WO2009052861A1 - Structure textile thermoscellable, fabrication et utilisation - Google Patents

Structure textile thermoscellable, fabrication et utilisation Download PDF

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Publication number
WO2009052861A1
WO2009052861A1 PCT/EP2007/061467 EP2007061467W WO2009052861A1 WO 2009052861 A1 WO2009052861 A1 WO 2009052861A1 EP 2007061467 W EP2007061467 W EP 2007061467W WO 2009052861 A1 WO2009052861 A1 WO 2009052861A1
Authority
WO
WIPO (PCT)
Prior art keywords
heat
silane
sealable
textile fabric
adhesive layer
Prior art date
Application number
PCT/EP2007/061467
Other languages
German (de)
English (en)
Inventor
Reinhard Klein
Abdul-Hamid Nauros
Original Assignee
Kufner Textil Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kufner Textil Gmbh filed Critical Kufner Textil Gmbh
Priority to CN2007801020918A priority Critical patent/CN101910505A/zh
Priority to PCT/EP2007/061467 priority patent/WO2009052861A1/fr
Priority to JP2010530282A priority patent/JP2011500985A/ja
Priority to MX2010004448A priority patent/MX2010004448A/es
Priority to KR1020107011244A priority patent/KR20100091189A/ko
Priority to EP07821830.2A priority patent/EP2203587B1/fr
Priority to CA2703353A priority patent/CA2703353A1/fr
Priority to PE2008001824A priority patent/PE20091276A1/es
Priority to ARP080104636A priority patent/AR069018A1/es
Publication of WO2009052861A1 publication Critical patent/WO2009052861A1/fr
Priority to IL205259A priority patent/IL205259A0/en

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M17/00—Producing multi-layer textile fabrics
    • D06M17/04—Producing multi-layer textile fabrics by applying synthetic resins as adhesives
    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
    • A41D27/00—Details of garments or of their making
    • A41D27/02—Linings
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06N3/042—Acrylic polymers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/121—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyesters, polycarbonates, alkyds
    • D06N3/123—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyesters, polycarbonates, alkyds with polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N7/00—Flexible sheet materials not otherwise provided for, e.g. textile threads, filaments, yarns or tow, glued on macromolecular material
    • D06N7/0092—Non-continuous polymer coating on the fibrous substrate, e.g. plastic dots on fabrics
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/12—Permeability or impermeability properties
    • D06N2209/126—Permeability to liquids, absorption
    • D06N2209/128—Non-permeable
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2211/00—Specially adapted uses
    • D06N2211/10—Clothing

