WO2009047456A3 - Procede continu d ' obtention de fibres composites a base de particules colloïdales et fibre obtenue par ce procede - Google Patents

Procede continu d ' obtention de fibres composites a base de particules colloïdales et fibre obtenue par ce procede Download PDF

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Publication number
WO2009047456A3
WO2009047456A3 PCT/FR2008/051679 FR2008051679W WO2009047456A3 WO 2009047456 A3 WO2009047456 A3 WO 2009047456A3 FR 2008051679 W FR2008051679 W FR 2008051679W WO 2009047456 A3 WO2009047456 A3 WO 2009047456A3
Authority
WO
WIPO (PCT)
Prior art keywords
fibre
composite fibres
colloidal particles
obtaining composite
continuous method
Prior art date
Application number
PCT/FR2008/051679
Other languages
English (en)
Other versions
WO2009047456A2 (fr
Inventor
Alain DERRÉ
Antoine Lucas
Philippe Poulin
Original Assignee
Arkema France
Centre National De La Recherche Scientifique - Cnrs -
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to US12/677,619 priority Critical patent/US20100196250A1/en
Application filed by Arkema France, Centre National De La Recherche Scientifique - Cnrs - filed Critical Arkema France
Priority to CN200880107385A priority patent/CN101802276A/zh
Priority to JP2010524559A priority patent/JP2010539342A/ja
Priority to EP08838292A priority patent/EP2191045A2/fr
Publication of WO2009047456A2 publication Critical patent/WO2009047456A2/fr
Publication of WO2009047456A3 publication Critical patent/WO2009047456A3/fr

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Classifications

    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62231—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62231—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
    • C04B35/6224—Fibres based on silica
    • C04B35/62245—Fibres based on silica rich in aluminium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62272—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on non-oxide ceramics
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62272—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on non-oxide ceramics
    • C04B35/62277—Fibres based on carbides
    • C04B35/62281—Fibres based on carbides based on silicon carbide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62272—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on non-oxide ceramics
    • C04B35/62286—Fibres based on nitrides
    • C04B35/6229—Fibres based on nitrides based on boron nitride
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632—Organic additives
    • C04B35/634—Polymers
    • C04B35/63404—Polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C04B35/63416—Polyvinylalcohols [PVA]; Polyvinylacetates
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632—Organic additives
    • C04B35/636—Polysaccharides or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632—Organic additives
    • C04B35/636—Polysaccharides or derivatives thereof
    • C04B35/6365—Cellulose or derivatives thereof
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/06—Wet spinning methods
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/5208—Fibers
    • C04B2235/5264—Fibers characterised by the diameter of the fibers

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Textile Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Inorganic Fibers (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Artificial Filaments (AREA)
  • Materials For Medical Uses (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

La présente invention concerne un procédé d'obtention de fibres composites, comprenant la dispersion de particules colloïdales dans un solvant, l'injection de la dispersion dans un co-écoulement d'une solution de coagulation polymérique pour former une pré- fibre, la circulation de la pré-fibre dans une conduite, l'extraction, le lavage éventuel et le séchage de la pré- fibre pour obtenir une fibre, et le bobinage de la fibre ainsi obtenue, caractérisé en ce que le temps de résidence minimum de la pré-fibre au sein de la conduite est ajusté afin qu'elle ait une résistance mécanique suffisante pour être extraite de la conduite, et en ce que son extraction soit verticale continue. L'invention concerne également les fibres composites susceptibles d'être obtenues suivant ce procédé.
PCT/FR2008/051679 2007-09-18 2008-09-18 Procede continu d ' obtention de fibres composites a base de particules colloïdales et fibre obtenue par ce procede WO2009047456A2 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
US12/677,619 US20100196250A1 (en) 2007-09-18 2008-03-18 Continuous method for obtaining composite fibres containing colloidal particles and resulting fibre
CN200880107385A CN101802276A (zh) 2007-09-18 2008-09-18 获得基于胶粒的复合纤维的连续方法
JP2010524559A JP2010539342A (ja) 2007-09-18 2008-09-18 コロイド粒子を含む複合繊維の連続製造方法
EP08838292A EP2191045A2 (fr) 2007-09-18 2008-09-18 Procede continu d'obtention de fibres composites a base de particules colloidales et fibre obtenue par ce procede

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0706542 2007-09-18
FR0706542A FR2921075B1 (fr) 2007-09-18 2007-09-18 Procede continu d'obtention de fibres composites a base de particules colloidales et dispositif pour sa mise en oeuvre

Publications (2)

Publication Number Publication Date
WO2009047456A2 WO2009047456A2 (fr) 2009-04-16
WO2009047456A3 true WO2009047456A3 (fr) 2009-09-03

Family

ID=39495671

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2008/051679 WO2009047456A2 (fr) 2007-09-18 2008-09-18 Procede continu d ' obtention de fibres composites a base de particules colloïdales et fibre obtenue par ce procede

Country Status (7)

