separation collected in the first collection tank, the dispersion medium collected in the third collection tank, a new primary separation and a new dispersion medium are charged into the mixing tank and regenerated. A slurry regeneration method comprising producing a slurry. - 前記質量流量計により前記廃スラリー又は前記混合液の実流量値を計測し、前記PID制御部にて前記実流量値と設定流量値を比較し、前記実流量値が前記設定流量値になるように、前記可変制御式定量供給手段をPID制御することを特徴とする請求項5に記載のスラリー再生方法。 The actual flow rate value of the waste slurry or the mixed solution is measured by the mass flow meter, the actual flow rate value is compared with the set flow rate value by the PID control unit, and the actual flow rate value becomes the set flow rate value. 6. The slurry regeneration method according to claim 5, wherein the variable control type quantitative supply means is PID controlled.
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TWI461258B (en) * | 2012-11-09 | 2014-11-21 | Sino American Silicon Prod Inc | Slurry recycling method and slurry recycling apparatus for the same |
JP2017012974A (en) * | 2015-06-30 | 2017-01-19 | 日立工機株式会社 | Centrifugal machine |
WO2020246162A1 (en) * | 2019-06-03 | 2020-12-10 | 株式会社industria | Fine material amount detection device, clamp-type holder, centrifugal separation device, and fine material removal system |
TWI779280B (en) * | 2019-06-03 | 2022-10-01 | 日商英達斯特股份有限公司 | System for removing fine material |
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