Definitions

  • Heat-sealable textile fabric its manufacture and use
  • the present invention relates to a heat-sealable textile fabric for reinforcing garments, in particular to articles of clothing rendered hydrophobic, to the production thereof and to particularly advantageous uses thereof.
  • Such fabrics use as support material woven, knitted fabric, optionally with weft insertion, and nonwovens, being used as material yarns, in particular polyethylene, polypropylene, polyethylene terephthalate, polyamide, polyacrylonitrile, cellulose or cotton or mixtures thereof.
  • material yarns in particular polyethylene, polypropylene, polyethylene terephthalate, polyamide, polyacrylonitrile, cellulose or cotton or mixtures thereof.
  • highly elastic or even less elastic inserts can be produced, wherein said yarns can also be textured yarns.
  • a (enamel TM) adhesive layer is then applied, with this
  • Adhesive layer the connection with the garment takes place.
  • the chemical and physical-chemical properties of the heat-sealable adhesive layer are selected so that the respective requirements for melting range,
  • Such fabrics can also be used for applications other than outerwear such as technical applications, with other criteria being important such as adequate heat resistance, low lamination temperatures, or the like
  • the required requirements for the sufficient adhesive forces between the fabric and the outerwear fabric are generally met if the adhesive system is suitably selected.
  • the adhesive system is suitably selected.
  • polyurethane, copolyester or copolyamide as well as polyacrylate are used as the material of the adhesive.
  • At least one silane used in admixture with the polymeric material are preferred
  • Epoxysilanes, aminosilanes and acrylic silanes or mixtures thereof used are particularly preferred among these silanes, with those having alkoxy functional groups being particularly preferred according to the following general formula:
  • R l alkyl radical having 1-8 C atoms or an alkyl radical of 2 to 8 C atoms, which is an oxygen atom in the
  • n 0 or 1
  • R2 H or alkyl radical having 1-8 C atoms
  • R 3 alkyl radical of 1-8 C atoms or an aryl or cycloalkyl radical or an arylalkyl radical
  • R 4 alkyl radical of 1-8 C atoms
  • the mixture between the polymeric material and the at least one silane may, according to a particularly preferred embodiment, be carried out by the so-called "dry-blending" process, which mixture may consist of the powder of the polymeric material and a powder of the at least one silane. wherein these substances are mixed dry in a suitable mixing ratio, usually at room temperature.
  • the material for the adhesive layer in the form of a paste.
  • the materials to be used for this purpose from the powder of the polymeric material and the powder of the at least one silane are mixed with water, preferably at room temperature, if appropriate with the additional use of a customary flow aid, a thickener and optionally further customary additives. These materials are mixed into a paste and then applied in the usual way in the form of a so-called paste point.
  • a suitable mixing ratio between the at least one silane and the polymeric material is in the range (weight ratio) of 99.95-95.00% of the polymeric material and 0.05-5.00% of the total amount of the silane, preferably 99.90-98 , 00% of the polymer and 0.10-2.00% of the total amount of silane.
  • the content of the silane is particularly preferably 0.5-1.5% by weight. If larger quantities of silane are used to produce the mixture of the polymeric material and the silane, a deterioration of the adhesive force may occur. If this adhesive composition is applied in the form of a powder, amounts of more than about 10% by weight of silane can impair the flowability of the resulting scattering powder.
  • This invention also relates to a process for producing a heat sealable fabric.
  • a raw fabric, raw knit fabric, optionally with weft insertion, or a nonwoven fabric in the usual manner. This is usually followed by a washing and / or shrinking process, optionally followed by a dyeing process.
  • a washing and / or shrinking process optionally followed by a dyeing process.
  • thermal stabilization of the raw fabric, raw knit fabric or nonwoven fabric thus obtained one side thereof is usually applied in raster form with an adhesive layer which contains the mixture of the polymeric material with the at least one silane claimed according to the invention.
  • the application weight of the adhesive according to the invention is generally 8-15 g / m 2 , preferably 9-13 g / m 2 .
  • the adhesive layer can by the well-known
  • Paste dot method, powder dot method or even a double-point method are applied to the carrier material.
  • Such coating methods have long been state of the art and can be used according to the invention without restriction.
  • the adhesive is applied in the form of a colon, it is possible to use the adhesive of the polymeric material with the silane, respectively to use for the top and bottom.
  • the sub-point is based on polyurethane, polyacrylate, copolyester or copolyamide and thus no mixture with silane is used.
  • the upper point consists of the described mixture of the polymeric material with the at least one silane. This results in a particularly good adhesion to a hydrophobically finished outer fabric, which is used for example for rainwear.
  • An adhesive used particularly preferably is a mass of copolyamide with the abovementioned