Country Link
US (1) US20100196250A1 (fr)
EP (1) EP2191045A2 (fr)
JP (1) JP2010539342A (fr)
KR (1) KR20100059874A (fr)
CN (1) CN101802276A (fr)
FR (1) FR2921075B1 (fr)
WO (1) WO2009047456A2 (fr)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2946178A1 (fr) 2009-05-27 2010-12-03 Arkema France Procede de fabrication d'une fibre conductrice multicouche par enduction-coagulation.
FR2946177B1 (fr) 2009-05-27 2011-05-27 Arkema France Procede de fabrication de fibres composites conductrices a haute teneur en nanotubes.
FR2978170B1 (fr) 2011-07-21 2014-08-08 Arkema France Fibres composites conductrices a base de graphene
DE102012004807A1 (de) * 2012-03-09 2013-09-12 Glanzstoff Bohemia S.R.O. Cellulosische Regeneratfasern und Verfahren zu deren Herstellung
JP5924103B2 (ja) * 2012-04-27 2016-05-25 東レ株式会社 カーボンナノチューブ分散液の製造方法
CN104718170A (zh) 2012-09-04 2015-06-17 Ocv智识资本有限责任公司 碳强化的增强纤维在含水或非水介质内的分散
WO2014065747A1 (fr) 2012-10-22 2014-05-01 Innventia Ab Procédé de filage de fibres ou d'extrusion, et produits obtenus
CN104746160A (zh) * 2013-12-27 2015-07-01 中国科学院上海硅酸盐研究所 红外透过率/反射率可变的纳米复合纤维以及制备方法
FR3019563B1 (fr) 2014-04-03 2016-04-29 Centre Nat Rech Scient Procede de preparation de fibres macroscopiques de dioxyde de titane par extrusion unidirectionnelle continue, fibres obtenues et applications
CN107002306B (zh) * 2015-07-24 2020-05-12 Lg化学株式会社 用于制造碳纳米管纤维的装置
GB201810746D0 (en) 2018-06-29 2018-08-15 Mereo Biopharma 3 Ltd Use of sclerostin antagonist
US20220380947A1 (en) * 2021-05-26 2022-12-01 Direct Air Capture, Llc Apparatus, system and method for making a carbon nanomaterial fiber and textiles from carbon dioxide and materials and materials and products thereof

Citations (3)

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WO2001063028A1 (fr) * 2000-02-23 2001-08-30 Centre National De La Recherche Scientifique (C.N.R.S.) Procede d'obtention de fibres et de rubans macroscopiques a partir de particules colloïdales, et notamment de nanotubes de carbone
WO2004074558A1 (fr) * 2003-02-19 2004-09-02 NANOLEDGE (Société Anonyme) Dispositif pour la fabrication de fibres et/ou de rubans, a partir de particules placees en suspension dans une premiere solution
WO2007101936A2 (fr) * 2006-03-06 2007-09-13 Nanoledge Procede de fabrication de produits extrudes composites polymeres et nanotubes de carbone

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US2711559A (en) * 1952-06-28 1955-06-28 Celanese Corp Viscose spinning process and apparatus
GB787557A (en) * 1953-09-02 1957-12-11 British Celanese Improvements in the production of artificial filamentary materials
US3393080A (en) * 1965-10-20 1968-07-16 Fmc Corp Microcrystalline colloidal collagen dispersions in dispersing media containing dimethyl sulfoxide and water-miscible organic solvents
US4663230A (en) * 1984-12-06 1987-05-05 Hyperion Catalysis International, Inc. Carbon fibrils, method for producing same and compositions containing same
JP3991602B2 (ja) * 2001-03-02 2007-10-17 富士ゼロックス株式会社 カーボンナノチューブ構造体の製造方法、配線部材の製造方法および配線部材

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001063028A1 (fr) * 2000-02-23 2001-08-30 Centre National De La Recherche Scientifique (C.N.R.S.) Procede d'obtention de fibres et de rubans macroscopiques a partir de particules colloïdales, et notamment de nanotubes de carbone
WO2004074558A1 (fr) * 2003-02-19 2004-09-02 NANOLEDGE (Société Anonyme) Dispositif pour la fabrication de fibres et/ou de rubans, a partir de particules placees en suspension dans une premiere solution
WO2007101936A2 (fr) * 2006-03-06 2007-09-13 Nanoledge Procede de fabrication de produits extrudes composites polymeres et nanotubes de carbone

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
VIGOLO B ET AL: "MACROSCOPIC FIBERS AND RIBBONS OF ORIENTED CARBON NANOTUBES", SCIENCE, WASHINGTON, DC, vol. 290, no. 290, 17 November 2000 (2000-11-17), pages 1331 - 1334, XP008004074, ISSN: 0036-8075 *

Also Published As

Publication number Publication date
FR2921075B1 (fr) 2010-03-12
FR2921075A1 (fr) 2009-03-20
WO2009047456A2 (fr) 2009-04-16
KR20100059874A (ko) 2010-06-04
US20100196250A1 (en) 2010-08-05
JP2010539342A (ja) 2010-12-16
CN101802276A (zh) 2010-08-11
EP2191045A2 (fr) 2010-06-02

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