  • the textile fabric described according to the invention will preferably be used to reinforce garments, in particular hydrophobically finished or siliconized garments. Especially when the fabric is used for a rainwear such as a raincoat, rain jacket or pants, good adhesion values are associated with a high waterproofness of the produced composite.
  • a polyester fabric made of texturized yarns (warp dtex 35 f 24/1, weft dtex 100 f 72/1, basis weight about 25 g / m 2 ) is crosslinked in the usual way
  • Silicone softener equipped (12 g / l, liquor uptake 85%) and thermally fixed.
  • this interlining material is printed in a known manner with a polyurethane paste prepared from a polyurethane dispersion, acrylate thickener and running aid and sprinkled with copolyamide scattering powder (Vestamelt X1027 80-200 ⁇ m from Degussa). Excess dust is sucked out.
  • the coated web is then driven through a Tockenofen, in which the printed polymer dots are dried and sintered. At the end of the dryer tunnel, the web is cooled by means of cooling rolls and wound up on a quay.
  • the coating weight of the insert is 9-11 g / m 2 .
  • Example 2 The same polyester fabric as in Example 1 is equipped as described there with silicone plasticizer and thermally fixed.
  • the interlining material is printed as described in Example 1 and sprinkled with copolyamide scattering powder to which 1% aminosilane (N- (2-aminoethyl) -3-aminopropyltrimethoxysilane) was mixed homogeneously. After sucking off the excess scattering powder is dried as described in Example 1, sintered, cooled and wound up. The coating weight is 9-11 g / m 2 . (Insert 2)
  • a knit fabric made of 100% polyamide (warp dtex 17 f 5; weft dtex 22 f 14/2; basis weight approx. 18 g / m 2 ) is equipped, thermally fixed and coated as described in Example 1.
  • the coating weight is 8 ⁇ 10 g / m 2 . (Insert 3)
  • a knit fabric of 100% polyamide as described in Example 3 is printed with polyurethane paste as described in Example 2 and sprinkled with silane-modified copolymide (1% aminosilane, 99% copolyamide).
  • the product is freed by suction from excess dusting powder and dried in a drying oven and sintered. After cooling on a cooling roller, the coated goods are wound onto a quay.
  • the coating weight is 8-10 g / m 2 .
  • Thermobonded nonwoven 100% polyamide (basis weight 22 g / m 2 ) is coated and wound up as described in Example 1.
  • the coating weight is 10-12 g / m 2 . (Insert 5)
  • Thermobonded nonwoven made of 100% polyamide is printed with polyurethane paste as described in Example 2 and sprinkled with silane-modified Copolyamidstreupulver, vacuumed, sintered, cooled and wound ..
  • the coating weight is 10-12 g / m 2 .
  • a knit fabric of 100% polyamide as described in Example 3 is printed with polyurethane paste as described in Example 2 and copolyamide scattering powder modified with epoxy silane (3-glycidyloxypropyltrimethoxysilane ⁇ sprinkled, filtered off with suction, sintered, cooled and wound up.
  • the coating weight is 10-13 g / m 2 .
  • a knit fabric of 100% polyamide as described in Example 2 is printed with a paste which in addition to the usual paste ingredients such as flow aids and thickeners also copolyamide powder sized 80-200 microns sprinkled, vacuumed, sintered, cooled and wound up.
  • the coating weight is 10-13 g / m 2 .
  • a knit fabric printed as in Example 8 is included
  • the coating weight is 10-13 g / m 2 . (Insert 9)
  • a knitted fabric as described in Example 3 is equipped as described in Example 1, thermally fixed, and (on a powder-point system by means of gravure roll 28 mesh ⁇ dot coated with copolyamide.
  • the coating weight of between 12 and 15 g / m 2. (Insert 10)
  • Example 12 A knit fabric prepared as in Example 10 is coated with aminosilane-modified copolyamide powder (1% aminosilane, 99% copolyamide) as described therein. The coating weight is also 12-15 g / m 2 . (Insert 11) Example 12
  • Example 3 A knit fabric as described in Example 3 is prepared according to Example 1, thermally fixed and printed with a paste containing about 30% copolyamide paste powder (0-80 microns). The product is dried as usual and the coating is sintered. The coating weight of the insert is 9-11 g / m 2 . (Insert 12)
  • Example 3 A knit fabric as described in Example 3 is equipped according to Example 1, thermally fixed and printed with a copolyamide paste to which 0.5% aminosilane was mixed homogeneously.
  • the coating weight of the insert is 7-9 g / m 2 .
  • the test fabric for the adhesion tests is a polyester fabric which has been pad-finished with a three-dimensional cross-linkable silicone.
  • the interlining of Example 1-13 were pressed with this outer fabric on a fuser press at 127 0 C joint temperature, a pressure of 1.5 bar and a residence time of 10 s and then cut into 5 cm wide strips. These specimens were tested after storage for 48 hours under standard conditions (DIN 53 802-79) with the aid of an adhesion tester from Instron (INSTRON 44443) with regard to the adhesive strength of the insert on the outer fabric in accordance with DIN 54 310.
  • the outer material and the insert are separated by hand so that the outer fabric and insert can be clamped in the clamping device of the Trennkraftprüfauss in the test specimens.
  • Inlay and outer fabric are separated at a defined terminal removal speed. It will determines the force required to separate the two interconnected fabrics. The average values from 5 measurements are given.

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Laminated Bodies (AREA)
  • Adhesive Tapes (AREA)
  • Manufacturing Of Multi-Layer Textile Fabrics (AREA)

Abstract

L'invention concerne une structure textile thermoscellable comportant un support à base de tissu, de maillage, éventuellement à insertion de la trame, ou de non-tissé, et une couche adhésive appliquée en forme de grille sur le support, la couche adhésive contenant un matériau polymère et au moins un silane. La couche adhésive peut être produite sous forme d'un point de pâte, d'un point de poudre ou d'un point double. Lorsque cette structure textile thermoscellable est notamment employée avec des vêtements à traitement hydrophobe, il est possible d'obtenir une grande force adhésive associée à une grande imperméabilité à l'eau. L'invention concerne également un procédé de fabrication d'une telle structure textile.
PCT/EP2007/061467 2007-10-25 2007-10-25 Structure textile thermoscellable, fabrication et utilisation WO2009052861A1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
CN2007801020918A CN101910505A (zh) 2007-10-25 2007-10-25 可热密封的平面织物结构、其的制备和应用
PCT/EP2007/061467 WO2009052861A1 (fr) 2007-10-25 2007-10-25 Structure textile thermoscellable, fabrication et utilisation
JP2010530282A JP2011500985A (ja) 2007-10-25 2007-10-25 ヒートシール可能なシート状織物構造、その製造および使用
MX2010004448A MX2010004448A (es) 2007-10-25 2007-10-25 Estructura textil plana, termosellable, produccion y uso de la misma.
KR1020107011244A KR20100091189A (ko) 2007-10-25 2007-10-25 열접착성의 평면형 직물 구조체, 이의 제조 방법 및 용도
EP07821830.2A EP2203587B1 (fr) 2007-10-25 2007-10-25 Structure textile thermoscellable, fabrication et utilisation
CA2703353A CA2703353A1 (fr) 2007-10-25 2007-10-25 Structure textile thermoscellable, fabrication et utilisation
PE2008001824A PE20091276A1 (es) 2007-10-25 2008-10-24 Estructura textil plana, termosellable, produccion y uso de la misma
ARP080104636A AR069018A1 (es) 2007-10-25 2008-10-24 Estructura textil plana, termosellable, produccion y uso de la misma
IL205259A IL205259A0 (en) 2007-10-25 2010-04-22 Heat-sealable sheet - like textile structure, production of the same and use

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP2007/061467 WO2009052861A1 (fr) 2007-10-25 2007-10-25 Structure textile thermoscellable, fabrication et utilisation

Publications (1)

Publication Number Publication Date
WO2009052861A1 true WO2009052861A1 (fr) 2009-04-30

Family

ID=39523745

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2007/061467 WO2009052861A1 (fr) 2007-10-25 2007-10-25 Structure textile thermoscellable, fabrication et utilisation

Country Status (10)

Country Link
EP (1) EP2203587B1 (fr)
JP (1) JP2011500985A (fr)
KR (1) KR20100091189A (fr)
CN (1) CN101910505A (fr)
AR (1) AR069018A1 (fr)
CA (1) CA2703353A1 (fr)
IL (1) IL205259A0 (fr)
MX (1) MX2010004448A (fr)
PE (1) PE20091276A1 (fr)
WO (1) WO2009052861A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102389174B (zh) * 2011-07-25 2014-04-02 温州鸿马科技有限公司 双点非织造热熔衬的生产工艺
CN102793319A (zh) * 2012-07-03 2012-11-28 昆山市周市镇吉盛服装厂 一种高伸展性面料
CN108135300B (zh) * 2015-10-06 2020-03-10 耐克创新有限合伙公司 用于结合接缝的感应加热方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06145413A (ja) * 1992-11-02 1994-05-24 Nippon Zeon Co Ltd ホットメルト樹脂浸透防止用組成物及び接着芯地
JP2001336072A (ja) * 2000-05-30 2001-12-07 Mitsubishi Chemicals Corp 接着用布地
EP1541751A1 (fr) 2003-12-12 2005-06-15 Dr. Th. Böhme KG Chem. Fabrik GmbH & Co. Utilisation de polymères stabilisées au moyen de colloides protecteurs en tant que revêtements

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06145413A (ja) * 1992-11-02 1994-05-24 Nippon Zeon Co Ltd ホットメルト樹脂浸透防止用組成物及び接着芯地
JP2001336072A (ja) * 2000-05-30 2001-12-07 Mitsubishi Chemicals Corp 接着用布地
EP1541751A1 (fr) 2003-12-12 2005-06-15 Dr. Th. Böhme KG Chem. Fabrik GmbH & Co. Utilisation de polymères stabilisées au moyen de colloides protecteurs en tant que revêtements

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Week 200244, Derwent World Patents Index; AN 2002-408584, XP002485651 *

Also Published As

Publication number Publication date
CN101910505A (zh) 2010-12-08
KR20100091189A (ko) 2010-08-18
EP2203587A1 (fr) 2010-07-07
PE20091276A1 (es) 2009-09-03
AR069018A1 (es) 2009-12-23
MX2010004448A (es) 2010-05-13
JP2011500985A (ja) 2011-01-06
CA2703353A1 (fr) 2009-04-30
EP2203587B1 (fr) 2013-08-28
IL205259A0 (en) 2010-12-30

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